Enhanced microstructural control and mechanical performance of selective laser melted 2Cr13 martensitic stainless steel: The role of post-process heat treatment
Source abstract
Abstract
Despite the growing industrial interest in selective laser melting (SLM) of stainless steels, the microstructural evolution mechanisms and microstructure-property relationships in SLM-fabricated 2Cr13 martensitic stainless steel remain insufficiently explored, hindering its optimized application.This study investigates the microstructure and mechanical properties of 2Cr13 martensitic stainless steel fabricated by selective laser melting (SLM), and the regulatory role of post-process heat treatment. Using optimized SLM parameters (180 W power, 620 mm/s scanning speed, 90° interlayer rotation), samples with 99.70 % relative density were prepared. As-built samples featured a martensite-dominated microstructure (with ∼6.3 % residual austenite and δ-ferrite), fine-grained regions in molten pools (prominent in the heat-affected zone), and excellent mechanical properties: 1673 ± 12 MPa ultimate tensile strength (UTS), and ∼9.28 % elongation(EL). Quenching at 950 °C–1050 °C showed 950 °C as optimal, fully transforming residual austenite and δ-ferrite into martensite without obvious grain growth, and achieving a peak hardness of 605.0 ± 7.3 HV 0.5 . Tempering the 950 °C-quenched samples at 500 °C–700 °C induced (Fe, Cr) 23 C 6 carbide nucleation, precipitation, and growth. Tempering at 500 °C yields balanced properties (1232 ± 5 MPa YS, 1429 ± 13 MPa UTS, ∼11.58 % EL). As the tempering temperature rose to 700 °C, UTS decreased to 861 ± 8 MPa, while elongation increased to ∼16.89 %.
Source: openalex_inverted_index · Quality: baseline
Research context
OpenAlex topics: Additive Manufacturing Materials and Processes · High Entropy Alloys Studies · Laser Material Processing Techniques
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (53)
Show source-provided references
1. Metal additive manufacturing: a review10.1007/s11665-014-0958-z ↗
2. Thermal analysis of synchronous induction-assisted laser deposition of Ti-6Al-4V using different laser-induction interaction modes
3. Seynergistic effect of Mo and Zr additions on microstructure and mechanical properties of Nb‐Ti‐Si‐based alloys additively manufactured by laser directed energy deposition10.1016/j.jmst.2021.06.027 ↗
4. Investigation on the composite effect of Zr and Cr on oxidation behavior and fracture toughness of Nb-Ti-Si-based alloys manufactured by directed energy deposition10.1016/j.matchar.2024.114078 ↗
5. Effect of the volume energy density and heat treatment on the defect, microstructure, and hardness of L-PBF inconel 62510.1007/s11661-020-05992-x ↗
6. Additive manufacturing of steels: a review of achievements and challenges10.1007/s10853-020-05109-0 ↗
7. Comparison of powder bed fusion and directed energy deposition for tailoring mechanical properties of traditionally brittle alloys10.1016/j.mfglet.2021.02.003 ↗
8. A current state of metal additive manufacturing methods: a review10.1016/j.matpr.2021.11.503 ↗
9. Defect formation mechanismsin selective laser melting: a review10.1007/s10033-017-0121-5 ↗
10. Influence of SLM process parameters on the surface finish, porosity rate and fatigue behavior of as-built inconel 625 parts10.1016/j.jmatprotec.2017.12.043 ↗
11. Three-dimensional microstructure and mechanical properties of CX stainless steel formed by selective laser melting10.1007/s12540-024-01879-3 ↗
12. Effect of processing parameters on the fractions of martensite in 17-4 PH stainless steel fabricated by selective laser melting10.1016/j.jallcom.2020.157758 ↗
13. Effects of post-printing heat treatment on the microstructure and mechanical properties of a wire arc additive manufactured 420 martensitic stainless steel part10.1016/j.msea.2021.141167 ↗
14. Influence of the heat treatment on the corrosion resistance of the martensitic stainless steel type AISI 42010.1023/A:1025179128333 ↗
15. Stichel · 1994 · vol. 8
16. Microstructural evolution in a thin wall of 2Cr13 martensitic stainless steel during wire arc additive manufacturing10.1016/j.matchar.2021.111520 ↗
17. Tailoring microstructural features of wire arc additive manufacturing 2Cr13 part via varying inter-layer dwelling time10.1016/j.matlet.2018.08.037 ↗
18. Location-related thermal history, microstructure, and mechanical properties of arc additively manufactured 2Cr13 steel using cold metal transfer welding10.1016/j.msea.2017.12.076 ↗
19. Microstructure-property relationships of 420 stainless steel fabricated by laser-powder bed fusion10.1016/j.powtec.2018.11.075 ↗
20. Compressive behavior of 420 stainless steel after asynchronous laser processing10.1016/j.cirp.2020.04.059 ↗
21. Laser powder bed fusion of ultra-high-strength 420 stainless steel: microstructure characterization, texture evolution and mechanical properties10.1016/j.msea.2021.140790 ↗
22. Martensitic stainless steel AISI 420—mechanical properties, creep and fracture toughness10.1007/s11043-011-9137-x ↗
23. Comparative study on life cycle assessment of components produced by additive and conventional manufacturing process10.1016/j.matpr.2022.04.840 ↗
24. Review of selective laser melting: materials and applications10.1063/1.4935926 ↗
25. The effect of heat treatment on mechanical properties and corrosion behavior of AISI420 martensitic stainless steel10.1016/j.jallcom.2010.12.174 ↗
26. Homogenization timing effect on microstructure and precipitation strengthening of 17–4PH stainless steel fabricated by laser powder bed fusion
27. Ultra-high strength martensitic 420 stainless steel with high ductility
28. Additive manufacturing of metals10.1016/j.actamat.2016.07.019 ↗
29. Additive manufacturing of AISI 420 stainless steel: process validation, defect analysis and mechanical characterization in different process and post-process conditions10.1007/s00170-021-07639-6 ↗
30. Microstructure and fracture toughness of a Nb–Ti–Si-based in-situ composite fabricated by laser-based directed energy deposition10.1016/j.compositesb.2024.111427 ↗
31. Selective laser melting of stainless steel 316L with low porosity and high build rates10.1016/j.matdes.2016.05.035 ↗
32. Effects of laser additive manufacturing on microstructure and crystallographic texture of austenitic and martensitic stainless steels
33. Interfacial bonding between a wire arc additive manufactured 420 martensitic stainless steel part and its wrought base plate10.1016/j.matchemphys.2020.123199 ↗
34. Microstructure and mechanical properties of AISI 420 stainless steel produced by wire arc additive manufacturing
35. Formation of Delta ferrite in 9 Wt pct Cr steel investigated by In-Situ X-Ray diffraction using synchrotron radiation10.1007/s11661-010-0371-7 ↗
36. Effect of δ-Ferrite on the properties of martensitic steels10.1007/s11041-013-9652-2 ↗
37. Role of evolving microstructure on the mechanical behaviour of P92 steel welded joint in as-welded and post weld heat treated state10.1016/j.jmatprotec.2018.08.032 ↗
38. In situ heat treatment in selective laser melted martensitic AISI 420 stainless steels10.1016/j.matdes.2015.08.045 ↗
39. Effect of heat treatments on microstructural evolution of additively manufactured and wrought 17-4PH stainless steel10.1016/j.matdes.2018.07.015 ↗
40. Additive manufacturing of metallic components – process, structure and properties10.1016/j.pmatsci.2017.10.001 ↗
41. Effects of building direction and heat treatment on the local mechanical properties of direct metal laser sintered 15-5 PH stainless steel10.1016/j.matchar.2020.110468 ↗
42. Microstructure and property of a selective laser melting process induced oxide dispersion strengthened 17-4 PH stainless steel10.1016/j.jallcom.2019.06.289 ↗
43. Microstructural characterization of 15-5PH stainless steel processed by laser powder-bed fusion10.1016/j.matchar.2021.111485 ↗
44. Study on influential factors for process monitoring and control in laser aided additive manufacturing10.1016/j.jmatprotec.2012.10.006 ↗
45. Reducing porosity in AlSi10Mg parts processed by selective laser melting
46. Laser engineered net shaping advances additive manufacturing and repair
47. Heterogeneously tempered martensitic high strength steel by selective laser melting and its micro-lattice: processing, microstructure, superior performance and mechanisms
48. Characterization of wire arc additive manufacturing 2Cr13 part: process stability, microstructural evolution, and tensile properties10.1016/j.jallcom.2018.03.222 ↗
49. HE Wei4, effect of heat treatment process on the microstructure and properties of 2Cr13 stainless steel
50. Homogenization of microstructure and mechanical properties of wire arc additive manufactured martensitic stainless steel through optimization of post-process heat treatment10.1016/j.jmrt.2022.10.077 ↗
51. Quantification of 8-ferrite and austenite retention in laser-deposited martensitic stainless steel10.1016/j.jmrt.2024.07.037 ↗
52. Simultaneously enhanced strength and ductility for 3D-printed stainless steel 316L by selective laser melting10.1038/s41427-018-0018-5 ↗
53. Additive manufacturing of martensitic stainless steel matrix composites with simultaneously enhanced strength-ductility and corrosion resistance