journal article·2020-03Open access

Measurements of thermophysical properties of solid and liquid NIST SRM 316L stainless steel

Peter Pichler, Brian J. Simonds, Jeffrey W. Sowards, Gernot Pottlacher

Journal of Materials Science· Volume 55· Issue 9

Abstract

Abstract In this work, we perform high accuracy measurements of thermophysical properties for the National Institute of Standards and Technology standard reference material for 316L stainless steel. As these properties can be sensitive to small changes in elemental composition even within the allowed tolerances for an alloy class, by selecting a publicly available standard reference material for study our results are particularly useful for the validation of multiphysics models of industrial metal processes. An ohmic pulse-heating system was used to directly measure the electrical resistivity, enthalpy, density, and thermal expansion as functions of temperature. This apparatus applies high current pulses to heat wire-shaped samples from room temperature to metal vaporization. The great advantage of this particular pulse-heating apparatus is the very short experimental duration of 50 $$\upmu {{\hbox {s}}}$$, which is faster than the collapse of the liquid wire due to gravitational forces, as well as that it prevents any chemical reactions of the hot liquid metal with its surroundings. Additionally, a differential scanning calorimeter was used to measure specific heat capacity from room temperature to around 1400 K. All data are accompanied by uncertainties according to the guide to the expression of uncertainty in measurement.
Source: crossref · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Calibration and Measurement Techniques · Chemical Thermodynamics and Molecular Structure · nanoparticles nucleation surface interactions

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (18)

Show source-provided references
1. Simonds BJ, Sowards J, Hadler J, Pfeif E, Wilthan B, Tanner J, Harris C, Williams P et al (2018) Time-resolved absorptance and melt pool dynamics during intense laser irradiation of a metal. Phys Rev Appl 10(4):044061. https://doi.org/10.1103/PhysRevApplied.10.04406110.1103/PhysRevApplied.10.044061 ↗
2. Jenkins R, Westover R (1962) Thermal diffusivity of stainless steel from 20$$\circ $$ to 1000$$\circ $$ C. J Chem Eng Data 7(3):434–437. https://doi.org/10.1021/je60014a03810.1021/je60014a038 ↗
3. Lucks C, Deem H (1958) Thermal properties of 13 metals: thermal properties of 13 metals. ASTM 9:795–795. https://doi.org/10.1002/maco.1958009121610.1002/maco.19580091216 ↗
4. Mills K (2002) Recommended values of thermophysical properties for selected commercial alloys. Woodhead Publishing, Sswston10.1533/9781845690144 ↗
5. Specification for Chromium and Chromium-Nickel Stainless Steel Plate, Sheet, and Strip for Pressure Vessels and for General Applications. https://doi.org/10.1520/a0240_a0240m-1710.1520/a0240_a0240m-17 ↗
6. Mills K, Su Y, Li Z, Brooks R (2004) Equations for the calculation of the thermo-physical properties of stainless steel. ISIJ Int 44(10):1661–1668. https://doi.org/10.2355/isijinternational.44.166110.2355/isijinternational.44.1661 ↗
7. Lippold L (1994) Solidification behavior and cracking susceptibility of pulsed-laser welds in austenitic stainless steels. Weld J 73(6):129–139
8. SRM 1155a (2013) AISI 316 Stainless Steel. National Institute of Standards and Technology; U.S. Department of Commerce, Gaithersburg, MD
9. Kaschnitz E, Pottlacher G, Jaeger H (1992) A new microsecond pulse-heating system to investigate thermophysical properties of solid and liquid metals. Int J Thermophys 13(4):699–710. https://doi.org/10.1007/bf0050195010.1007/bf00501950 ↗
10. Leitner M, Leitner T, Schmon A, Aziz K, Pottlacher G (2017) Thermophysical properties of liquid aluminum. Metall Mater Trans A 48:3036–3045. https://doi.org/10.1007/s11661-017-4053-610.1007/s11661-017-4053-6 ↗
11. Pearson Electronics I (2019) Pearson current monitor model 3025. http://www.pearsonelectronics.com/pdf/3025.pdf. Accessed 05 Apr
12. Huepf T (2010) Density determination of liquid metals: Ph.D. thesis, Graz University of Technology
13. Leitner M, Schroer W, Pottlacher G (2018) Density of liquid tantalum and estimation of critical point data. Int J Thermophys 39(11):124. https://doi.org/10.1007/s10765-018-2439-310.1007/s10765-018-2439-3 ↗
14. Wilthan B, Reschab H, Tanzer R, Schuetzenhoefer W, Pottlacher G (2008) Thermophysical properties of a chromium–nickel–molybdenum steel in the solid and liquid phases. Int J Thermophys 29(1):434–444. https://doi.org/10.1007/s10765-007-0300-110.1007/s10765-007-0300-1 ↗
15. Kaschnitz E, Kaschnitz H, Schleutker T, Guelhan A Bonvoisin B (2017) Electrical resistivity measured by millisecond pulse-heating in comparison to thermal conductivity of the stainless steel AISI 316L at elevated temperature. High Temp High Press 46
16. Fukuyama H, Higashi H, Yamano H (2019) Thermophysical properties of molten stainless steel containing 5 mass% B4C. Nucl Technol 0(0):1–10. https://doi.org/10.1080/00295450.2019.157857210.1080/00295450.2019.1578572 ↗
17. Joint Committee for Guides in Metrology (JCGM/WG 1), WG (ed) (1993) Guide to the expression of uncertainty in measurement: BIPM
18. Matus M (2005) Koeffizienten und Ausgleichsrechnung: Die Messunsicherheit nach GUM. Teil 1: Ausgleichsgeraden (Coefficients and adjustment calculations: measurement uncertainty under GUM. Part 1: best fit straight lines): tm—Technisches Messen 72(10/2005). https://doi.org/10.1524/teme.2005.72.10_2005.58410.1524/teme.2005.72.10_2005.584 ↗