Effect of forging temperature and subsequent heat treatment on the microstructure, strength anisotropy, and mechanical properties of the Ti-1300 alloy
Source abstract
Abstract
Metastable β titanium alloys are attractive for demanding structural applications, but achieving a balanced combination of ultra-high strength, toughness, and low anisotropy remains challenging. In this work, the influence of forging temperature and subsequent heat treatment on the microstructure and mechanical response of a Ti-1300 alloy was investigated. Billets were forged at 750 °C (α+β region) and 870 °C (β region), followed by either duplex α+β solution treatment plus aging or β-region solution treatment plus aging. α+β forging produced a bimodal microstructure with fine equiaxed primary α and a recrystallized β phase, resulting in a weak texture and nearly isotropic tensile properties. β forging generated coarse, fibrous β grains suggesting a discontinuous dynamic recrystallization (DDRX)-like restoration behavior, which enhanced impact toughness but introduced pronounced strength anisotropy. Duplex α+β heat treatment increased the tensile strength under both forging conditions, whereas β-region heat treatment produced lamellar α+β microstructures with reduced toughness and increased anisotropy, which may be associated with α-variant selection and the preferential alignment of lamellar α features within coarse prior-β grains. Overall, 750 °C α+β forging followed by duplex α+β heat treatment provided a favorable balance of strength, ductility, toughness, and reduced strength anisotropy in the Ti-1300 alloy.
Source: openalex_inverted_index · Quality: baseline
Research context
OpenAlex topics: Titanium Alloys Microstructure and Properties · Shape Memory Alloy Transformations · Intermetallics and Advanced Alloy Properties
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (68)
Show source-provided references
1. An overview on research and development of low-cost titanium alloys
2. Transformation of phase and microstructure in Ti-1300 alloy during isothermal aging
3. Microstructure and properties of Ti-based alloys for aerospace applications
4. Phase transformation behavior of Ti-1023 under static heat treatment and dynamic thermo-mechanical coupling10.1016/j.matchar.2022.112248 ↗
5. Nb modified Ti-5553 alloy: effects of heating rate on mechanical properties, corrosion behavior, and crystallographic texture10.1016/j.jmrt.2023.02.138 ↗
6. Advances in low-cost β-type titanium alloys: design and applications
7. Additive manufacturing of low-cost titanium alloys: process–structure–property relationships
8. Effect of aging temperatures on the microstructure and mechanical properties of TC21 forgings with basket–weave microstructure10.1016/j.matchar.2024.114270 ↗
9. Development of Ti alloys for structural applications in China
10. Influence of microstructure on cyclic deformation response and micromechanics of Ti–55531 alloy10.1016/j.msea.2020.140505 ↗
11. Influence of notch root radius on high cycle fatigue properties and fatigue crack initiation behavior of Ti-55531 alloy with a multilevel lamellar microstructure10.1016/j.jmrt.2023.04.211 ↗
12. Influence of multilevel lamellar microstructure on notch high cycle fatigue properties and crack initiation behavior of Ti-55531 alloy10.1016/j.jallcom.2024.177684 ↗
13. High-strength titanium alloys for aerospace engineering applications: a review on melting-forging process10.1016/j.msea.2022.143260 ↗
14. Improvements in surface integrity, corrosion and wear resistances of TA2 titanium alloy via cool-assisted ball burnishing
15. Microstructure evolution and enhanced wear and corrosion resistance of additively manufactured TA1 pure titanium by hybrid electric-ultrasonic burnishing10.1016/j.engfailanal.2026.110667 ↗
16. Gradient microstructure-mediated superior torsional properties in a metastable β Ti-55531 alloy10.1016/j.jallcom.2025.183953 ↗
17. Hot deformation behavior of β titanium alloy
18. Effect of heat treatment on microstructure of Ti alloys
19. Industrial progress in low-cost titanium alloys
20. Precipitation behavior and tensile properties of new high strength beta titanium alloy Ti-130010.1016/j.jallcom.2015.02.222 ↗
21. Effect of microstructure characteristic on mechanical properties and corrosion behavior of new high strength Ti-1300 beta titanium alloy10.1016/j.jallcom.2017.08.239 ↗
22. Microstructural design of β titanium alloys
23. Mechanical behavior of metastable β titanium alloys
24. Effect of processing parameters on microstructure of Ti alloys
25. Microstructural evolution of β titanium alloys during deformation
26. Hot deformation and processing map of metastable β titanium alloy
27. Hot deformation characteristics of Ti-based alloys
28. Study on thermomechanical processing of titanium alloys10.4028/www.scientific.net/MSF.1016.1181 ↗
29. Low-cost design strategies for titanium alloys
30. Hot deformation behavior and processing maps of Ti-1300 alloy10.1016/j.msea.2014.03.016 ↗
31. Effect of heat treatment on the microstructure and mechanical properties of investment casting Ti-1300 alloy10.1007/s11661-024-07544-z ↗
32. Effect of micro-alloying elements on the microstructure and properties of Ti-1300 alloy fabricated by directed energy deposition
33. Anisotropy in tensile properties of a high strength metastable β titanium alloy10.1016/j.matdes.2024.113401 ↗
34. The microstructure and texture evolution of large-sized metastable β titanium alloy bar during forging processes10.1007/s11665-024-09674-2 ↗
35. Effect of microstructure on high-speed tensile mechanical properties of Ti-1300 alloy10.3390/ma16134725 ↗
36. Achieving high strength and ductility of a metastable β-titanium alloy via coupling thermomechanical processing and heat treatments10.1016/j.msea.2023.145970 ↗
37. Enhanced strength–ductility synergy in Ti55531 titanium alloys through gradient microstructural design strategy10.1016/j.msea.2024.146823 ↗
38. On the effect of deformation conditions on the metal flow behavior during upsetting process using finite element simulation DEFORM 3D software10.1007/s12008-024-02051-2 ↗
39. Friction compensation in the upsetting of cylindrical test specimens10.1007/s11340-016-0164-z ↗
40. Grain size model for continuous dynamic recrystallization of titanium alloy in hot deformation10.1007/s11431-018-9336-9 ↗
41. Deformation behavior and microstructure evolution during hot working of a coarse-grained Ti-5Al-5Mo-5V-3Cr-1Zr titanium alloy in β phase field10.1016/j.msea.2017.03.095 ↗
42. Flow behavior and dynamic recrystallization mechanism of a new near-α titanium alloy Ti-0.3Mo-0.8Ni-2Al-1.5Zr10.1016/j.jmrt.2024.04.076 ↗
43. In-situ characterization of slip activity and lattice strain evolution in a metastable β titanium alloy under uniaxial loading
44. Influence of anisotropy on deformation processes operating in Ti-5Al-5Mo-5V-3Cr at room temperature10.1016/j.actamat.2017.09.023 ↗
45. Microstructure and texture evolution of large-sized metastable β-titanium alloy Ti-55511 during multistep forging
46. Quantification of plastic strain from crystal lattice curvature10.1016/j.actamat.2005.08.046 ↗
47. A review of dynamic recrystallization phenomena in metallic materials10.1016/j.matdes.2016.09.012 ↗
48. Modelling discontinuous dynamic recrystallization using a physically based model for nucleation10.1016/j.actamat.2009.07.024 ↗
49. A model of continuous dynamic recrystallization10.1016/S1359-6454(03)00078-8 ↗
50. Synergic strength–ductility enhancement in bimodal titanium alloy via a heterogeneous structure induced by the ⟨c+a⟩ slip10.1016/j.jmst.2024.04.012 ↗
51. Synergistic strengthening and toughening in β titanium alloy via enhanced micron-sized primary α with fiber-like β grains10.1016/j.matdes.2025.113816 ↗
52. High temperature deformation behavior and microstructural characterization of Ti-35421 titanium alloy10.3390/ma13163623 ↗
53. High-temperature deformation behavior and recrystallization mechanism of Ti-55511 alloy in β phase region
54. Tensile performance and impact toughness of Ti-55531 alloy with multilevel lamellar microstructure10.1007/s10853-021-05844-y ↗
55. Combination of multiple strengthening mechanisms facilitates excellent strength–ductility balance in metastable β titanium alloy10.1016/j.jmrt.2024.05.217 ↗
56. The anisotropy of fracture toughness of an α+β titanium alloy by β forging10.1016/j.jmrt.2023.10.230 ↗
57. Ductile to brittle transition of an A508 steel characterized by charpy impact test. Part I: experimental results10.1016/j.engfracmech.2004.03.010 ↗
58. Ductile to brittle transition of an A508 steel characterized by charpy impact test. Part II: modelling of the charpy transition curve
59. Quantitative relationships between mechanical properties and microstructure of Ti17 alloy after thermomechanical treatment10.3390/met10010067 ↗
60. Slip and fatigue crack formation processes in an α/β titanium alloy in the very high cycle fatigue regime
61. Plastic strain localization in metals: origins and consequences10.1016/j.pmatsci.2013.06.001 ↗
62. Effect of hot working parameters on microstructure and texture evolution of a hot-deformed Zr–45Ti–5Al–3V alloy10.3390/ma15041382 ↗
63. Synergistically improving the strength-impact toughness in dual-phase titanium alloy via martensite-engineered α+ α′+ β microstructure
64. Variant selection by dislocations during α precipitation in α/β titanium alloys10.1016/j.actamat.2014.12.044 ↗
65. Bunge · 2013
66. On the entropy to texture index relationship in quantitative texture analysis10.1107/S0021889806055476 ↗
67. Tensile anisotropy associated microstructural and microtextural evolution in a metastable beta titanium alloy10.1016/j.msea.2019.01.053 ↗
68. An orientation relationship between parent grains and its application to variant selection of transformed α in titanium alloys10.1007/s11661-025-07684-w ↗