journal article·2026-05Open access

Enhanced ductility of a 18Ni-300 maraging steel produced by directed energy deposition using cyclic austenitisation.

H. Huttenschmitt, J. Hugues, F. Galliano, D. Poquillon, M. Dehmas, B. Viguier

Abstract

This study focuses on maraging steel 18Ni-300 produced using directed energy deposition (DED). Electrical resistivity was successfully implemented to investigate the α′↔γ transformation during the austenitisation heat treatment. It was found that this transformation occurs in two steps: the first is governed by a diffusion-controlled mechanism involving local equilibrium with partitioning (PLE), while the second involves local equilibrium with negligible partitioning (NPLE). Thanks to the resistivimetric study, the transformation kinetics were monitored and compared between the DED alloy and a wrought reference sample. The two-steps transformation induces chemical segregation in the microstructure, which can be reduced by holding the sample at high temperature or, conversely, enhanced through short austenitic cycling, as demonstrated in this study. Applying five cycles of 15 min at 820 °C to the DED-processed steel resulted in both microstructural refinement and an increase in austenite content, which reached 5.3 vol %. This treatment also induced a significant increase in the ductility of the DED alloy, despite its anisotropy.
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Research context

OpenAlex topics: Surface Treatment and Residual Stress · Additive Manufacturing Materials and Processes · High Entropy Alloys Studies

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References (44)

Show source-provided references
1. 1990
2. Effects of aging time on the microstructure and mechanical properties of laser-cladded 18Ni300 maraging steel10.1007/s10853-021-05841-1 ↗
3. Comparative study of the influence of heat treatment and additive manufacturing process (LMD & L-PBF) on the mechanical properties of specimens manufactured from 1.270910.3390/cryst13020157 ↗
4. Mechanical properties of lamellar-structured 18Ni300 maraging steel manufactured via directed energy deposition10.1016/j.msea.2023.146031 ↗
5. Influence of processing parameters and heat treatment on the mechanical properties of 18Ni300 manufactured by laser based directed energy deposition10.1016/j.optlastec.2018.03.011 ↗
6. Phase chemistry and precipitation reactions in maraging steels: part IV. Discussion and conclusions10.1007/BF02668193 ↗
7. Precipitation and austenite reversion behavior of a maraging steel produced by selective laser melting10.1557/jmr.2014.204 ↗
8. Effect of the as-built microstructure on the martensite to austenite transformation in a 18Ni maraging steel after laser-based powder bed fusion
9. Structural transformations produced during tempering of fe-ni-co-mo alloys10.1007/BF00566241 ↗
10. Tailoring the nanostructure of laser powder bed fusion additively manufactured maraging steel
11. Precipitation hardening in 350 grade maraging steel10.1007/BF02646522 ↗
12. Increased fracture toughness in a 300 grade maraging steel as a result of thermal cycling10.1007/BF02644658 ↗
13. Effect of thermal cycling on the mechanical properties of 350-grade maraging steel10.1007/BF02648963 ↗
14. Effect of thermal cycling and aging stages on the microstructure and bending strength of a selective laser melted 300-grade maraging steel10.1016/j.msea.2019.03.129 ↗
15. Effect of a direct aging heat treatment on the microstructure and the tensile properties of a 18Ni-300 maraging steel produced by laser powder bed fusion10.1016/j.msea.2023.144921 ↗
16. Mechanical properties and microstructure of laser powder bed fusion‐processed 18Ni300 maraging steel according to direct aging treatment conditions10.1002/srin.202400348 ↗
17. Effect of aging treatment on the microstructure and tribological properties of a new maraging steel manufactured by laser directed energy deposition10.1016/j.matchar.2024.113767 ↗
18. 2019
19. Comparison of maraging steel Micro- and nanostructure produced conventionally and by laser additive manufacturing10.3390/ma10010008 ↗
20. Dilatometric technique for evaluation of the kinetics of solid-state transformation of maraging steel
21. Quantification of phase transformation kinetics of 18 wt. % Ni C250 maraging steel10.1016/j.msea.2004.01.040 ↗
22. Characterization of phase transformation and strengthening mechanisms in a novel maraging steel produced using laser-based powder bed fusion10.1016/j.matchar.2023.113522 ↗
23. Reaction kinetics in differential thermal analysis10.1021/ac60131a045 ↗
24. Building a continuous cooling transformation diagram of β- CEZ alloy by metallography and electrical resistivity measurements10.1007/s11661-997-0004-y ↗
25. Control of retained austenite stability during the heat treatment of the high performance steel ferrium® M54®10.1016/j.jmrt.2025.03.230 ↗
26. A dilatometric study of the phase transformations in 300 and 350 maraging steels during continuous heating rates10.1590/S1516-14392013005000069 ↗
27. The phase transitions in selective laser-melted 18-NI (300-grade) maraging steel10.1007/s10973-020-09316-4 ↗
28. Composition equivalents of stainless steels understood via gamma stabilizing efficiency10.1038/s41598-021-84917-z ↗
29. Phase chemistry and precipitation reactions in maraging steels: part I. Introduction and study of Co-containing C-300 steel10.1007/BF02668190 ↗
30. Concurrent improvement of strength and ductility in heat-treated C300 maraging steels produced by laser powder bed fusion technique
31. The role of titanium on the microstructure and mechanical properties of additively manufactured C300 maraging steels10.1016/j.matdes.2020.108965 ↗
32. Precipitation and reverted austenite formation in maraging 350 steel: competition or cooperation?10.1016/j.actamat.2024.119865 ↗
33. Directed energy deposition of 18NiM300 steel: effect of process and post processing conditions on microstructure and properties10.1080/14686996.2024.2346071 ↗
34. A dilatometric study of the continuous heating transformations in 18wt. % Ni maraging steel of grade 35010.1016/S0921-5093(02)00934-6 ↗
35. Phase transformation in a nanostructured M300 maraging steel obtained by SPS of mechanically alloyed powders10.1007/s10973-010-0745-5 ↗
36. Towards controlling intrinsic heat treatment of maraging steel during laser directed energy deposition10.1016/j.scriptamat.2021.113973 ↗
37. Hillert · 1953
38. Hillert · 1969 · 231
39. Diffusion in multicomponent metallic systems: ii. Solutions for two-phase systems with applications to transformations in steel10.1139/p58-097 ↗
40. Growth of proeutectoid ferrite in ternary iron-carbon-manganese austenites
41. Cyclic quenching treatment doubles the Charpy V-notch impact energy of a 2.3 GPa maraging steel10.1016/j.jmst.2024.05.026 ↗
42. Extension of the martensite transformation temperature relation to larger alloying elements and contents10.1002/adem.201300116 ↗
43. Predicting the Ms temperature of steels with a thermodynamic based model including the effect of the prior austenite grain size10.1016/j.actamat.2016.12.029 ↗
44. Variation of stacking fault energy with austenite grain size and its effect on the MS temperature of g ì o martensitic transformation in Fe–Mn alloy10.1016/S0921-5093(98)00994-0 ↗