Study of the World’s finest 15 μm stainless-steel wire: Microstructure, electro-thermal annealing mechanisms, and wire-bond joint electrical performance
Source abstract
Abstract
This study reports, for the first time, the successful fabrication and implementation of the world’s finest 15 μm 304L stainless-steel bonding wire for advanced electronic packaging applications. Unlike conventional Au, Cu, or Ag bonding wires, the proposed Fe-based wire offers a low-cost alternative while avoiding intermetallic compound (IMC) formation at bonding interfaces. The ultrafine wire, produced through severe cold drawing (∼98% reduction), exhibits an ultrahigh tensile strength approaching 3000 MPa due to strain-induced martensitic transformation. A controlled electro-thermal annealing process (0.08 A, 5 min) effectively induces recrystallization, grain growth, and martensite-to-austenite reversion, reducing excessive work hardening while stabilizing elongation at 8–10% and maintaining tensile strength near 1000 MPa. Electrically assisted tensile tests further reveal current-dependent softening mechanisms governed by Joule heating, dynamic strain effects, and surface oxide formation. Notably, even at 80% of the fusing current, the wire retains substantial tensile strength (∼800 MPa) together with enhanced ductility. Wire-bonding evaluations demonstrate reliable first and second bonds on both Cu and Al substrates, with stable resistance and fusing current behavior independent of current direction. The absence of IMC formation, combined with high mechanical robustness and electro-thermal stability, establishes a new Fe-based wire-bonding strategy and highlights the strong potential of stainless-steel ultrafine wires as next-generation interconnection materials.
Source: openalex_inverted_index · Quality: baseline
Research context
OpenAlex topics: Electronic Packaging and Soldering Technologies · Advanced Welding Techniques Analysis · Shape Memory Alloy Transformations
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (36)
Show source-provided references
1. Tu · 2021
2. An overview of electrical and mechanical aspects of electronic packaging
3. Research progress on bonding wire for microelectronic packaging10.3390/mi14020432 ↗
4. The electrothermal fracture mechanism between aluminum and copper wires10.1016/j.microrel.2022.114819 ↗
5. The reliability of wire bonding using Ag and Al10.1016/j.microrel.2016.05.009 ↗
6. Evaluation of Ag wire reliability on fine pitch wire bonding
7. Low cost Pd coated Ag bonding wire for high quality FAB in air
8. Microstructure evolution and failure mechanism of electromigration in Ag-alloy bonding wire10.1016/j.jallcom.2022.165266 ↗
9. Mechanism of microweld formation and breakage during Cu–Cu wire bonding investigated by molecular dynamics simulation10.1088/1674-1056/ac0e24 ↗
10. The mechanism of Pd distribution in the process of FAB formation during Pd-coated Cu wire bonding10.1007/s10854-018-9508-z ↗
11. Mechanism to improve the reliability of copper wire bonding with palladium-coating of the wire10.1016/j.microrel.2019.04.010 ↗
12. Comparison of Au/Al, Cu/Al, and Ag/Al in wirebonding assembly and IMC growth behavior
13. Iron-Based high-temperature alloys: alloying strategies and new opportunities10.3390/ma18132989 ↗
14. Development of single-stage TiNbMoMnFe high-entropy alloy coating on 304L stainless steel using HVOF thermal spray10.1007/s11666-021-01294-9 ↗
15. Application characteristics of ultra-fine 15 μm stainless steel wires: microstructures, electrical fatigue, and ball Formation mechanisms10.3390/mi16030326 ↗
16. Study on material properties and copper-to-copper wire bonding of Cu-Pt-Au-Pd fine micro-alloyed wires10.1007/s11664-024-11456-4 ↗
17. Effect of drawing and annealing on the microstructure and mechanical properties of 304 austenitic stainless steel wire10.1088/2053-1591/ac44d6 ↗
18. Temperature-Dependent martensitic transformation in cold-rolled AISI 304 stainless steel10.3390/cryst15070652 ↗
19. Effects of oxidation and surface roughening on drawing limit in dieless drawing process of SUS304 stainless steel microtubes10.1016/j.jmatprotec.2015.03.033 ↗
20. Formability analysis and oxidation layer effects in dieless drawing of stainless steel wires10.3390/met9080828 ↗
21. Influence of surface and grain-boundary scattering on the resistivity of copper in reduced dimensions10.1063/1.1703844 ↗
22. Contribution of grain boundary to strength and electrical conductivity of annealed copper wires10.1016/j.jmrt.2023.08.012 ↗
23. Strain induced martensite formation and its effect on strain hardening behavior in the cold drawn 304 austenitic stainless steels10.1016/S1359-6462(96)00338-7 ↗
24. A study of the reverse martensitic transformations in austenitic stainless steels by calorimetry and isothermal heat treatments
25. Feng · 2015
26. Formation of Cr23C6 during the sensitization of AISI 304 stainless steel and its effect to pitting corrosion10.1016/S1452-3981(23)16211-0 ↗
27. The role of grain boundary ferrite evolution and thermal aging on creep cavitation of type 316H austenitic stainless steel10.1016/j.msea.2021.140859 ↗
28. Rate of propagation of martensite
29. Comparison of copper, silver and gold wire bonding on interconnect metallization
30. Stress-state dependence of dynamic strain aging: thermal hardening and blue brittleness10.1007/s12613-021-2250-1 ↗
31. Morphological characteristics of dimples of ductile fracture of VT23M titanium alloy and identification of dimples on fractograms of different scale10.3390/ma12132051 ↗
32. Case study of the tensile fracture investigation of additive manufactured austenitic stainless steels treated at cryogenic conditions10.3390/ma13153328 ↗
33. Aluminium wires have the free air balls (FABs): electronic flame-off, fracture strength, electrical properties, and bonding characteristics of nano Zn Film Al–Si bonding wires10.3390/met7050152 ↗
34. Characteristic of copper wire and transient analysis on wirebonding process10.1016/j.microrel.2010.11.008 ↗
35. Effects of bonding parameters on free air ball properties and bonded strength of Ag-10Au-3.6 Pd alloy bonding wire10.3390/mi11080777 ↗
36. Development of a fast method for optimization of Au ball bond process10.1016/j.microrel.2014.12.013 ↗