journal article·2025-11Open access

The influence of the heat treatment on the microstructure evolution and strengthening mechanism of the Al–Mg–Mn–Sc–Zr alloy via selective laser melting

Linzhi Wang, Ting Li, He Wang, Honglin Liu, Chentao Li

Abstract

In this study, Al-Mg-Mn-Sc-Zr alloy was prepared using selective laser melting (SLM). The research focused on the evolution of the microstructure and the changes in mechanical properties under various heat treatment temperatures. Additionally, the mechanisms behind the strength and toughness of both the as-printed and heat-treated samples were analyzed. The microstructure exhibits a bimodal microstructure characterized by alternating fine coarse regions. Sc/Zr elements preferentially segregate to grain boundaries to form Al 3 (Sc, Zr) phases, serving as potent heterogeneous nucleation sites, refining the α-Al matrix and contributing to precipitation strengthening. After aging heat treatment, the mixed crystal structure and the grain size in the equiaxed crystal region remained largely unchanged, while the grains in the columnar region showed signs of coarsening. Aging treatment facilitated the diffusion-mediated redistribution within the matrix, leading to the nanoscale precipitation of Al3(Sc, Zr) phases with an L1 2 structure. These phases contributed to significant precipitation strengthening, enhancing the overall mechanical properties. The ultimate tensile strength of 480 MPa was achieved at 330 °C/5h, representing a 34 % enhancement over the as-printed condition, The dislocation density decreased by solution aging treatment, reducing the grain boundary's hindering effect and significantly lowering toughness, with a reduction to just 9.3 %. Synergistic strengthening mechanisms are identified: (i) grain refinement from Al 3 (Sc,Zr) nucleants, (ii) solid solution hardening, and (iii) L1 2 nanoprecipitation.
Source: openalex_inverted_index · Quality: baseline

Research context

OpenAlex topics: Additive Manufacturing Materials and Processes · Aluminum Alloy Microstructure Properties · High Entropy Alloys Studies

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (42)

Show source-provided references
1. Hot compression behaviors and microstructural evolution of high-Mg crossover Al-Mg-Zn based alloys
2. Effect of annealing temperature on microstructure, mechanical properties and corrosion behavior of Al-Mg-Mn-Sc-Zr alloy10.1016/j.apsusc.2020.146081 ↗
3. Study on the mechanical properties and corrosion behavior of lightweight Al10Mg1Zn0. 1Cu0. 3Si (wt.%) high-magnesium aluminum alloy
4. Magnesium-based nanocomposites: a review from mechanical, creep and fatigue properties10.1016/j.jma.2023.08.005 ↗
5. Strengthening mechanisms of an Al-mg-Sc-Zr alloy10.1016/S1359-6454(02)00258-6 ↗
6. Hot deformation analysis and microstructure evolution of Al–Mg–Mn-Sc-Zr alloy by isothermal compression10.1016/j.jallcom.2020.157655 ↗
7. Mechanical properties of SLM-printed aluminium alloys
8. Mechanical and corrosion performances of Al–Mg-Mn 5083 rolled alloys microalloyed with Sc and Zr in different thermomechanical processing conditions10.1007/s10853-024-10044-5 ↗
9. The S-Al2CuMg precipitates and L12-Al3 (Sc, Zr) dispersoids co-existing in the SLM fabricated Al-Cu-Mg-Sc-Zr alloy10.1016/j.msea.2025.149069 ↗
10. In-situ TEM study on the precipitation behavior of an Al-Mn-Mg-Sc-Zr alloy formed by SLM10.1016/j.matchar.2024.114578 ↗
11. Influence of laser power and scanning speed on microstructure evolutions and mechanical properties of the SLM fabricated Al–Mg–Mn–Sc–Zr alloy10.1016/j.jmrt.2024.10.134 ↗
12. Additive manufacturing of biodegradable magnesium-based materials: design strategies, properties, and biomedical applications10.1016/j.jma.2022.12.001 ↗
13. An SLM-Processed Er-and Zr-modified Al–Mg alloy: microstructure and mechanical properties at room and elevated temperatures10.1016/j.msea.2023.145485 ↗
14. Characterisation of a novel Sc and Zr modified Al–Mg alloy fabricated by selective laser melting10.1016/j.matlet.2017.03.089 ↗
15. The effect of Mn content on a novel Al–Mg–Si-Sc-Zr alloy produced by laser powder bed fusion: the microstructure and mechanical behavior10.1016/j.jmrt.2023.11.048 ↗
16. The evolution and characterizations of Al3 (ScxZr1-x) phase in Al–Mg-based alloys proceeded by SLM10.1016/j.msea.2021.141863 ↗
17. Quasi-in-situ investigation on recrystallization behavior of an Al-Mg-Sc-Zr alloy under different homogenization processes10.1016/j.jmrt.2025.08.047 ↗
18. Anisotropic tensile creep behavior in laser powder bed fusion manufactured Al–Mn–Mg–Sc–Zr alloy10.1016/j.jmrt.2023.12.128 ↗
19. The effects of η phases and Al3 (Er, Zr) particles pre-precipitation on the hot workability and recrystallization of Al–Zn–Mg–Er–Zr alloy10.1016/j.jmrt.2024.01.223 ↗
20. Influence of SLM scan-speed on microstructure, precipitation of Al3Sc particles and mechanical properties in Sc-and Zr-modified Al-Mg alloys10.1016/j.matdes.2017.11.053 ↗
21. Strength-ductility synergy of selective laser melted Al-Mg-Sc-Zr alloy with a heterogeneous grain structure
22. Influence of heat treatment on corrosion behavior of rare earth element Sc modified Al-Mg alloy processed by selective laser melting10.1016/j.apsusc.2020.145330 ↗
23. Effect of the heat treatment on the mechanical properties and microstructure of Scalmalloy® manufactured by selective laser melting (SLM) under certified conditions10.1016/j.matchar.2022.112549 ↗
24. Manipulating the microstructure and tensile properties of selective laser melted Al–Mg-Sc-Zr alloy through heat treatment10.1016/j.jallcom.2020.154773 ↗
25. Selective laser melting Al-3.4Mg-0.5Mn-0.8Sc-0.4Zr alloys: from melting pool to the microstructure and mechanical properties10.1016/j.msea.2021.141889 ↗
26. Selective laser melting of a high strength AlMnSc alloy: alloy design and strengthening mechanisms10.1016/j.actamat.2019.04.014 ↗
27. Microstructure and properties of SLM AlSi10Mg: understanding the influence of the local thermal history10.1016/j.promfg.2020.04.121 ↗
28. Impact of layer rotation on micro-structure, grain size, surface integrity and mechanical behaviour of SLM Al-Si-10Mg alloy10.1016/j.jmrt.2020.06.090 ↗
29. Additive manufacturing of a high strength Al-5Mg2Si-2Mg alloy: microstructure and mechanical properties10.1016/j.jmst.2021.02.048 ↗
30. Effects of porosity and microstructure on the fatigue fracture properties of ti6al4v alloy produced through selective laser melting
31. Propagation characteristics of ultrasonic in SLM manufactured AlSi10Mg10.1016/j.ultras.2023.107134 ↗
32. Enhanced mechanical performance of SLM-printed inconel 718 lattice structures through heat treatments10.3390/met15070686 ↗
33. Microstructure and mechanical properties of Zr-modified aluminum alloy 5083 manufactured by laser powder bed fusion
34. Selective laser melting of Al-Fe-V-Si heat-resistant aluminum alloy powder: modeling and experiments10.1007/s00170-015-7137-8 ↗
35. Influence of heat treatment on corrosion behavior of rare earth element Sc modified Al-Mg alloy processed by selective laser melting10.1016/j.apsusc.2020.145330 ↗
36. Investigation and characterization of an Al-Mg-Zr-Sc alloy with reduced Sc content for laser powder bed fusion10.1016/j.jallcom.2022.166519 ↗
37. Anisotropic corrosion behavior of Sc and Zr modified Al-Mg alloy produced by selective laser melting10.1016/j.corsci.2020.108657 ↗
38. Dynamic recrystallization and precipitation in an Al–Mg–Sc alloy: effect of strain rate10.1016/j.jmrt.2022.05.132 ↗
39. Influences of trace additions of Sc/Zr elements on high-temperature tensile behaviors of the Al-Mg-Mn alloys
40. The evolutions of flow stress and microstructure of Al-Mg-Mn-Sc-Zr alloy at elevated temperatures10.1016/j.matchar.2021.111560 ↗
41. Spatiotemporal correlations in the Portevin-Le chatelier band dynamics during the type B-type C transition10.1016/j.msea.2019.04.036 ↗
42. Enhancement of strength and electrical conductivity for a dilute Al-Sc-Zr alloy via heat treatments and cold drawing10.1016/j.jmst.2018.12.023 ↗