Hot deformation behavior and processing optimization of a Co–Ni secondary hardening steel: Constitutive modeling, processing maps and microstructural analysis
Source abstract
Abstract
The hot deformation behavior of a Co–Ni secondary hardening steel was investigated using Gleeble-3800 compression tests at 900–1150 °C and strain rates of 0.05–5 s –1 . A strain-compensated Arrhenius-type constitutive model based on the hyperbolic sine law was established using friction- and temperature-corrected flow stress data. The activation energy was determined to be 447 kJ·mol –1 , indicating high deformation resistance during hot deformation. The model showed high fitting and predictive accuracy within the investigated deformation domain. Processing maps based on the dynamic materials model reveal that high power dissipation efficiency domains were mainly located at 1000–1150 °C, whereas flow instability occurs under low-temperature and high-strain-rate conditions. EBSD analysis shows a transition from elongated deformed grains to more equiaxed recrystallized microstructures with increasing temperature and decreasing strain rate, accompanied by a reduction in KAM values. The dominant softening mechanism evolved from work hardening to dynamic recovery and dynamic recrystallization. An optimal processing window of 1000–1050 °C was identified over the entire investigated strain-rate range of 0.05–5 s –1 , where flow instability can be avoided while stable deformation and refined microstructures can be simultaneously achieved.
Source: openalex_inverted_index · Quality: baseline
Research context
OpenAlex topics: High Temperature Alloys and Creep · Metallurgy and Material Forming · Microstructure and Mechanical Properties of Steels
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (40)
Show source-provided references
1. Design of a 2.7 GPa ultra-high-strength high Co–Ni secondary hardening steel by two-step nano-size precipitation tailoring10.1016/j.jmrt.2024.01.038 ↗
2. Microstructures and mechanical properties of novel 2.3 GPa secondary hardening steels with different Ni contents10.1016/j.jmrt.2025.01.017 ↗
3. Effects of Co on Mechanical Properties and precipitates in a novel secondary−hardening steel with duplex strengthening of M2C and β−NiAl10.3390/ma17133261 ↗
4. Novotny PM, McCaffrey TJ. An advanced alloy for landing - gear and aircraft structural applications AerometrB 100 alloy n.d.
5. Role of microstructural characteristics in combination of strength and fracture toughness of Laser additively manufactured ultrahigh-strength AerMet100 steel10.1007/s11661-021-06148-1 ↗
6. Influence of microstructure on strain-controlled fatigue and fracture behavior of ultra high strength alloy steel AerMet 10010.1016/j.msea.2014.01.094 ↗
7. Progress on improving strength-toughness of ultra-high strength martensitic steels for aerospace applications: a review10.1016/j.jmrt.2022.12.177 ↗
8. Effect of ageing temperature on the microstructural evolution and mechanical properties in M2C and NiAl co-precipitation secondary hardening ultrahigh-strength steel10.1016/j.jmrt.2024.04.116 ↗
9. Concomitant precipitation of Intermetallic β-NiAl and carbides in a precipitation hardened steel10.1007/s11661-023-07291-7 ↗
10. Effects of NiAl on precipitation behavior and mechanical properties of M2C strengthened secondary hardening steel10.1016/j.jmrt.2025.02.002 ↗
11. Making low alloy ultrahigh strength steel tough by high-density NiAl clusters10.1016/j.matchar.2025.115480 ↗
12. Hot deformation behavior of Fe-25Mn-12Al-1C-3.5Ni low-density steel: constitutive analysis and processing maps10.1007/s10853-025-11272-z ↗
13. Abdelghany
14. Dynamic recrystallization: plasticity enhancing structural development10.1016/j.jallcom.2003.10.067 ↗
15. Deformation mechanisms in ultrafine-grained metals with an emphasis on the Hall–Petch relationship and strain rate sensitivity10.1016/j.jmrt.2021.06.016 ↗
16. Strain rate dependent constitutive behavior investigation of AerMet 100 steel10.1016/j.matdes.2015.08.063 ↗
17. High-strain-rate behavior of maraging steel linear cellular alloys: mechanical deformations10.1016/j.msea.2011.11.093 ↗
18. Constitutive modelling of a new high-strength low-alloy steel using modified Zerilli–Armstrong and arrhenius model10.1007/s12666-019-01763-4 ↗
19. Strength and structure under hot-working conditions10.1179/095066069790138056 ↗
20. On the mechanism of hot deformation10.1016/0001-6160(66)90207-0 ↗
21. High-temperature hot deformation behavior and processing map of Ti-22Al-25Nb alloy
22. Evaluation of the deformation behaviors and hot workability of a high-strength low-alloy steel10.1016/j.msea.2021.141031 ↗
23. The microstructural origin of work hardening stages10.1016/j.actamat.2018.02.002 ↗
24. High-temperature deformation behavior and recrystallization mechanism of a near beta titanium alloy Ti-55511 in β phase region10.1016/j.msea.2022.143335 ↗
25. A one-parameter approach to determining the critical conditions for the initiation of dynamic recrystallization10.1016/1359-6454(95)00146-7 ↗
26. Dynamic recrystallization kinetics model of X70 pipeline steel10.1016/j.matdes.2012.02.034 ↗
27. Microstructure prediction of 80MnSi8-6 steel after hot deformation based on dynamic recrystallization kinetics and FEM simulation10.1007/s11837-024-06648-6 ↗
28. Prediction of flow stress for hot deformation processing10.1016/j.commatsci.2012.11.054 ↗
29. Correction of flow stress data due to non-homogeneous deformation and thermal conditions during hot compression testing of a polycrystalline nickel-base superalloy10.1007/s10853-020-05714-z ↗
30. Constitutive modelling and microstructural analysis of 92W-5Co-3Ni alloy subjected to high strain rate testing at elevated temperatures10.1016/j.matdes.2025.114035 ↗
31. A systematic study on thermo-mechanical behavior, processing maps and recrystallization mechanism of Incoloy825 superalloy during hot compression10.1016/j.jmrt.2024.01.042 ↗
32. Constitutive modeling and prediction of hot deformation flow stress under dynamic recrystallization conditions10.1016/j.mechmat.2015.02.014 ↗
33. Quantitative description of the flow-stress dependence of aluminum alloys at the stage of steady flow upon hot deformation on the Zener–Hollomon parameter10.1134/S0031918X17090046 ↗
34. A new mathematical model for predicting flow stress up to the critical strain during hot deformation10.1016/j.matdes.2014.09.072 ↗
35. A comparative study of phenomenological, physically-based and artificial neural network models to predict the hot flow behavior of API 5CT-L80 steel
36. Establishment and validity verification of the hot processing map of a Ti-47.5Al-2.5V-1.0Cr-0.2Zr alloy with a lamellar microstructure10.1016/j.matchar.2021.111599 ↗
37. Investigation on the hot deformation behavior of powder metallurgy TiAl-based alloy using 3D processing map10.1016/j.matchar.2014.12.011 ↗
38. Hot working characteristics of nimonic 75, 80A and 90 superalloys: a comparison using processing maps10.1016/0924-0136(94)01602-W ↗
39. Correlation between strain-rate sensitivity and dynamic softening behavior during hot processing10.1016/j.jallcom.2014.12.270 ↗
40. Softening mechanisms and microstructure evolution of 42CrMo steel during hot compressive deformation10.1016/j.jmrt.2023.02.141 ↗