Overcoming the strength-ductility trade-off in 300 M steel via spatially-controlled heterostructure design
Source abstract
Abstract
A paradigm for spatially-controlled heterostructure design is proposed to overcome the strength-ductility trade-off in ultra-high-strength 300M steel fabricated via laser powder bed fusion (LPBF). This mechanism-guided approach deliberately modulates the spatial distribution of laser energy using a hybrid linear scanning (LS) and oscillating scanning (OS) strategy to construct lamellar heterostructured (HS) 300M steel with tailored microstructures. The innovation significantly enhances the mechanical property mismatch between the hard (LS-derived) and soft (OS-derived) regions, which is critical for amplifying back-stress strengthening, manifested as hetero-deformation-induced (HDI) stress. The HS materials fabricated via this optimized spatial control achieved a superior mechanical synergy: an ultimate tensile strength of 1761±4.4 MPa and an exceptional elongation of 17.5±0.3%. This performance represents improvements of 104 MPa in strength and 4.7% points in ductility compared to the non-HS samples. Furthermore, the study systematically investigates the influence of hard-phase fraction, lamellar thickness, and soft-hard phase contrast on HDI stress and mechanical performance. These findings establish a robust framework for designing high-performance additive-manufactured materials through coordinated control of lamellar geometry, phase contrast, and hard-phase fraction.
Source: openalex_inverted_index · Quality: baseline
Research context
OpenAlex topics: High Temperature Alloys and Creep · Microstructure and mechanical properties · Microstructure and Mechanical Properties of Steels
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (50)
Show source-provided references
1. Metastable high-entropy dual-phase alloys overcome the strength–ductility trade-off10.1038/nature17981 ↗
2. Control of grain structure, phases, and defects in additive manufacturing of high-performance metallic components10.1016/j.pmatsci.2023.101153 ↗
3. Additive manufacturing of voxelized heterostructured materials with hierarchical phases
4. Mechanical properties of nanocrystalline materials10.1016/j.pmatsci.2005.08.003 ↗
5. Enhanced strength and ductility in a high-entropy alloy via ordered oxygen complexes10.1038/s41586-018-0685-y ↗
6. Extra strengthening and work hardening in gradient nanotwinned metals10.1126/science.aau1925 ↗
7. On the damage tolerance of 3-D printed Mg-Ti interpenetrating-phase composites with bioinspired architectures10.1038/s41467-022-30873-9 ↗
8. An all-natural bioinspired structural material for plastic replacement10.1038/s41467-020-19174-1 ↗
9. Bioinspired structural materials10.1038/nmat4089 ↗
10. Strain partitioning in dual-phase steels containing tempered martensite10.1016/j.msea.2014.05.078 ↗
11. Heterostructured materials10.1016/j.pmatsci.2022.101019 ↗
12. High tensile ductility in a nanostructured metal10.1038/nature01133 ↗
13. Heterostructure enables anomalous improvement of cryogenic mechanical properties in titanium10.1016/j.actamat.2024.119982 ↗
14. Exceptional strength and ductility in heterogeneous multi-gradient TiAl alloys through additive manufacturing10.1016/j.actamat.2024.120395 ↗
15. Obtaining ultra-fine and uniform two-phase structures: evolution of morphology and phase redistribution in a dual-phase Mg–Li alloy during submerged friction stir processing10.1016/j.msea.2024.146238 ↗
16. Mechanical properties of lamellar-structured 18Ni300 maraging steel manufactured via directed energy deposition10.1016/j.msea.2023.146031 ↗
17. Achieving superior combined cryogenic strength and ductility in a high-entropy alloy via the synergy of low stacking fault energy and multiscale heterostructure10.1016/j.scriptamat.2023.115809 ↗
18. Pursuing ultrastrong and ductile medium entropy alloys via architecting nanoprecipitates-enhanced hierarchical heterostructure10.1016/j.actamat.2023.119492 ↗
19. Control of grain structure, phases, and defects in additive manufacturing of high-performance metallic components10.1016/j.pmatsci.2023.101153 ↗
20. Effects of processing parameters on microstructure and mechanical property of selective laser melted Ti6Al4V10.1016/j.matdes.2011.09.051 ↗
21. Additive manufacturing of metals: microstructure evolution and multistage control10.1016/j.jmst.2021.06.011 ↗
22. Additive manufacturing of alloys with programmable microstructure and properties10.1038/s41467-023-42326-y ↗
23. Novel strengthening mechanism of laser powder bed fusion-manufactured Inconel 718: effects of customized hierarchical interfaces
24. Architectured heterogeneous alloys with selective laser melting10.1016/j.scriptamat.2021.114332 ↗
25. The modelling of dynamic recrystallization in the isothermal compression of 300M steel10.1016/j.msea.2013.03.011 ↗
26. Flow stress behaviors and microstructure evolution of 300M high strength steel under isothermal compression10.1016/S1006-706X(14)60192-8 ↗
27. In-situ investigation of phase transformation behaviors of 300M steel in continuous cooling process10.1016/j.matchar.2018.07.034 ↗
28. Quenching microstructure and properties of 300M ultra-high strength steel electron beam welded joints10.1016/j.matdes.2012.04.010 ↗
29. Microstructure and mechanical properties of laser solid formed 300M steel10.1016/j.jallcom.2014.09.111 ↗
30. Selective laser melting of an equiatomic CoCrFeMnNi high-entropy alloy: Processability, non-equilibrium microstructure and mechanical property10.1016/j.jallcom.2018.02.298 ↗
31. Microstructure and mechanical properties of high strength AlCoCrFeNi2.1 eutectic high entropy alloy prepared by selective laser melting (SLM)10.1016/j.matlet.2021.131511 ↗
32. Heterostructured AlCoCrFeNi2.1 high entropy alloy with simultaneously improved strength and ductility via laser powder bed fusion10.1016/j.msea.2025.148496 ↗
33. Enhanced strength and ductility of oscillating laser additive manufactured aluminum alloys with micron-sized Ti3AlC2 MAX-phase10.1016/j.scriptamat.2023.115937 ↗
34. Controlling macroscopic segregation of direct energy deposited Cu–Fe alloy by laser oscillation
35. Defect elimination and microstructure improvement of laser powder bed fusion β-solidifying γ-TiAl alloys via circular beam oscillation technology10.1016/j.msea.2023.145019 ↗
36. Microstructures and tensile properties of laser cladded AerMet100 steel coating on 300M steel10.1016/j.jmst.2017.11.037 ↗
37. Multimodal synchrotron characterization of the formation and spatial distribution of retained austenite in PBF-LB/M-manufactured ferritic–martensitic steel
38. Effect of quenching and tempering treatments on microstructure and mechanical properties of 300M ultra-high strength steel fabricated by laser powder bed fusion10.1016/j.matchar.2024.113935 ↗
39. Effect of tempering on microstructure and mechanical properties of 3Mn-Si-Ni martensitic steel10.1016/j.msea.2017.11.037 ↗
40. Dendrite growth at the limit of stability: tip radius and spacing10.1016/0001-6160(81)90082-1 ↗
41. Microstructural evolution and mechanical properties of 300M steel produced by low and high power selective laser melting10.1016/j.jmst.2019.12.020 ↗
42. Heterogeneous lamella structure unites ultrafine-grain strength with coarse-grain ductility10.1073/pnas.1517193112 ↗
43. The deformation of plastically non-homogeneous materials
44. On the origin of the tensile flow stress in the stainless steel AISI 316L at 300 K: back stress and effective stress10.1016/S1359-6454(99)00222-0 ↗
45. Back stress strengthening and strain hardening in gradient structure10.1080/21663831.2016.1153004 ↗
46. A precipitation-hardened high-entropy alloy with outstanding tensile properties10.1016/j.actamat.2015.08.076 ↗
47. Synergetic strengthening by gradient structure10.1080/21663831.2014.935821 ↗
48. A novel dual-heterogeneous-structure ultralight steel with high strength and large ductility10.1016/j.actamat.2023.118925 ↗
49. Heterolamellar structure design simultaneously enhances strength and plasticity in ultrahigh strength steel
50. Mechanism-based strain gradient crystal plasticity—II. Analysis10.1016/j.jmps.2005.01.004 ↗