journal article·2025-03Open access

Multi-scale mechanical properties of Al–Mg–Zr–Sc alloys fabricated by direct metal laser sintering: Towards single-material composites

Dominic Zettel, Piotr Breitkopf, Ludovic Cauvin, Pascal Nicolay, Roland Willmann

Abstract

This study proposes a methodology for experimentally deriving parameter-dependent mechanical properties of DMLS-printed aluminum. Eighty-five specimens were produced using seventeen distinct parameter sets, designed through a Design of Experiments approach, and subjected to non-destructive and destructive testing. The results reveal a strong correlation between printing parameters, porosity, and mechanical performance, with average pore areas ranging from 0.037% to 21.161% and varied pore types (spherical pores, keyhole pores, and lack of fusion). Correspondingly, mechanical properties showed a broad range: tensile strength (105.3 MPa–459.0 MPa), Young's modulus (23.38 GPa–69.77 GPa), and yield strength (105.2 MPa–444.8 MPa). Single-material composites were fabricated by integrating dense and porous structures within a single geometry. Tensile testing of these composites showed that geometry and the cross-sectional ratio of ductile material influence mechanical properties significantly (tensile strengths ranging from 89.8 MPa to 112.2 MPa), with stress-strain responses displaying atypical behavior due to the brittle, porous matrix and embedded ductile truss-lattice structures.
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Research context

OpenAlex topics: Additive Manufacturing Materials and Processes · Additive Manufacturing and 3D Printing Technologies · High Entropy Alloys Studies

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (53)

Show source-provided references
1. Zhang · 2018
2. Toyserkani · 2021
3. Reducing porosity in AlSi10Mg parts processed by selective laser melting
4. Additive manufacturing: technology, applications and research needs10.1007/s11465-013-0248-8 ↗
5. Optimization of parameters in laser powder deposition AlSi10Mg alloy using Taguchi method10.1016/j.optlastec.2018.10.030 ↗
6. A review on process parameters, microstructure and mechanical properties of additively manufactured AlSi10Mg alloy10.1016/j.matpr.2022.09.100 ↗
7. An overview of direct metal laser sintering (DMLS) technology for metal 3D printing10.18311/jmmf/2022/30681 ↗
8. Effect of process parameters on powder bed fusion maraging steel 300: a review10.1007/s40516-022-00182-6 ↗
9. Influence of process parameters on part quality and mechanical properties for DMLS and SLM with iron-based materials10.1007/s00170-011-3643-5 ↗
10. Achieving low surface roughness AlSi10Mg_200C parts using direct metal laser sintering
11. Investigating mechanical and surface porosity values of high-performing 3D-printed titanium alloys along with stress-relieving heat treatments10.1007/s00170-023-12552-1 ↗
12. Size effects on geometrical accuracy for additive manufacturing of Ti-6Al-4V ELI parts10.1007/s00170-019-04184-1 ↗
13. Additive manufactured AlSi10Mg samples using Selective Laser Melting (SLM): microstructure, high cycle fatigue, and fracture behavior10.1016/j.matdes.2011.07.067 ↗
14. Investigation of laser scan strategy on tensile and microstructural characteristics of Inconel 718 fabricated by DMLS process
15. Evaluation of overall marginal accuracy of DMLS copings fabricated using 3 different DMLS printing machines
16. Dimensional accurary of internal cooling channel made by selevtive laser melting (SLM) and direct metal laser sintering (DMLS) process in fabrication of internally cooled cutting tools
17. Comparison of the structure and properties of samples from Ti-6Al-4V alloy received on different printers for 3D printing
18. Investigation and characterization of an Al-Mg-Zr-Sc alloy with reduced Sc content for laser powder bed fusion10.1016/j.jallcom.2022.166519 ↗
19. Influence of LPBF-surface characteristics on fatigue properties of scalmalloy10.3390/met11121961 ↗
20. Influence of contour scans on surface roughness and pore formation using Scalmalloy manufactured by laser powder bed fusion (PBF-LB)
21. Microstructural evaluation and tensile properties of Al-Mg-Sc-Zr alloys prepared by LPBF10.3390/cryst13060913 ↗
22. C. N. Kuo, P. C. Peng, D. H. Liu and C. Y. Chao, "Microstructure Evolution and Mechanical Property Response of 3D-Printed Scalmalloy with different Heat-Treatment times at 325°C," Metals, Volume 11, Issue 4, ISSN: 2075-4701, https://doi.org/10.3390/met11040555, pp. 1-12, 29 March 2021.10.3390/met11040555 ↗
23. Study of the influence of laser energy density on the surface roughness of Scalmalloy samples manufactured by DMLS technology10.1088/1757-899X/1193/1/012036 ↗
24. The effect of powder reuse on the surface chemical composition of the Scalmalloy powder in Powder Bed Fusion - laser Beam process
25. An improved process scan stretegy to obtain high-performance fatigue properties for Scalmalloy10.1016/j.matdes.2022.111410 ↗
26. An investigation of the influence of changing energy volume densities to produce a complete process parameter window for selective laser melting of scalmalloy
27. A detailed study on optimizing DMLS process parameters to enhance AlSi10Mg metal component properties
28. R. Sitek,. K. Kulikowski,. K. Paradowski, K. Gancarczyk,. M. Losertová,. A. Kobayashi,. J. Moneta and. J. Kamiński, "Influence of Ion Nitriding on Microstructure and Properties of Haynes 282 Nickel Superalloy Specimens Produced Using DMLS Technique," Materials, Volume 16, Issue 14, ISSN 1996-1944, https://doi.org/10.3390/ma16145020, pp. 1-17, 15 July 2023.10.3390/ma16145020 ↗
29. R. Vandzura,. V. Simkulet,. M. Gelatko,. M. Hatala and. Z. Mitalova, "Effect of Hardening Temperature on Maraging Steel Samples Prepared by Direct Metal Laser Sintering Process," Machines, Volume 11, Issue 3, ISSN 2075-1702, https://doi.org/10.3390/machines11030351, pp. 1-15, 3 March 2023.10.3390/machines11030351 ↗
30. Investigation of impact strength, micro hardness and metallurgical analysis of DMLS fabricated CoCrMo alloy samples10.1007/s40516-022-00195-1 ↗
31. Process-dependent material characteristics of additively manufactured specimens
32. 15ème colloque national en calcul des structures (CSMA), Université Polytechnique Hauts-de-Franz [UPHF]
33. European community on computational methods in applied Sciences (ECCOMAS)
34. Direct Metal Laser Sintering - setup-dependent material characteristics of topologies for multi-functional part optimization
35. Myers · 1972
36. L. Ramosena, T. C. Dzogbewu and W. B. du Preez, "Direct metal laser sintering production of Ti6Al4V parts from a purely elemental powder blend," Materials, Volume 15, Issue 22, ISSN 1996-1944, https://doi.org/10.3390/ma15228193, pp. 1-21, 18 November 2022.10.3390/ma15228193 ↗
37. The effect of manufacturing defects on the fatigue behavior of Ti-6Al-4V specimens fabricated using selective laser melting10.4028/www.scientific.net/AMR.891-892.1519 ↗
38. 3D printing of Aluminium alloys: additive manufacturing of Aluminium alloys using selective laser melting10.1016/j.pmatsci.2019.100578 ↗
39. Kalpakjian · 2011
40. Läpple · 2010
41. Rolfe · 1977
42. Effect of grain refinement on jerky flow in an Al-Mg-Sc alloy10.1007/s11661-016-3381-2 ↗
43. Serrated plastic flow10.1007/BF02743993 ↗
44. Cryogenic forming of Al-Mg alloy sheet for car outer body applications10.1002/adem.201900089 ↗
45. The Portevin-Le Chatelier effect: a review of experimental findings10.1088/1468-6996/12/6/063001 ↗
46. Effect of powder reuse on mechanical properties of Ti-6Al-4V produced through selective laser melting10.1016/j.ijrmhm.2020.105273 ↗
47. Antony · 2023
48. Montgomery · 2017
49. Laser powder bed fusion of high solute Al-Zn-Mg alloys: processing, characterisation and properties10.1016/j.matdes.2020.109183 ↗
50. Failure of metals I: brittle and ductile fracture10.1016/j.actamat.2015.12.034 ↗
51. A review on phase-field models of brittle fracture and a new fast hybrid formulation10.1007/s00466-014-1109-y ↗
52. Recycling of composite materials10.1016/j.cep.2011.09.007 ↗
53. Composite material recycling technology - state of the art and sustainable development for the 2020s10.3390/jcs5010028 ↗