journal article·2022-06Open access

Metal fused filament fabrication of the nickel-base superalloy IN 718

Yvonne Thompson, Kai Zissel, Andreas Förner, Joamin Gonzalez-Gutierrez, Christian Kukla, Steffen Neumeier, Peter Felfer

Journal of Materials Science· Volume 57· Issue 21

Abstract

Abstract This study demonstrates metal fused filament fabrication (MF3) as an alternative additive and highly flexible manufacturing method for free-form fabrication of high-performance alloys. This novel processing, which is similar to Metal injection molding (MIM), enables a significant reduction in manufacturing costs for complex geometries, since expensive machining can be avoided. Utilizing existing equipment and reducing material expense, MF3 can pave the way for new and low-cost applications of IN 718, which were previously limited by high manufacturing costs. Iterative process optimization is used to find the most suitable MF3 process parameters. High relative density above 97% after pressureless sintering can be achieved if temperature profiles and atmospheres are well adjusted for thermal debinding and sintering. In this study, the influence of processing parameters on the resulting microstructure of MF3 IN 718 is investigated. Samples sintered in vacuum show coarse-grained microstructure with an area fraction of 0.36% NbC at grain boundaries. Morphology and composition of formed precipitates are analyzed using transmission electron microscopy and atom probe tomography. The γ/γ″/γ′ phases’ characteristics for IN 718 were identified. Conventional heat treatment is applied for further tailoring of mechanical properties like hardness, toughness and creep behavior. Fabricated samples achieve mechanical properties similar to MIM IN 718 presented in literature. Graphical abstract
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Research context

OpenAlex topics: Additive Manufacturing Materials and Processes · Additive Manufacturing and 3D Printing Technologies · Injection Molding Process and Properties

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References (46)

Show source-provided references
1. Akca E, Gürsel A (2015) A Review on Superalloys and IN718 Nickel-Based INCONEL Superalloy. PEN. https://doi.org/10.21533/pen.v3i1.4310.21533/pen.v3i1.43 ↗
2. Horke K, Meyer A, Singer RF (2019) Metal injection molding (MIM) of nickel-base superalloys. Handbook of Metal Injection Molding. Elsevier, pp 575–60810.1016/B978-0-08-102152-1.00028-3 ↗
3. Diehl W, Stöver D (1990) Injection moulding of superalloys and intermetallic phases. Met Powder Rep 45:333–338. https://doi.org/10.1016/S0026-0657(10)80241-310.1016/S0026-0657(10)80241-3 ↗
4. Valencia JJ, McCabc T, Hens K et al (1994) Microstructure and Mechanical Properties of Inconel 625 and 718 Alloys Processed by Powder Injection Molding. Superalloys 718, 625, 706 and Various Derivatives (1994). TMS, pp 935–94510.7449/1994/Superalloys_1994_935_945 ↗
5. AMS F Corrosion Heat Resistant Alloys Committee (2017) AMS5917 Metal Injection Molded Nickel Based Alloy 718 Parts Hot Isostatically Pressed, Solutioned and Aged
6. An XL, Zhou L, Zhang B (2019) Inconel 718 treated with two-stage solution and aging processes: microstructure evolution and enhanced properties. Materials Research Express 6:11. https://doi.org/10.1088/2053-1591/ab129010.1088/2053-1591/ab1290 ↗
7. Özgün Ö, Gülsoy HÖ, Yılmaz R, Fındık F (2013) Microstructural and mechanical characterization of injection molded 718 superalloy powders. J Alloys Compd 576:140–153. https://doi.org/10.1016/j.jallcom.2013.04.04210.1016/j.jallcom.2013.04.042 ↗
8. Chang L, Sun W, Cui Y, Yang R (2014) Influences of hot-isostatic-pressing temperature on microstructure, tensile properties and tensile fracture mode of Inconel 718 powder compact. Mater Sci Eng, A 599:186–195. https://doi.org/10.1016/j.msea.2014.01.09510.1016/j.msea.2014.01.095 ↗
9. Sidambe AT, Derguti F, Russell AD, Todd I (2013) Influence of processing on the properties of IN718 parts produced via Metal Injection Moulding. PIM Int 7:81–85
10. Thompson Y, Gonzalez-Gutierrez J, Kukla C, Felfer P (2019) Fused filament fabrication, debinding and sintering as a low cost additive manufacturing method of 316L stainless steel. Addit Manuf 30:100861. https://doi.org/10.1016/j.addma.2019.10086110.1016/j.addma.2019.100861 ↗
11. Gonzalez-Gutierrez J, Arbeiter F, Schlauf T et al (2019) Tensile properties of sintered 17–4PH stainless steel fabricated by material extrusion additive manufacturing. Mater Lett 248:165–168. https://doi.org/10.1016/j.matlet.2019.04.02410.1016/j.matlet.2019.04.024 ↗
12. Lieberwirth C, Harder A, Seitz H (2017) Extrusion based additive manufacturing of metal parts. JMEA. https://doi.org/10.17265/2159-5275/2017.02.00410.17265/2159-5275/2017.02.004 ↗
13. Gonzalez-Gutierrez J, Cano S, Ecker JV et al (2021) Bending properties of lightweight copper specimens with different infill patterns produced by material extrusion additive manufacturing. Solvent Debinding Sinter Appl Sci 11:7262. https://doi.org/10.3390/app1116726210.3390/app11167262 ↗
14. Thompson Y, Polzer M, Gonzalez-Gutierez J et al (2021) Fused filament fabrication-based additive manufacturing of commercially pure titanium. Adv Eng Mater. https://doi.org/10.1002/adem.20210038010.1002/adem.202100380 ↗
15. Miura H, Ikeda H, Iwahashi T, Osada T (2010) High temperature and fatigue properties of injection moulded superalloy compacts. In: Proceedings of the world powder metallurgy congress and exhibition, World PM 2010, vol 4
16. Youhua H, Yimin L, Hao H et al (2010) Preparation and mechanical properties of Inconel718 alloy by metal injection molding. Rare Met Mater Eng 39:775–780. https://doi.org/10.1016/S1875-5372(10)60100-210.1016/S1875-5372(10)60100-2 ↗
17. Kloeden B, Weissgaerber T, Kieback B, Langer I (2013) The processing and properties of metal injection moulded superalloys. Powder Inject Mould Int: PIM 7:53–66
18. Johnson JL, Tan LK, Suri P, German RM (2004) Mechanical properties and corrosion resistance of MIM Ni-based superalloys. In: PM2Tec2004. pp 89–101
19. Klöden B, Jehring U, Weißgärber T et al (2010) High temperature properties of MIM processed superalloys. Powder Inject Mould Int 4:63–67
20. Moussaoui K, Rubio W, Mousseigne M et al (2018) Effects of Selective Laser Melting additive manufacturing parameters of Inconel 718 on porosity, microstructure and mechanical properties. Mater Sci Eng, A 735:182–190. https://doi.org/10.1016/j.msea.2018.08.03710.1016/j.msea.2018.08.037 ↗
21. Popovich VA, Borisov EV, Popovich AA et al (2017) Functionally graded Inconel 718 processed by additive manufacturing: crystallographic texture, anisotropy of microstructure and mechanical properties. Mater Des 114:441–449. https://doi.org/10.1016/j.matdes.2016.10.07510.1016/j.matdes.2016.10.075 ↗
22. Diepold B, Vorlaufer N, Neumeier S et al (2020) Optimization of the heat treatment of additively manufactured Ni-base superalloy IN718. Int J Miner Metall Mater 27:640–648. https://doi.org/10.1007/s12613-020-1991-610.1007/s12613-020-1991-6 ↗
23. Gonzalez-Gutierrez J, Godec D, Kukla C, et al (2017) Shaping, debinding and sintering of steel components via fused filament fabrication. In: 16th international scientific conference on production engineering—computer integrated manufacturing and high speed machining. Zadar, Croatia
24. Burkhardt C, Freigassner P, Weber O, et al (2016) Fused Filament Fabrication (FFF) of 316L Green Parts for the MIM process. World PM 2016, Hamburg
25. Parenti P, Cataldo S, Grigis A et al (2019) Implementation of hybrid additive manufacturing based on extrusion of feedstock and milling. Procedia Manuf 34:738–746. https://doi.org/10.1016/j.promfg.2019.06.23010.1016/j.promfg.2019.06.230 ↗
26. Godec D, Cano S, Holzer C, Gonzalez-Gutierrez J (2020) Optimization of the 3D printing parameters for tensile properties of specimens produced by fused filament fabrication of 17–4PH stainless steel. Materials 13:774. https://doi.org/10.3390/ma1303077410.3390/ma13030774 ↗
27. Paramore JD, Fang ZZ, Dunstan M et al (2017) Hydrogen-enabled microstructure and fatigue strength engineering of titanium alloys. Sci Rep. https://doi.org/10.1038/srep4144410.1038/srep41444 ↗
28. Felfer P (2021) Atom Probe Toolbox. https://github.com/peterfelfer/Atom-Probe-Toolbox. Accessed 13 Sep 2021
29. Gonzalez-Gutierrez J, Thompson Y, Handl D et al (2021) Powder content in powder extrusion moulding of tool steel: dimensional stability, shrinkage and hardness. Mater Lett 283:128909. https://doi.org/10.1016/j.matlet.2020.12890910.1016/j.matlet.2020.128909 ↗
30. Rohrer GS (1948) Introduction to grains, phases, and interfaces—an interpretation of microstructure. Metall Mater Trans A 175:15–51
31. Coble RL (1961) Sintering crystalline solids. I. Intermediate and final state diffusion models. J Appl Phys 32:787–792. https://doi.org/10.1063/1.173610710.1063/1.1736107 ↗
32. German RM (2010) Coarsening in sintering: grain shape distribution, grain size distribution, and grain growth kinetics in solid-pore systems. Crit Rev Solid State Mater Sci 35:263–305. https://doi.org/10.1080/10408436.2010.52519710.1080/10408436.2010.525197 ↗
33. Ferreri NC, Vogel SC, Knezevic M (2020) Determining volume fractions of γ, γ′, γ″, δ, and MC-carbide phases in Inconel 718 as a function of its processing history using an advanced neutron diffraction procedure. Mater Sci Eng, A 781:139228. https://doi.org/10.1016/j.msea.2020.13922810.1016/j.msea.2020.139228 ↗
34. Sindhura D, Sravya MV, Murthy GVS (2019) Comprehensive Microstructural Evaluation of Precipitation in Inconel 718. Metallogr Microstruct Anal 8:233–240. https://doi.org/10.1007/s13632-018-00513-010.1007/s13632-018-00513-0 ↗
35. Cozar R, Pineau A (1973) Morphology of y’ and y” precipitates and thermal stability of inconel 718 type alloys. MT 4:47–59. https://doi.org/10.1007/BF0264960410.1007/BF02649604 ↗
36. Miller MK, Babu SS, Burke MG (2002) Comparison of the phase compositions in Alloy 718 measured by atom probe tomography and predicted by thermodynamic calculations. Mater Sci Eng, A 327:84–88. https://doi.org/10.1016/S0921-5093(01)01881-010.1016/S0921-5093(01)01881-0 ↗
37. Miller MK, Babu SS, Burke MG (1999) Intragranular precipitation in alloy 718. Mater Sci Eng, A 270:14–18. https://doi.org/10.1016/S0921-5093(99)00235-X10.1016/S0921-5093(99)00235-X ↗
38. Shi R, McAllister DP, Zhou N et al (2019) Growth behavior of, γ′/γ″ coprecipitates in Ni-Base superalloys. Acta Mater 164:220–236. https://doi.org/10.1016/j.actamat.2018.10.02810.1016/j.actamat.2018.10.028 ↗
39. Hajmrle K, Angers R, Dufour G (1982) Phase analysis of sintered and heat treated alloy 718. MTA 13:5–12. https://doi.org/10.1007/BF0264241010.1007/BF02642410 ↗
40. EOS GmbH (2020) EOS NickelAlloy IN718
41. Hayes RW (1991) Creep deformation of Inconel alloy 718 in the 650 °C to 760 °C temperature regime. Superalloys 718, 625 and various derivatives (1991). TMS, pp 549–56210.7449/1991/Superalloys_1991_549_562 ↗
42. Caliari FR, Candioto KCG, Couto AA et al (2016) Effect of double aging heat treatment on the short-term creep behavior of the Inconel 718. J Mater Eng Perform 25:2307–2317. https://doi.org/10.1007/s11665-016-2051-210.1007/s11665-016-2051-2 ↗
43. Pröbstle M, Neumeier S, Hopfenmüller J et al (2016) Superior creep strength of a nickel-based superalloy produced by selective laser melting. Mater Sci Eng, A 674:299–307. https://doi.org/10.1016/j.msea.2016.07.06110.1016/j.msea.2016.07.061 ↗
44. Han Y, Chaturvedi MC (1987) Steady state creep deformation of superalloy inconel 718. Mater Sci Eng 89:25–33. https://doi.org/10.1016/0025-5416(87)90246-110.1016/0025-5416(87)90246-1 ↗
45. Chaturvedi MC, Han Y (1989) Creep deformation of alloy 718. Superalloys 718 metallurgy and applications (1989). TMS, pp 489–49810.7449/1989/Superalloys_1989_489_498 ↗
46. Li S, Zhuang J, Yang J et al (1994) The effect of delta-phase on crack propagation under creep and fatigue conditions in alloy 718. Minerals Met Mater Soc 718:545–555