journal article·2026-05Open access

Effect of annealing treatment on the microstructure evolution and corrosion behavior of 316L stainless steel manufactured by laser powder bed fusion

Zhihong Liu, Xiaoqing Zhang, Jiaxing Fan, Guanghui Li, Lanlan Yang, Yanxin Qiao, Yanbing Tang, Shujin Chen

Abstract

The microstructure and corrosion behavior of 316L stainless steel (316L SS) fabricated by laser powder bed fusion (LPBF) and subsequently annealed at 800 o C, 1000 o C, and 1200 o C for 4 h were investigated. Surface characterization and electrochemical measurements were employed. The results showed that the annealing treatment did not alter the phase composition of LPBF 316L SS. However, the grain size increased progressively with annealing temperature increasing. The low angle grain boundaries (LAGBs) gradually decreased and the cellular substructures inside the grains disappeared after annealing treatment. The LPBF 316L SS would recrystallize and numerous recrystallized twin grains appear at 1200 °C annealing treatment. The electrochemical tests revealed that annealing treatment detrimentally affected the corrosion resistance of the LPBF 316L SS. The passive film formed on the annealed samples became less stable with higher charge carrier density. Meanwhile, the thickness and the O 2- /OH - ratios of the passive film decreased after annealing treatment. These indicated that the annealing treatment reduced the protection of the passive film.
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Research context

OpenAlex topics: Additive Manufacturing Materials and Processes · High Entropy Alloys Studies · Laser Material Processing Techniques

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References (38)

Show source-provided references
1. A review of post-processing technologies in additive manufacturing
2. A contemporary investigation of metal additive manufacturing techniques10.1007/s12046-021-01770-6 ↗
3. Annealing treatment on corrosion resistance deterioration of LPBF 316L SS in 0.1 mol/L HCl solution10.1007/s42243-025-01491-8 ↗
4. Influence of low temperature heat treatment on microstructure, corrosion resistance and biological performance of 316L stainless steel manufactured by selective laser melting10.1016/j.cirpj.2022.11.006 ↗
5. Enhanced corrosion resistance of additively manufactured 316L stainless steel after heat treatment10.1149/1945-7111/abc10e ↗
6. Effect of annealing on the mechanical and corrosion properties of 316L stainless steel manufactured by laser powder bed fusion10.1016/j.msea.2022.144263 ↗
7. Electrochemical studies on the effect of residual stress on the corrosion of 316L manufactured by selective laser melting10.1016/j.corsci.2019.108314 ↗
8. Determining the necessity of post‐processing heat treatment for the 316L stainless steel manufactured by laser powder bed fusion through evaluation of mechanical and corrosion properties
9. Corrosion resistance of laser powder bed fused AISI 316L stainless steel and effect of direct annealing10.3390/ma15186336 ↗
10. Effect of heat treatment on the corrosion resistance of 316L stainless steel manufactured by laser powder bed fusion10.1016/j.jmrt.2024.08.194 ↗
11. New insights on cellular structures strengthening mechanisms and thermal stability of an austenitic stainless steel fabricated by laser powder-bed-fusion10.1016/j.actamat.2020.11.018 ↗
12. Unanticipated drastic decline in pitting corrosion resistance of additively manufactured 316L stainless steel after high-temperature post-processing10.1016/j.corsci.2019.108412 ↗
13. On the stress corrosion crack growth behaviour in high temperature water of 316L stainless steel made by laser powder bed fusion additive manufacturing10.1016/j.corsci.2017.09.017 ↗
14. Effects of heat treatment and applied stresses on the corrosion performance of additively manufactured super duplex stainless steel clads10.1016/j.mtla.2020.100878 ↗
15. Elucidating the grain-orientation dependent corrosion rates of austenitic stainless steels10.1016/j.matdes.2020.108583 ↗
16. Effects of crystallographic orientation on the corrosion behavior of stainless steel 316L manufactured by laser powder bed fusion
17. Tailoring the theory of critical distances to better assess the combined effect of complex geometries and process-inherent defects during the fatigue assessment of SLM Ti-6Al-4V
18. Decomposition of cellular structure in selective laser melted cu–zn–si silicon brass and its influence on microstructure, mechanical and corrosion properties10.1016/j.msea.2022.143055 ↗
19. Improvement in corrosion resistance of wire arc additive manufactured inconel 625 alloy through heat treatment10.1088/2053-1591/ac0b0b ↗
20. Effect of grain size on mechanical property and corrosion resistance of the Ni-based alloy 69010.1016/j.jmst.2017.12.017 ↗
21. Grain size distribution effects on the corrosion behaviour of materials10.1016/j.corsci.2012.04.040 ↗
22. Passivation behavior of different building planes of selective laser melting 316L stainless steel in 3.5% NaCl solution10.1002/srin.202200759 ↗
23. Unveiling the significant contribution of matrix elements to passivation behaviour and corrosion resistance of alloys by modelling approach
24. Perchlorate and oxygen reduction during Zn corrosion in a neutral medium10.1016/j.electacta.2006.03.065 ↗
25. Corrosion behavior of wire arc additive manufactured Inconel 718 superalloy10.1016/j.jallcom.2020.154455 ↗
26. Corrosion behavior of different building planes of selective laser melting 316L stainless steel in 0.1 M HCl solution10.1016/j.jmrt.2024.01.078 ↗
27. Effect of hydrogen charging on microstructural evolution and corrosion behavior of Ti-4Al-2V-1Mo-1Fe alloy10.1016/j.jmst.2020.06.010 ↗
28. The passivity of selective laser melted 316L stainless steel10.1016/j.apsusc.2019.144495 ↗
29. Corrosion behavior of a selective laser melted inconel 718 alloy in a 3.5 wt.% NaCl solution10.1007/s11665-021-05909-8 ↗
30. Effect of Mo and Mn additions on the corrosion behaviour of AISI 304 and 316 stainless steels in H2SO410.1016/j.corsci.2007.11.004 ↗
31. Electrochemical corrosion and passive behavior of a new high-nitrogen austenitic stainless steel in chloride environment10.1016/j.matchemphys.2022.126837 ↗
32. A comparative study of primary and secondary passive films formed on AM355 stainless steel in 0.1 M NaOH10.1016/j.apsusc.2017.08.151 ↗
33. Effect of microstructure on the passive behavior of selective laser melting-fabricated Hastelloy X in NaNO3 solution10.1016/j.matchar.2020.110370 ↗
34. Electrochemical noise (EN) technique: review of recent practical applications to corrosion electrochemistry research10.1080/01694243.2019.1587224 ↗
35. In-situ monitoring of pitting corrosion of Q235 carbon steel by electrochemical noise: wavelet and recurrence quantification analysis10.1016/j.jelechem.2020.114776 ↗
36. Study on cavitation erosion-corrosion behavior of CoCrFeNiMoCu0.1 high entropy alloy in 3.5 wt% NaCl solution10.1016/j.ultsonch.2024.107021 ↗
37. Electrochemical noise characterization of corrosion behavior for NiCrAl-NiC coating
38. Detection of corrosion degradation using electrochemical noise (EN): review of signal processing methods for identifying corrosion forms