journal article·2026-07Open access

Quantitative characterization of intrinsic plastic properties in carburized 18CrNiMo7-6 steel via dual sharp indentation

Guangtao Xu, Hengyang Wang, Guangzhao Han, Xuhui Zhang, Wenbiao Jian, Minghao Zhao

Abstract

: Residual stress significantly alters the load-depth response in sharp indentation, frequently resulting in inaccurate predictions of intrinsic mechanical properties. By incorporating the influence of initial stress on indentation curvature, an analytical framework is derived based on the energy density equivalence principle and the concept of representative strain, establishing an explicit relationship between representative stress, residual stress, loading curvature, and equivalent cone angle. Leveraging this theoretical foundation, a dual-sharp indentation method (DSIM) is proposed to identify the intrinsic plastic properties of metallic materials under equibiaxial residual stress. This framework operates on the premise of prior knowledge of the elastic modulus and residual stress, provided that the initial stress magnitude remains below the yield strength. The effectiveness and robustness of the DSIM are substantiated through systematic numerical simulations spanning a wide range of elastoplastic attributes, as well as experimental validations on four representative metallic materials. Furthermore, the methodology is implemented to characterize the carburized gradient layer of 18CrNiMo7-6 steel via layer-by-layer dual-sharp indentation, yielding the precise depth-dependent distribution of intrinsic plastic properties. The results demonstrate that compressive residual stress induces an overestimation of yield stress by up to 8.2% while concurrently leading to an underestimation of the strain-hardening exponent. This work achieves the mechanistic decoupling of the initial stress field from the constitutive response, providing a powerful tool for the localized micromechanical assessment of surface-modified components.
Source: openalex_inverted_index · Quality: baseline

Research context

OpenAlex topics: Metal and Thin Film Mechanics · Surface Treatment and Residual Stress · Microstructure and mechanical properties

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (28)

Show source-provided references
1. Recent progress in gradient-structured metals and alloys10.1016/j.pmatsci.2023.101194 ↗
2. Application of ultrasonic nanocrystal surface modification (UNSM) technique for surface strengthening of titanium and titanium alloys: a mini review10.1016/j.jmrt.2021.01.013 ↗
3. Indentation hardness measurements at macro-, micro-, and nanoscale: a critical overview10.1007/s11249-016-0805-5 ↗
4. A critical assessment of the effect of indentation spacing on the measurement of hardness and modulus using instrumented indentation testing
5. An improved technique for determining hardness and elastic modulus using load and displacement sensing indentation experiments10.1557/JMR.1992.1564 ↗
6. Plastic indentation in metals with cones10.1016/0022-5096(65)90018-9 ↗
7. Computational modeling of the forward and reverse problems in instrumented sharp indentation10.1016/S1359-6454(01)00295-6 ↗
8. Uniqueness of reverse analysis from conical indentation tests10.1557/JMR.2004.0306 ↗
9. On the uniqueness of measuring elastoplastic properties from indentation: the indistinguishable mystical materials10.1016/j.jmps.2007.01.010 ↗
10. Determination of plastic properties of metals by instrumented indentation using different sharp indenters10.1016/S1359-6454(02)00568-2 ↗
11. Depth-sensing instrumented indentation with dual sharp indenters10.1016/S1359-6454(03)00186-1 ↗
12. Influences of stress on the measurement of mechanical properties using nanoindentation: part I. Experimental studies in an aluminum alloy10.1557/JMR.1996.0091 ↗
13. Estimation of surface equi-biaxial residual stress by using instrumented sharp indentation10.1016/j.msea.2014.07.041 ↗
14. Recent advances in residual stress measurement10.1016/j.ijpvp.2007.10.007 ↗
15. Residual stress indentation model based on material equivalence10.1016/j.cja.2022.01.025 ↗
16. A novel model for obtaining both equi-biaxial and uniaxial residual stress of metallic materials by instrumented sharp indentation10.1016/j.ijpvp.2023.104942 ↗
17. Spherical indentation method for estimating equibiaxial residual stress and elastic–plastic properties of metals simultaneously10.1557/jmr.2018.57 ↗
18. Estimation of residual stress of metal material without plastic plateau by using continuous spherical indentation10.1016/j.ijpvp.2019.04.008 ↗
19. Determination of gradient residual stress for elastoplastic materials by nanoindentation10.1016/j.jmapro.2023.10.030 ↗
20. Theoretical model for predicting uniaxial stress-strain relation by dual conical indentation based on equivalent energy principle10.1016/j.actamat.2016.09.008 ↗
21. An elastoplastic energy model for predicting the deformation behaviors of various structural components10.1016/j.apm.2018.11.024 ↗
22. A novel flat indentation test method for obtaining stress–strain relationships of metallic materials based on energy density equivalence10.1016/j.ijsolstr.2023.112195 ↗
23. The correlation of indentation experiments10.1016/0022-5096(70)90029-3 ↗
24. Extended expanding cavity model for measurement of flow properties using instrumented spherical indentation10.1016/j.ijplas.2013.02.014 ↗
25. A machine learning perspective on the inverse indentation problem: uniqueness, surrogate modeling, and learning elasto-plastic properties from pile-up10.1016/j.jmps.2024.105557 ↗
26. Novel bulk triaxial residual stress mapping in an additive manufactured bridge sample by coupling energy dispersive X-ray diffraction and contour method measurements
27. Estimation of residual stress relaxation in low alloy steel with different hardness during fatigue by in situ X-ray measurement10.1016/j.ijfatigue.2023.107989 ↗
28. Determination of the mechanical properties of surface-modified layer of 18CrNiMo7-6 steel alloys after carburizing heat treatment10.1016/j.ijmecsci.2018.08.021 ↗