journal article·2026-07Open access

Towards restoring mechanical properties by aging only after friction screw extrusion additive manufacturing of Al–Mg–Si alloy

Saed Sayyad Rezaeinejad, Ton C. Bor, Martin Luckabauer, Remko Akkerman

Abstract

This study examines whether post-deposition aging alone, without solutionizing and quenching, can recover strength in AA6060 builds produced by friction screw extrusion additive manufacturing (FSEAM), a solid-state process that avoids melting-related defects. In FSEAM, the feedstock is preheated inside the printhead by a rotating threaded tool before deposition, which can generate temperatures high enough to dissolve strengthening precipitates. If cooling during deposition is sufficiently rapid, a supersaturated solid solution may be retained, enabling strength recovery by aging only. AA6060, an Al-Mg-Si alloy with a relatively low critical cooling rate, was selected to assess this concept. Builds were fabricated at deposition velocities of 100-500 mm/min. Samples produced above 200 mm/min showed no major defects, and printhead temperatures increased with deposition velocity, exceeding the alloy solvus temperature at velocities above 200 mm/min. After fabrication, samples were aged at 170 °C for 3 h and 20 h, omitting the conventional solutionizing and quenching steps of the full T6 treatment. Aging significantly increased hardness and strength, particularly in the top layers of builds processed above the solvus temperature. Hardness reached 85-88 HV, compared with about 76 HV for the T6 feedstock and 79 HV after a full T6 treatment. The ultimate tensile strength increased to approximately 230 MPa after aging-only, compared with about 211 MPa for the feedstock. These results indicate that solute supersaturation can be retained during FSEAM and exploited by post-deposition aging alone. The findings show that key elements of T6 strengthening can be partially integrated into FSEAM, reducing post-processing requirements.
Source: openalex_inverted_index · Quality: baseline

Research context

OpenAlex topics: Microstructure and mechanical properties · Metal Forming Simulation Techniques · Metallurgy and Material Forming

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (67)

Show source-provided references
1. Additive manufacturing Technologies- 3D printing
2. Additive manufacturing of metallic components – process, structure and properties10.1016/j.pmatsci.2017.10.001 ↗
3. Metal additive manufacturing: a review10.1007/s11665-014-0958-z ↗
4. Robotic wire-based friction stir additive manufacturing
5. Metal alloys for fusion-based additive manufacturing10.1002/adem.201700952 ↗
6. Challenges in additive manufacturing of high-strength aluminium alloys and current developments in hybrid additive manufacturing
7. Microstructure evolution and mechanical properties of Multilayer AA6061 alloy fabricated by additive friction stir deposition10.1007/s11661-024-07303-0 ↗
8. Solidification in metal additive manufacturing: challenges, solutions, and opportunities
9. Composition-dependent solidification cracking of aluminum-silicon alloys during laser powder bed fusion10.1016/j.actamat.2021.116698 ↗
10. Effect of post-deposition heat treatment on the mechanical behavior and deformation mechanisms of a solid-state additively manufactured al–mg–si alloy10.1115/1.4064179 ↗
11. Processing and characterization of crack-free 7075 aluminum alloys with elemental Zr modification by laser powder bed fusion
12. Relationship between process parameters and defects in laser powder bed fusion additive manufacturing of crack-sensitive al–cu–mg alloy10.1007/s11661-024-07498-2 ↗
13. Parameter study of an Al–Cr–Mo–Sc–Zr alloy processed by laser powder bed fusion reaching high build rates
14. Wires using multi-hole SolidStir extrusion
15. Challenges and opportunities in friction-based additive manufacturing of heat-treatable aluminum alloys10.3390/jmmp10060214 ↗
16. Friction stir welding and processing10.1016/j.mser.2005.07.001 ↗
17. Friction stir based welding, processing, extrusion and additive manufacturing10.1016/j.pmatsci.2024.101330 ↗
18. Microstructure evolution and mechanical properties of friction stir additive manufacturing for Al-6061 alloy builds under thermal cycling10.1016/j.jallcom.2025.180559 ↗
19. Linear and cylindrical friction stir additive manufacturing (FSAM) of AA6061-T6 by consumable rods: metallurgical structure, wear, and corrosion properties10.1007/s40194-024-01839-w ↗
20. Friction stir additive manufacturing of B4C and graphene reinforced aluminum matrix hybrid nanocomposites using consumable pins10.1016/j.jmrt.2023.12.065 ↗
21. Anisotropy and mechanical properties of dissimilar Al additive manufactured structures generated by multi-layer friction surfacing10.1007/s00170-022-10685-3 ↗
22. Additive friction stir deposition of aluminum alloys: a critical review10.1016/j.matdes.2025.114543 ↗
23. A novel approach for enhanced mechanical properties in solid-state additive manufacturing by additive friction stir deposition using thermally stable al-ce-mg alloy10.1007/s11837-023-06044-6 ↗
24. Microstructure evolution and tensile behaviour of fine-grained 6082 Al wire with high ultimate strength and high work hardening by friction stir extrusion of bulk Al sheet10.1016/j.msea.2023.144589 ↗
25. Investigation on in-situ tensile behaviors of 6061 aluminum alloy fabricated by wire additive friction stir deposition10.1016/j.jallcom.2024.176780 ↗
26. 3D printing of fine-grained aluminum alloys through extrusion-based additive manufacturing: microstructure and property characterization10.1016/j.jmst.2022.08.017 ↗
27. Advances in additive friction extrusion deposition (AFED): process and tool design10.3390/jmmp8020057 ↗
28. The effect of solutionizing and artificial aging on the microstructure and mechanical properties in solid-state additive manufacturing of precipitation hardened Al–Mg–Si alloy10.1016/j.msea.2021.141351 ↗
29. Friction screw extrusion additive manufacturing of an Al-Mg-Si alloy
30. Solid-state additive manufacturing of AA6060 employing friction screw extrusion additive manufacturing
31. SolidStir additive manufacturing: a novel deformation-based additive manufacturing using friction stir technology
32. Bor · 2023 · 27
33. The influence of the deposition speed during friction screw extrusion additive manufacturing of AA606010.4028/p-05VfP4 ↗
34. Additive manufacturing and mechanical properties of the dense and crack free Zr-modified aluminum alloy 6061 fabricated by the laser-powder bed fusion
35. Heat treatment of 7xxx series aluminium alloys—Some recent developments10.1016/S1003-6326(14)63306-9 ↗
36. Precipitation hardening: unravelling mechanisms of trade-off between strength and ductility/formability of Al-Mg-Si alloys10.1016/j.jallcom.2025.178443 ↗
37. Precipitation behavior in an Al–Cu–Mg–Si alloy during ageing10.1016/j.msea.2019.138369 ↗
38. Precipitation phenomena in ultrafine grained Al–Mg–Si alloy with heterogeneous microstructure10.1016/j.actamat.2015.10.030 ↗
39. Precipitation processes in Al–Mg–Si extending down to initial clustering revealed by the complementary techniques of positron lifetime spectroscopy and dilatometry10.1007/s10853-018-2612-x ↗
40. Mechanisms controlling the artificial aging of Al–Mg–Si alloys10.1016/j.actamat.2011.02.010 ↗
41. Diffusion on demand to control precipitation aging: application to al-mg-si alloys10.1103/PhysRevLett.112.225701 ↗
42. Additive manufacturing of commercial Al–Zn–Mg–Cu aluminum alloys with mechanical properties comparable to extruded counterparts
43. Influence of aging time to achieve tensile build direction heat treated T74 forging properties in lubricant free AFSD AA7050
44. Study of microstructure evolution and mechanical properties in friction stir based additive multi-layer manufacturing of Al 6061 alloy: effect of feedstock material form and heat treatment
45. The effect of heat treatment on the microstructure and mechanical properties of 6082 aluminum alloy manufactured by friction stir additive10.1016/j.matchar.2024.114680 ↗
46. Review of the quench sensitivity of aluminium alloys: analysis of the kinetics and nature of quench-induced precipitation10.3390/ma12244083 ↗
47. Production of nanocomposite parts using AA6061-T6 consumable rods via friction stir method: a novel approach of solid-state additive manufacturing of CNT-reinforced aluminum matrix nanocomposites
48. Continuous cooling precipitation diagrams of Al–Mg–Si alloys10.1016/j.msea.2012.04.033 ↗
49. Additive friction stir deposition of a tantalum–tungsten refractory alloy10.3390/jmmp8040177 ↗
50. Initial characterization of the layer interface for graphite-free additive friction stir deposition of AA707510.3390/met15060614 ↗
51. Quantitative volumetric identification of precipitates in dilute alloys using high-precision isothermal dilatometry10.1080/09500839.2018.1542170 ↗
52. Microstructure evolution and strengthening mechanisms of an additive friction stir deposited multi-layer Al-Mg-Sc-Zr alloy10.1016/j.jallcom.2024.175783 ↗
53. The precipitation sequence in Al–Mg–Si alloys10.1016/S1359-6454(98)00059-7 ↗
54. Hall–Petch relation and boundary strengthening10.1016/j.scriptamat.2004.06.002 ↗
55. Serrated flow of aluminium alloys influenced by precipitates10.1016/S0921-5093(99)00650-4 ↗
56. Kinetics of the portevin-le chatelier effect in Al 6061 alloy10.1016/0001-6160(85)90148-8 ↗
57. Mechanism of low temperature deformation in aluminium alloys10.1016/j.msea.2020.139935 ↗
58. The influence of additive friction stir deposition process on mechanical properties, corrosion resistance, and electrical conductivity of Al5086-H32 alloy
59. Particle-based friction stir additive manufacturing of an Al-Mg-Mn alloy
60. 1991 · 841
61. The influence of temperature and storage time at RT on nucleation of the β″ phase in a 6082 Al–Mg–Si alloy10.1016/S1359-6454(02)00470-6 ↗
62. Influence of natural aging on the formability of Al-Mg-Si alloy blanks10.1016/j.jmapro.2023.03.021 ↗
63. An investigation on application of friction stir additive manufacturing (FSAM) for the production of AA6061/TiC-graphene hybrid nanocomposite in the shape of multi-layer cylindrical part10.1016/j.jmrt.2024.05.043 ↗
64. Understanding the impact of cooling systems on bulk additive friction stir deposition of aluminum10.3390/met16040382 ↗
65. The effect of cooling temperature on microstructure and mechanical properties of Al 6061-T6 aluminum alloy during submerged friction stir welding10.3390/met13071159 ↗
66. Exploring temperature-controlled friction stir powder additive manufacturing process for multi-layer deposition of aluminum alloys10.1016/j.jmrt.2022.07.049 ↗
67. Structure determination of Mg5Si6 particles in Al by dynamic electron diffraction studies10.1126/science.277.5330.1221 ↗