journal article·2026-05Open access

Cross-sectional microstructural and textural inhomogeneities in a Mg–Zn–Al–Ca (ZAX210) wire produced by the conform process

Franziska Ueberschär, Madlen Ullmann, Max Stirl, Marvin Gretschel, Christoph Kaden, Ulrich Prahl

Abstract

The Conform process (Continuous Rotary Extrusion, CRE) enables the production of magnesium alloy wires like Mg-Zn-Al-Ca (ZAX210) with refined microstructures and tailored textures, but also introduces cross-sectional inhomogeneities that affect the final material response. In this work, a combined experimental and finite element (FE) simulation approach was used to analyse these inhomogeneities in terms of microstructure, texture, and deformation conditions. Optical and electron backscatter diffraction (EBSD) analyses revealed an overall fine grain structure (∼5.7 μm), with slightly smaller grains in the surface layers due to enhanced dynamic recrystallization. Texture development is governed by extrusion- and shear-induced deformation, resulting in a rotated B-fibre (basal plane parallel to shear plane) as the global texture component. Local variations include a B-fibre with weak C 1 -fibre component (c-axis is fibre axis first rotated 90° in shear direction, then 30° in shear plane direction) in the upper region, a strong B-fibre in the middle region, and C 1 /C 2 -fibres in the lower region caused by shear reversal. A fiber texture describes preferred crystallographic orientation, where most grains align a specific crystal direction with a common axis. Twinning activity reflects the heterogeneous deformation state, with ( tension twins dominating overall but being suppressed in high-shear regions. FE simulations confirmed the asymmetric shear stress distribution and complex flow near the abutment, providing a mechanistic link between local strain, recrystallization, and texture evolution. The middle region, representing ∼62 % of the cross-sectional area, was found to dominate the global microstructure and texture.
Source: openalex_inverted_index · Quality: baseline

Research context

OpenAlex topics: Magnesium Alloys: Properties and Applications · Aluminum Alloys Composites Properties · Microstructure and mechanical properties

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (52)

Show source-provided references
1. Applications of magnesium alloys for aerospace: a review10.1016/j.jma.2023.09.015 ↗
2. Recent advances in the development of aerospace materials10.1016/j.paerosci.2018.01.001 ↗
3. Advancements in lightweight materials for aerospace structures: a comprehensive review10.61359/11.2106-2409 ↗
4. Recent advances in light metals and manufacturing for automotive applications10.1080/19236026.2021.1947088 ↗
5. Development and application of magnesium alloy parts for automotive OEMs: a review10.1016/j.jma.2022.12.015 ↗
6. Bioabsorbable WE43 Mg alloy wires modified by continuous plasma-electrolytic oxidation for implant applications. Part I: processing, microstructure and mechanical properties
7. Direct extrusion of thin Mg wires for biomedical applications10.1016/S1003-6326(20)65219-0 ↗
8. A review of additive manufacturing of magnesium alloys10.1063/1.5044305 ↗
9. Wire arc additive manufacturing of AZ31 Magnesium alloy: grain refinement by adjusting pulse frequency10.3390/ma9100823 ↗
10. Microstructure and texture evolution in AZ31 magnesium alloy during caliber rolling at different temperatures
11. Influence of single-pass caliber rolling on the microstructural evolution and mechanical properties of Mg 10Gd binary alloy10.1016/j.jma.2024.04.030 ↗
12. Effects of caliber rolling on microstructure and room temperature tensile properties of Mg–3Al–1Zn alloy10.1016/j.jma.2013.07.005 ↗
13. Heat treated AZ61 magnesium alloy obtained by direct extrusion and continuous rotary extrusion process10.1515/amm-2016-0074 ↗
14. The effect of extrusion parameters on possibility of extrusion of magnesium alloys in continuous rotary extrusion process/Wpływ parametrów procesu wyciskania Na możliwość wyciskania stopów magnezu metodą ciągłego wyciskania Na Kole10.1515/amm-2015-0476 ↗
15. Effect of tool geometry on the velocity and strain rate fields in continuous rotary extrusion of magnesium AZ91 alloy10.1016/j.promfg.2018.07.218 ↗
16. Continuous rotary extrusion of AZ81 magnesium alloy10.1016/j.promfg.2018.07.217 ↗
17. Grain refinement of magnesium alloys by CONFORM: a continuous severe plastic deformation route?10.4028/www.scientific.net/MSF.706-709.1781 ↗
18. Microstructures and tensile properties of AZ31 magnesium alloy by continuous extrusion forming process
19. Microstructure, texture, and mechanical properties of continuously extruded and rolled AZ31 Magnesium alloy sheets10.1007/s11665-019-04394-4 ↗
20. Study of the microstructure, bonding evolution and mechanical properties of continuously extruded magnesium AZ31 sheet
21. Characterisation of conform™ and conventionally extruded Al–4Mg–1Zr. Effect of extrusion route on superplasticity10.1007/s10853-010-4513-5 ↗
22. Deformation mechanisms and microstructural characteristics of AZ61 magnesium alloys processed by a continuous expansion extrusion approach10.1016/j.jma.2022.11.019 ↗
23. Microstructure of AZ31 magnesium alloy produced by the CONFORM process under different extrusion wheel velocities10.4028/www.scientific.net/AMR.189-193.2609 ↗
24. The microstructural features and strengthening mechanisms of Mg-Al-Zn-Ca-(RE) extruded alloys having high-volume fractions of second-phase particles
25. Experimental investigation of the phase equilibria of the al–ca–zn system at 623K10.1016/j.jallcom.2012.06.029 ↗
26. Texture analysis with MTEX – free and open source software toolbox10.4028/www.scientific.net/SSP.160.63 ↗
27. Microstructure and hot deformation behavior of twin roll cast Mg-2Zn-1Al-0.3Ca alloy10.3390/ma12071020 ↗
28. Contact friction in Metal forming
29. Code validation and development of user routines for microstructural prediction with qform10.1016/j.matpr.2015.10.052 ↗
30. Numerical investigation of the material behaviour during compression tests for samples with rough surfaces represented in different geometry scale factors10.4028/www.scientific.net/KEM.716.736 ↗
31. Ideal orientations and persistence characteristics of hexagonal close packed crystals in simple shear10.1016/j.actamat.2006.12.021 ↗
32. Characterization, modelling and simulation of deformation and fracture behaviour of the light-weight wrought alloys under high strain rate loading10.1016/j.ijimpeng.2005.03.008 ↗
33. Effect of stress triaxiality on the flow and fracture of Mg alloy AZ3110.1007/s11661-014-2211-7 ↗
34. The effect of material properties and tooling design on deformation and fracture during equal channel angular extrusion10.1016/S1359-6454(00)00019-7 ↗
35. Study of surface cracking during extrusion of aluminium alloy AA 201410.1179/026708304225022016 ↗
36. Avoiding cracks and inhomogeneities in billets processed by ECAP10.1007/s10853-010-4384-9 ↗
37. The processing of difficult-to-work alloys by ECAP with an emphasis on magnesium alloys10.1016/j.actamat.2007.04.043 ↗
38. Serrated grain boundary modulation inhibits nano cracks propagation in pure magnesium: a phase field crystal and quasi in-situ EBSD study10.1016/j.actamat.2025.121573 ↗
39. Microstructure and mechanical properties of SPD-Processed an as-cast AZ91D+Y magnesium alloy by equal channel angular extrusion and multi-axial forging10.1016/j.matdes.2009.04.023 ↗
40. Dynamic and post-dynamic recrystallization under hot, cold and severe plastic deformation conditions10.1016/j.pmatsci.2013.09.002 ↗
41. A review of dynamic recrystallization phenomena in metallic materials10.1016/j.matdes.2016.09.012 ↗
42. Effects of Ca addition on the microstructure and mechanical properties of mg–zn–sn–mn alloys10.1016/j.jmrt.2023.06.194 ↗
43. Comparison of the effect of ECAP and SSE on microstructure, texture, and mechanical properties of magnesium10.1016/j.jallcom.2022.164407 ↗
44. Microstructure evolution of pure copper during a single pass of simple shear extrusion (SSE): role of shear reversal
45. Microstructure and texture characterization of Mg–Al and Mg–Gd binary alloys processed by simple shear extrusion10.1016/j.jmrt.2018.06.023 ↗
46. Analysis of microstructure and texture evolution in pure magnesium during symmetric and asymmetric rolling10.1016/j.actamat.2009.07.008 ↗
47. Agnew · 2002 · 169
48. Strain rate-induced crystallographic texture development in tensile deformation of a rapidly solidified thin-strip cast AA5182 Al-Mg alloy
49. Microstructure, deformation, and property of wrought magnesium alloys10.1007/s11661-020-05974-z ↗
50. Investigation of twin-dislocation interactions using a novel discrete dislocation plasticity framework10.1016/j.ijplas.2025.104465 ↗
51. The experimental simulation of deformation behavior of metals in the conform process
52. The mechanics of the continuous rotary extrusion process investigated by FEM analysis