journal article·2023-10

Influence of eutectic-Si in as-cast and fibrous-eutectic-Si in LPBF-processed AlSi10Mg alloys on wear and corrosion behaviors treated with direct aging route

A. Sathishkumar, R. Soundararajan, S. Sivasankaran, A. Ramesh

Journal of Materials Science· Volume 58· Issue 37
Publisher page

Abstract

This study investigates the wear and corrosion performance of AlSi10Mg alloy produced through casting and laser powder bed fusion (LPBF), followed by direct aging (DA) treatment at 180 °C for 6 h. Further, metallurgical characteristics and hardness performance were analyzed to assess the impact of DA heat treatment and to correlate the microstructure and the mechanical performances. Cast samples exhibited dendritic α-Al with eutectic Si, while LPBF samples showed a cellular structure with fibrous eutectic Si owing to the variation in the solidification rates of cast (~ 102 °C/s or less) and LPBF (103–106 °C/s) techniques. Besides, LPBF specimens displayed improved hardness (123.4 HV), a lower wear rate (0.92 × 10−5 g/m), and a coefficient of friction (0.27) compared to their cast counterparts, which exhibit the lowest hardness value of 98.7 HV, highest wear rate of 3.04 × 10−5 g/m and coefficient of friction of 0.395. Meanwhile, the DA treated AlSi10Mg alloy samples processed through LPBF possess the highest hardness of 131.6 HV, lowest wear rate (0.892 × 10−5 g/m) and coefficient of friction (0.26) among all the tested samples under a 10N applied load and 1 ms−1 sliding velocity condition, and this may be attributed to the hard nano-Si particles precipitated inside the cell boundary during the DA treatment. Furthermore, increasing the applied load from 10 to 40N and an increase in sliding velocity from 1 ms−1 to 5 ms−1 resulted in an increase and decrease in the wear rate, respectively. The worn SEM micrographs revealed mild delamination, avulsions, and uniform tribofilms on the worn surface, and the oxide films formed in the LPBF-processed AlSi10Mg alloy acted as a protective layer that reduced the rate of wear.
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Research context

OpenAlex topics: Additive Manufacturing Materials and Processes · Aluminum Alloy Microstructure Properties

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (61)

Show source-provided references
1. Maji P, Ghosh SK, Nath RK, Karmakar R (2020) Microstructural, mechanical and wear characteristics of aluminum matrix composites fabricated by friction stir processing. J Brazilian Soc Mech Sci Eng 42. https://doi.org/10.1007/s40430-020-02279-510.1007/s40430-020-02279-5 ↗
2. Li B, Wang H, Jie J, Wei Z (2011) Effects of yttrium and heat treatment on the microstructure and tensile properties of Al–7.5 Si–0.5 Mg alloy. Mater Des 32:1617–162210.1016/j.matdes.2010.08.040 ↗
3. Mazaheri Y, Heidarpour A, Jalilvand MM, Roknian M (2019) Effect of friction stir processing on the microhardness, wear and corrosion behavior of Al6061 and Al6061/SiO2 nanocomposites. J Mater Eng Perform 28:4826–483710.1007/s11665-019-04260-3 ↗
4. Hwang WJ, Bang GB, Choa S-H (2022) Effect of a Stress relief heat treatment of AlSi7Mg and AlSi10Mg alloys on mechanical and electrical properties according to silicon precipitation. Met Mater Int, 1–1210.1007/s12540-022-01304-7 ↗
5. Tan S, Wang Y, Liu W et al (2022) Anisotropy reduction of additively manufactured AlSi10Mg for metal mirrors. J Mater Sci 57:11934–11948. https://doi.org/10.1007/s10853-022-07080-410.1007/s10853-022-07080-4 ↗
6. Zhang X, Zhou Y, Zhong G et al (2022) Effects of Si and Sr elements on solidification microstructure and thermal conductivity of Al–Si-based alloys. J Mater Sci 57:6428–6444. https://doi.org/10.1007/s10853-022-07045-710.1007/s10853-022-07045-7 ↗
7. Park T-H, Baek M-S, Sohn Y, Lee K-A (2020) Effect of post-heat treatment on the wear properties of AlSi10Mg alloy manufactured by selective laser melting. Arch Metall Mater 65.10.1016/j.matchar.2021.111113 ↗
8. Read N, Wang W, Essa K, Attallah MM (2015) Selective laser melting of AlSi10Mg alloy: process optimisation and mechanical properties development. Mater Des 65:417–42410.1016/j.matdes.2014.09.044 ↗
9. Guan J, Wang Q (2022) The effect of a remelting treatment scanning strategy on the surface morphology, defect reduction mechanism, and mechanical properties of a selective laser-melted Al-based alloy. J Mater Sci 57:9807–9817. https://doi.org/10.1007/s10853-021-06761-w10.1007/s10853-021-06761-w ↗
10. Kang N, Mansori MEL (2020) A new insight on induced-tribological behaviour of hypereutectic Al-Si alloys manufactured by selective laser melting. Tribol Int 149:10575110.1016/j.triboint.2019.04.035 ↗
11. Alghamdi F, Haghshenas M (2019) Microstructural and small-scale characterization of additive manufactured AlSi10Mg alloy. SN Appl Sci 1:1–1010.1007/s42452-019-0270-5 ↗
12. Murugesan P, Satheeshkumar V, Jeyaprakash N, et al (2023) Effect of α-Al and Si precipitates on microstructural evaluation and corrosion behavior of laser powder bed fusion printed AlSi10Mg plates in seawater environment. Met Mater Int, 1–1810.1007/s12540-023-01394-x ↗
13. Zhao L, Song L, Macías JGS, et al (2022) Review on the correlation between microstructure and mechanical performance for laser powder bed fusion AlSi10Mg. Addit Manuf, 10291410.1016/j.addma.2022.102914 ↗
14. Hemachandra M, Thapliyal S, Adepu K (2022) A review on microstructural and tribological performance of additively manufactured parts. J Mater Sci 57:17139–17161. https://doi.org/10.1007/s10853-022-07736-110.1007/s10853-022-07736-1 ↗
15. Roveda I, Serrano-Munoz I, Mishurova T et al (2022) Influence of a 265 °C heat treatment on the residual stress state of a PBF-LB/M AlSi10Mg alloy. J Mater Sci 57:22082–22098. https://doi.org/10.1007/s10853-022-07997-w10.1007/s10853-022-07997-w ↗
16. Jalali M, Mohammadi K, Movahhedy MR, et al (2023) SLM additive manufacturing of NiTi porous implants: a review of constitutive models, finite element simulations, manufacturing, heat treatment, mechanical, and biomedical studies. Met Mater Int, 1–3410.1007/s12540-023-01401-1 ↗
17. Jia X, Xu Z, He Y et al (2023) Oxidation behavior of CoCrFeMnNi high-entropy alloy fabricated by selective laser melting. Met Mater Int, 1–1410.1007/s12540-023-01415-9 ↗
18. Zhang X, Chen L, Zhou J, Ren N (2020) Simulation and experimental studies on process parameters, microstructure and mechanical properties of selective laser melting of stainless steel 316L. J Brazilian Soc Mech Sci Eng 42:1–14. https://doi.org/10.1007/s40430-020-02491-310.1007/s40430-020-02491-3 ↗
19. Nikiel P, Wróbel M, Szczepanik S et al (2021) Microstructure and mechanical properties of Titanium grade 23 produced by selective laser melting. Arch Civ Mech Eng 21:1–16. https://doi.org/10.1007/s43452-021-00304-510.1007/s43452-021-00304-5 ↗
20. Wu J, Wang XQ, Wang W et al (2016) Microstructure and strength of selectively laser melted AlSi10Mg. Acta Mater 117:311–32010.1016/j.actamat.2016.07.012 ↗
21. Hadadzadeh A, Baxter C, Amirkhiz BS, Mohammadi M (2018) Strengthening mechanisms in direct metal laser sintered AlSi10Mg: comparison between virgin and recycled powders. Addit Manuf 23:108–120
22. Xi L, Wang P, Prashanth KG et al (2019) Effect of TiB2 particles on microstructure and crystallographic texture of Al-12Si fabricated by selective laser melting. J Alloys Compd 786:551–55610.1016/j.jallcom.2019.01.327 ↗
23. Wei P, Chen Z, Zhang S et al (2021) Effect of T6 heat treatment on the surface tribological and corrosion properties of AlSi10Mg samples produced by selective laser melting. Mater Charact 171:11076910.1016/j.matchar.2020.110769 ↗
24. Sander J, Hufenbach J, Giebeler L et al (2016) Microstructure and properties of FeCrMoVC tool steel produced by selective laser melting. Mater Des 89:335–34110.1016/j.matdes.2015.09.148 ↗
25. Girelli L, Tocci M, Gelfi M, Pola A (2019) Study of heat treatment parameters for additively manufactured AlSi10Mg in comparison with corresponding cast alloy. Mater Sci Eng A 739:317–32810.1016/j.msea.2018.10.026 ↗
26. Jägle EA, Sheng Z, Wu L et al (2016) Precipitation reactions in age-hardenable alloys during laser additive manufacturing. Jom 68:943–94910.1007/s11837-015-1764-2 ↗
27. Liu A, Chua CK, Leong KF (2010) Properties of test coupons fabricated by selective laser melting. In: Key engineering materials. Trans Tech Publ, pp 780–78410.4028/www.scientific.net/KEM.447-448.780 ↗
28. Dong S, Zhang X, Ma F et al (2020) Research on metallurgical bonding of selective laser melted AlSi10Mg alloy. Mater Res Express 7:2580110.1088/2053-1591/ab6dae ↗
29. Mishra AK, Upadhyay RK, Kumar A (2021) Surface wear anisotropy in AlSi10Mg alloy sample fabricated by selective laser melting: effect of hatch style, scan rotation and use of fresh and recycled powder. J Tribol 143:2170110.1115/1.4047788 ↗
30. Westlund V, Heinrichs J, Olsson M, Jacobson S (2016) Investigation of material transfer in sliding friction-topography or surface chemistry? Tribol Int 100:213–22310.1016/j.triboint.2016.01.022 ↗
31. Asgari H, Baxter C, Hosseinkhani K, Mohammadi M (2017) On microstructure and mechanical properties of additively manufactured AlSi10Mg_200C using recycled powder. Mater Sci Eng A 707:148–15810.1016/j.msea.2017.09.041 ↗
32. Barile C, Casavola C, Paramsamy Kannan V, Renna G (2022) The influence of AlSi10Mg recycled powder on corrosion-resistance behaviour of additively manufactured components: mechanical aspects and acoustic emission investigation. Arch Civ Mech Eng 22:1–16. https://doi.org/10.1007/s43452-022-00375-y10.1007/s43452-022-00375-y ↗
33. Maamoun AH, Elbestawi M, Dosbaeva GK, Veldhuis SC (2018) Thermal post-processing of AlSi10Mg parts produced by selective laser melting using recycled powder. Addit Manuf 21:234–247
34. Podgornik B, Šinko M, Godec M (2021) Dependence of the wear resistance of additive-manufactured maraging steel on the build direction and heat treatment. Addit Manuf 46:102123
35. Sitek R, Ciftci J, Moszczyńska D et al (2022) Effect of annealing on the microstructure and properties of IN 625 specimens manufactured by selective laser melting. Arch Civ Mech Eng 22:1–13. https://doi.org/10.1007/s43452-022-00522-510.1007/s43452-022-00522-5 ↗
36. Aboulkhair NT, Everitt NM, Ashcroft I, Tuck C (2014) Reducing porosity in AlSi10Mg parts processed by selective laser melting. Addit Manuf 1:77–86
37. Maleki E, Unal O, Bandini M et al (2022) Individual and synergistic effects of thermal and mechanical surface post-treatments on wear and corrosion behavior of laser powder bed fusion AlSi10Mg. J Mater Process Technol 302:11747910.1016/j.jmatprotec.2021.117479 ↗
38. Snopiński P, Woźniak A, Łukowiec D et al (2022) Evolution of microstructure, texture and corrosion properties of additively manufactured AlSi10Mg alloy subjected to equal channel angular pressing (ECAP). Symmetry (Basel) 14:67410.3390/sym14040674 ↗
39. Aboulkhair NT, Maskery I, Tuck C et al (2016) The microstructure and mechanical properties of selectively laser melted AlSi10Mg: the effect of a conventional T6-like heat treatment. Mater Sci Eng A 667:139–14610.1016/j.msea.2016.04.092 ↗
40. Shakil SI, Hadadzadeh A, Pirgazi H et al (2021) Indentation-derived creep response of cast and laser powder bed fused AlSi10Mg alloy: air temperature. Micron 150:10314510.1016/j.micron.2021.103145 ↗
41. Zhuo L, Wang Z, Zhang H et al (2019) Effect of post-process heat treatment on microstructure and properties of selective laser melted AlSi10Mg alloy. Mater Lett 234:196–20010.1016/j.matlet.2018.09.109 ↗
42. Alghamdi F, Song X, Hadadzadeh A et al (2020) Post heat treatment of additive manufactured AlSi10Mg: On silicon morphology, texture and small-scale properties. Mater Sci Eng A 783:13929610.1016/j.msea.2020.139296 ↗
43. Shakil SI, Hadadzadeh A, Amirkhiz BS et al (2021) Additive manufactured versus cast AlSi10Mg alloy: microstructure and micromechanics. Results Mater 10:10017810.1016/j.rinma.2021.100178 ↗
44. Prashanth KG, Debalina B, Wang Z et al (2014) Tribological and corrosion properties of Al–12Si produced by selective laser melting. J Mater Res 29:2044–205410.1557/jmr.2014.133 ↗
45. Cabrini M, Calignano F, Fino P et al (2018) Corrosion behavior of heat-treated AlSi10Mg manufactured by laser powder bed fusion. Materials (Basel) 11:105110.3390/ma11071051 ↗
46. Zhang C, Zhu H, Liao H et al (2018) Effect of heat treatments on fatigue property of selective laser melting AlSi10Mg. Int J Fatigue 116:513–52210.1016/j.ijfatigue.2018.07.016 ↗
47. Zakay A, Aghion E (2019) Effect of post-heat treatment on the corrosion behavior of AlSi10Mg alloy produced by additive manufacturing. Jom 71:1150–115710.1007/s11837-018-3298-x ↗
48. Kan WH, Huang S, Man Z et al (2021) Effect of T6 treatment on additively-manufactured AlSi10Mg sliding against ceramic and steel. Wear 482:20396110.1016/j.wear.2021.203961 ↗
49. Thasleem P, Kuriachen B, Kumar D et al (2021) Effect of heat treatment and electric discharge alloying on the tribological performance of selective laser melted AlSi10Mg. J Tribol 143:5111110.1115/1.4050897 ↗
50. Tonolini P, Montesano L, Tocci M et al (2021) Wear behavior of AlSi10Mg alloy produced by laser-based powder bed fusion and gravity casting. Adv Eng Mater 23:210014710.1002/adem.202100147 ↗
51. Rosenthal I, Shneck R, Stern A (2018) Heat treatment effect on the mechanical properties and fracture mechanism in AlSi10Mg fabricated by additive manufacturing selective laser melting process. Mater Sci Eng A 729:310–32210.1016/j.msea.2018.05.074 ↗
52. Park T-H, Baek M-S, Hyer H et al (2021) Effect of direct aging on the microstructure and tensile properties of AlSi10Mg alloy manufactured by selective laser melting process. Mater Charact 176:11111310.1016/j.matchar.2021.111113 ↗
53. Haghshenas M, Zarei-Hanzaki A, Fatemi-Varzaneh SM (2008) The effects of thermo-mechanical parameters on the microstructure of Thixocast A356 aluminum alloy. Mater Sci Eng A 480:68–7410.1016/j.msea.2007.06.075 ↗
54. Haghshenas M, Zarei-Hanzaki A, Jahazi M (2009) An investigation to the effect of deformation-heat treatment cycle on the eutectic morphology and mechanical properties of a Thixocast A356 alloy. Mater Charact 60:817–82310.1016/j.matchar.2009.01.020 ↗
55. Haghshenas M, Zarei-Hanzaki A, Sayed A (2010) Hot deformation behaviour of thixocast Al–Si–Mg alloy during compression at elevated temperatures. Mater Sci Technol 26:121–12610.1179/174328408X393422 ↗
56. Ramkumar KR, Radhika N, Sivasankaran S, Kim HS (2022) Evolution of microstructure and mechanical properties of [Cu–10Ni]–Si3N4 nanocomposites developed using mechanical alloying and spark plasma sintering. J Alloys Compd 899:16331910.1016/j.jallcom.2021.163319 ↗
57. Tonelli L, Liverani E, Morri A, Ceschini L (2021) Role of direct aging and solution treatment on hardness, microstructure and residual stress of the A357 (AlSi7Mg0. 6) alloy produced by powder bed fusion. Metall Mater Trans B 52:2484–249610.1007/s11663-021-02179-6 ↗
58. Fathi P, Mohammadi M, Duan X, Nasiri AM (2018) A comparative study on corrosion and microstructure of direct metal laser sintered AlSi10Mg_200C and die cast A360. 1 aluminum. J Mater Process Technol 259:1–1410.1016/j.jmatprotec.2018.04.013 ↗
59. Lakshmikanthan A, Bontha S, Krishna M et al (2019) Microstructure, mechanical and wear properties of the A357 composites reinforced with dual sized SiC particles. J Alloys Compd 786:570–58010.1016/j.jallcom.2019.01.382 ↗
60. Soundararajan R, Ali LF, Srinidhi MS, Prabhu TR (2022) Notch tensile and dry sliding wear studies on Mg-Nd-Gd-Zn alloy. Surf Topogr Metrol Prop 10:1505110.1088/2051-672X/ac5ebf ↗
61. Wu L, Zhao Z, Bai P et al (2020) Wear resistance of graphene nano-platelets (GNPs) reinforced AlSi10Mg matrix composite prepared by SLM. Appl Surf Sci 503:14415610.1016/j.apsusc.2019.144156 ↗