journal article·2026-05Open access

Effect of grain boundary types and aging precipitation in mechanical and fatigue properties of Al–Mg–Si alloy induced by extrusion and rolling processing

Xinming Feng, Haochen Xu, Xiangke Wang, Hu Niu, Dongnan Huang, Zhihao Zhang

Abstract

This study investigates the recrystallization mechanisms of the Al-Mg-Si alloy during the plastic deformation process (extrusion or rolling) and subsequent solid solution treatment, elucidating the effect of grain boundary types and aging precipitation characteristics on mechanical and fatigue properties. The results demonstrate that extrusion processing primarily generates abundant LAGBs through DRV and DRX mechanisms within original grains, and the extruded samples (ES) retain a high fraction of subgrain boundaries (68.9%) after solid solution treatment, while the rolled samples (RS) develop fully recrystallized structures bounded by HAGBs (with a fraction of 95.9%). Under peak aged condition (180 °C for 12 h), the ES exhibit finer grain boundary precipitates (GBPs) radius (3.7 nm) and narrower precipitate-free zones (PFZs) (15 nm) along LAGBs, enhancing boundary strength and achieving superior yield strength (419 ± 6 MPa) with moderate elongation (13% ± 1.5%), while the RS show coarser GBPs (7.8 nm) and wider PFZs (29 nm) at HAGBs, resulting in lower yield strength (375 ± 3 MPa) but better plasticity (18.5% ± 0.5 %) due to weaker obstruction to dislocation slip. During the fatigue cycling process, HAGBs in the RS facilitate accelerated intergranular crack propagation, while the high-density LAGBs in the ES reduce strength mismatch between grain interiors and boundaries, promoting transgranular propagation. The mixed distribution of LAGBs and HAGBs effectively blunts crack tips, endowing the ES with enhanced fatigue crack growth resistance.
Source: openalex_inverted_index · Quality: baseline

Research context

OpenAlex topics: Microstructure and mechanical properties · Metallurgy and Material Forming · Metal Forming Simulation Techniques

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (48)

Show source-provided references
1. Machining of aluminum alloys: a review10.1007/s00170-016-8431-9 ↗
2. Effect of pitting corrosion on fatigue life of T6 and T73 of 7075 aluminum alloy10.1016/j.ijfatigue.2025.109073 ↗
3. Intergranular crack during fatigue in al-mg-si aluminum alloy thin extrusions10.1016/j.ijfatigue.2017.03.028 ↗
4. Mechanisms determining bendability in al-mg-si-fe crossover alloys10.1016/j.actamat.2025.120810 ↗
5. Optimisation of heat treatment of Al-Cu-(Mg-Ag) cast alloys10.1007/s10973-019-08702-x ↗
6. Evolution of microstructure, texture and formability of al-mg-si alloys at different hot rolling finish temperatures10.1016/j.jmrt.2024.07.108 ↗
7. Hot deformation behavior and microstructure evolution of hot-extruded 6A02 aluminum alloy10.1016/j.matchar.2022.111908 ↗
8. Investigation of work softening mechanisms and texture in a hot deformed 6061 aluminum alloy at high temperature10.1016/j.msea.2014.03.086 ↗
9. Dynamic recrystallization mechanisms of 2195 aluminum alloy during medium/high temperature compression deformation10.1016/j.msea.2020.140650 ↗
10. Comprehensive study of hot compression behaviors and microstructure evolution of solutionized 6082 aluminum alloy extruded bar10.1016/j.jallcom.2022.167541 ↗
11. The dynamic recrystallization microstructure characteristics and the effects on static recrystallization and mechanical properties of al-mg-si alloy10.1016/j.msea.2024.146454 ↗
12. Tailoring the formability and planar anisotropy of al-mg-si-cu-zn alloys via cross hot rolling and two-stage cold rolling10.1016/j.jallcom.2024.174089 ↗
13. Effect of hot rolling finishing temperature and intermediate annealing on the microstructure, texture evolution, and comprehensive properties of al-mg-si alloy10.1016/j.jallcom.2023.172525 ↗
14. Influence of ageing on the intergranular corrosion of an al-mg-si alloy10.1007/s12540-020-00843-1 ↗
15. Microstructure evolution, plastic anisotropy, and intergranular corrosion of al-mg-si sheet processed through a combination of hot extrusion and cold rolling10.1016/j.matchar.2020.110299 ↗
16. Grain-boundary kinetics: a unified approach10.1016/j.pmatsci.2018.05.004 ↗
17. The effects of quench rate and pre-deformation on precipitation hardening in al-mg-si alloys with different Cu amounts10.1016/j.msea.2014.04.094 ↗
18. Effects of grain boundary chemistry and precipitate structure on intergranular corrosion in al-mg-si alloys doped with Cu and Zn10.1016/j.corsci.2024.112227 ↗
19. Corrosion behaviour of AA6082 al-mg-si alloy extrusion: Recrystallized and non-recrystallized structures10.1016/j.corsci.2018.08.047 ↗
20. Effect of interrupted ageing treatment on the mechanical properties and intergranular corrosion behavior of al-mg-si alloys10.1016/j.jmrt.2019.10.050 ↗
21. Influence of precipitates on low-cycle fatigue and crack growth behavior in an ultrafine-grained aluminum alloy10.1016/j.actamat.2014.07.061 ↗
22. Effect of artificial aging on the fatigue crack propagation resistance of 2000 series aluminum alloys10.1016/S0142-1123(01)00159-1 ↗
23. Enhanced low-cycle fatigue and crack propagation resistance of an al-cu-mg-si forging alloy by non-isothermal aging10.1016/j.msea.2018.07.002 ↗
24. Effect of strain path on structure and mechanical behavior of ultra-fine grain Cu/Cr alloy produced by equal-channel angular pressing10.1016/j.actamat.2005.01.046 ↗
25. Influence of grain structure and slip planarity on fatigue crack growth in low alloying artificially aged 2xxx aluminium alloys10.1016/j.ijfatigue.2006.08.005 ↗
26. Revealing the role of heterogeneous microstructure on fatigue crack propagation behaviors in T74 al-zn-mg-cu alloys10.1016/j.msea.2025.147971 ↗
27. Rollett · 2004
28. Dynamic and post-dynamic recrystallization under hot, cold and severe plastic deformation conditions
29. The deformation behavior and microstructure evolution of a Mn- and Cr-containing al-mg-si-cu alloy during hot compression and subsequent heat treatment10.1007/s11661-016-3881-0 ↗
30. Defeating strength-plasticity trade-off of al-zn-mg-cu alloy by spray forming and double step extrusion10.1016/j.jmrt.2025.09.219 ↗
31. Investigation on microstructural evolution of spray formed al-zn-mg-cu alloy during hot extrusion processes and subsequent solution treatment
32. The structural and compositional evolution of precipitates in al-mg-si-cu alloy10.1016/j.actamat.2017.12.036 ↗
33. Study on properties and precipitation behavior of 6000 series alloys with high Mg/Si ratios and Cu contents10.1016/j.matchar.2022.112402 ↗
34. Enhanced strength-conductivity trade-off in al-mg-si alloys with optimized Mg/Si ratio10.1016/j.jallcom.2023.172682 ↗
35. Effect of Cu content on central-segregation composition and mechanical properties of al-mg-si alloys produced by twin-roll casting10.1016/j.msea.2023.144782 ↗
36. The influence of Cu content and Mg/Si ratio on the strength and formability in al-mg-si-cu alloys10.1016/j.matchar.2023.113355 ↗
37. Fatigue failure analysis and life prediction of forged 6061 aluminum alloy wheel hubs based on precipitate size effects and multiaxial stress modeling10.1016/j.engfailanal.2025.110181 ↗
38. On the interaction of solute atoms with vacancies in diluted Al-alloys: a paradigmatic experimental and ab-initio study on indium and tin10.1016/j.actamat.2021.117228 ↗
39. A yield strength model for the Al-Mg-Si-Cu alloy AA611110.1016/S1359-6454(03)00028-4 ↗
40. The deformation and ageing of mild steel: III discussion of results10.1088/0370-1301/64/9/303 ↗
41. The cleavage strength of polycrystals
42. Precipitation strengthening of the aluminum alloy AA611110.1007/s11661-003-0191-0 ↗
43. Modeling the evolution in microstructure and properties during plastic deformation of f.c.c.-metals and alloys – an approach towards a unified model10.1016/S0921-5093(01)01130-3 ↗
44. Optimization of electrical conductivity and strength combination by structure design at the nanoscale in al-mg-si alloys10.1016/j.actamat.2015.07.039 ↗
45. Prediction of dislocation-grain boundary interactions in FCC aluminum bicrystals using a modified continuum criterion and machine learning methods10.1016/j.mtla.2023.101874 ↗
46. The effect of roll gap geometry on microstructure in cold-rolled aluminum10.1016/j.actamat.2004.08.028 ↗
47. Training high-strength aluminum alloys to withstand fatigue10.1038/s41467-020-19071-7 ↗
48. Exceptional fracture toughness in a high-strength Mg alloy with the synergetic effects of bimodal structure, LPSO, and nanoprecipitates10.1016/j.scriptamat.2023.115675 ↗