Semi-in-situ EBSD reveals decoupled morphological and crystallographic texture effects on early plasticity in SLM 316L stainless steel
Source abstract
Abstract
SLM 316L stainless steel contains a hierarchical microstructure, including columnar grains, EBSD-resolved low-angle boundary networks, and crystallographic texture. How these features jointly control early plastic anisotropy remains unclear. This study investigates the orientation-dependent deformation of stress-relieved SLM 316L using tensile testing and semi-in-situ EBSD. Miniature dog-bone specimens with tensile axes of 0°, 45° and 90° were interrupted at 0%, 2% and 10% engineering strain. Kernel average misorientation, geometrically necessary dislocation density, grain orientation spread, and Schmid-factor-based slip-tendency descriptors were analyzed to separate crystallographic slip tendency from morphological constraint. The 45° specimen showed the highest stress level during early yielding, followed by the 0° specimen, whereas the 90° specimen exhibited the lowest resistance to plastic flow. At 2% strain, the 45° specimen developed the largest increase in median GND density and high-GND area fraction, although the 90° specimen showed the highest maximum Schmid factor, m max , and the strongest multi-slip tendency. This mismatch shows that crystallographic slip tendency alone cannot explain early strain partitioning. From 2% to 10% strain, the 45° specimen also showed the largest increases in GND density and GOS, indicating sustained lattice-curvature accumulation and grain-scale orientation dispersion. Regional analysis further showed that LAGB-associated regions preferentially accumulated GND and KAM at 2%, while this contrast weakened at 10%. These results reveal that early plastic anisotropy in SLM 316L is governed by the coupling between crystallographic slip tendency, columnar morphological texture and retained low-angle boundary network.
Source: openalex_inverted_index · Quality: baseline
Research context
OpenAlex topics: Microstructure and mechanical properties · Hydrogen embrittlement and corrosion behaviors in metals · Microstructure and Mechanical Properties of Steels
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (47)
Show source-provided references
1. Additive manufacturing of AISI 316L stainless steel: a review10.3390/met13081370 ↗
2. Process parameter selection and optimization of laser powder bed fusion for 316L stainless steel: a review10.1016/j.jmapro.2021.12.064 ↗
3. Selective laser melting of stainless-steel: a review of process, microstructure, mechanical properties and post-processing treatments
4. Selective laser melting of stainless steels: a review of process, microstructure and properties10.1007/s12540-024-01650-8 ↗
5. In-situ laser shock peening for the fabrication of micro-textured cutting tool and mechanistic study of wear resistance
6. Prediction of laser cutting parameters for polymethylmethacrylate sheets using random vector functional link network integrated with equilibrium optimizer10.1007/s10845-020-01617-7 ↗
7. Surface quality measures analysis and optimization on machining titanium alloy using CO2 based laser beam drilling process10.1016/j.jmapro.2020.12.008 ↗
8. Investigation and TGRA based optimization of laser beam drilling process during machining of Nickel Inconel 718 alloy10.1016/j.jmrt.2022.02.112 ↗
9. Experimental investigation on laser cutting of PMMA sheets: effects of process factors on kerf characteristics10.1016/j.jmrt.2021.01.012 ↗
10. Additively manufactured hierarchical stainless steels with high strength and ductility10.1038/nmat5021 ↗
11. The effect of post-processing heat treatment on the microstructure, residual stress and mechanical properties of selective laser melted 316L stainless steel10.1016/j.msea.2021.141611 ↗
12. Thermal stability of hierarchical microstructural features in additively manufactured stainless steel10.1016/j.heliyon.2023.e16555 ↗
13. Investigation of microstructures and tensile properties of 316L stainless steel fabricated via laser powder bed fusion10.3390/ma17040913 ↗
14. Multi-scale characterisation of microstructure and texture of 316L stainless steel manufactured by laser powder bed fusion10.1016/j.matchar.2021.111663 ↗
15. A large-volume 3D EBSD study on additively manufactured 316L stainless steel10.1016/j.scriptamat.2023.115723 ↗
16. Cell structure in steels induced by additive manufacturing10.1177/02670836241255257 ↗
17. Delineating the ultra-low misorientation between the dislocation cellular structures in additively manufactured 316L stainless steel10.3390/ma17081851 ↗
18. Additive-manufacturing-induced cell structure in stainless steel 316L: 3D morphology and formation mechanism10.1007/s11661-024-07644-w ↗
19. Formation of two distinct cellular structures in 316L stainless steel fabricated by micro-laser beam powder-bed-fusion10.1080/21663831.2023.2292076 ↗
20. Microstructure and anisotropy of the mechanical properties of 316L stainless steel fabricated by selective laser melting10.3390/met11050775 ↗
21. Study on mechanism of structure angle on microstructure and properties of SLM-fabricated 316L stainless steel10.3389/fbioe.2021.778332 ↗
22. Mechanical anisotropy of additively manufactured stainless steel 316L: an experimental and numerical study10.1016/j.msea.2020.140154 ↗
23. An investigation of the anisotropic mechanical properties of additive-manufactured 316L SS with SLM10.3390/ma17092017 ↗
24. Anisotropy of mechanical property and fracture mechanism for SLM 316L stainless steel under quasi-uniaxial and biaxial tensile loadings10.1016/j.msea.2025.147960 ↗
25. Anisotropic spall failure of additively manufactured 316L stainless steel
26. Non-equilibrium microstructure, crystallographic texture and morphological texture synergistically result in unusual mechanical properties of 3D printed 316L stainless steel
27. Texture dependent strain hardening in additively manufactured stainless steel 316L10.1016/j.msea.2021.141483 ↗
28. Control of texture and microstructure in additive manufacturing of stainless steel 316L10.1016/j.jallcom.2023.173040 ↗
29. Crystallographic-orientation-dependent tensile behaviours of stainless steel 316L fabricated by laser powder bed fusion10.1016/j.msea.2019.138395 ↗
30. 316L austenitic stainless steel thin-walls fabricated via arc-based directed energy deposition: constitutive model description of anisotropic mechanical properties10.1016/j.conbuildmat.2024.139793 ↗
31. On the development of twinning-induced plasticity in additively manufactured 316L stainless steel
32. Strengthening mechanisms and strain hardening behavior of 316L stainless steel manufactured by laser-based powder bed fusion10.1002/adem.202201230 ↗
33. Investigation of porosity, texture, and deformation behavior using high energy X-rays during in-situ tensile loading in additively manufactured 316L stainless steel10.1016/j.msea.2021.141034 ↗
34. Process-induced micromechanics variations in additively manufactured 316 stainless steel characterised by quasi-in-situ EBSD10.1016/j.scriptamat.2025.117159 ↗
35. In-situ EBSD investigation of orientation induced mechanical anisotropy in selective laser melted aluminum alloy10.1080/21663831.2023.2255218 ↗
36. Process parameter selection and optimization of laser powder bed fusion for 316L stainless steel: a review10.1016/j.jmapro.2021.12.064 ↗
37. The effect of post-processing heat treatment on the microstructure, residual stress and mechanical properties of selective laser melted 316L stainless steel10.1016/j.msea.2021.141611 ↗
38. Stress relieving heat treatment of 316L stainless steel made by additive manufacturing process10.3390/ma16196461 ↗
39. Introduction and comparison of new EBSD post-processing methodologies10.1016/j.ultramic.2015.08.001 ↗
40. A step size dependence of KAM, GROD and GND parameters calculated from EBSD
41. Some geometrical relations in dislocated crystals10.1016/0001-6160(53)90054-6 ↗
42. Assessment of geometrically necessary dislocation levels derived by 3D EBSD10.1016/j.actamat.2015.06.051 ↗
43. Consistent determination of geometrically necessary dislocation density from simulations and experiments10.1016/j.ijplas.2018.05.001 ↗
44. A new grain orientation spread approach to analyze the dynamic recrystallization behavior of a cast-homogenized Mg-Zn-Zr alloy using electron backscattered diffraction10.1016/j.msea.2017.10.062 ↗
45. On the effect of slip transfer at grain boundaries on the strength of FCC polycrystals
46. Analysis of slip transfer across grain boundaries in Ti via diffraction contrast tomography and high-resolution digital image correlation: when the geometrical criteria are not sufficient10.1016/j.ijplas.2024.103941 ↗
47. Microscale residual stresses in additively manufactured stainless steel10.1038/s41467-019-12265-8 ↗