journal article·2025-01Open access

Investigation on the microstructure evolution and deformation behavior of Mg–2Zn-0.5Mn-0.2Ca-xNd/yLa alloy by in-situ tensile

Jie Mi, Shengquan Liang, Shiyu Luan, Qianlong Ren, Xin Che, Peipeng Jin

Abstract

Multi-microalloying rare earth elements are expected to improve the properties of magnesium alloys. In this study, Mg–2Zn-0.5Mn-0.2Ca-0.3Nd-0.7La (alloy A) and Mg–2Zn-0.5Mn-0.2Ca-0.7Nd-0.3La (alloy B) alloys with microalloying Nd and La were developed. Compared with alloy B, the tensile load of alloy A is higher and the plasticity is lower. The microstructure evolution and deformation behavior analyzed by in-situ SEM and EBSD show that the basal texture intensity of alloy A is larger, which promotes more prismatic slip during the tensile process, resulting in higher tensile load, while alloy B with higher Nd content produces more pyramidal slip in the later stage of deformation, which contributes to higher plasticity. The Nd–Zn phase, Mg–Zn phase and Mg–Mn phase are mainly formed in the two alloys. The alloy B with higher Nd content precipitates more Nd–Zn phase. The Nd–Zn phase rich in Zn layer promote dislocation transfer and improve the plasticity of alloy B, while more Mg–Zn phase and Mg–Mn phase in alloy A pin dislocations and improve strength. In addition, tensile twins are produced during the tensile of the two alloys and the content is similar, but the extremely low twin content makes its effect on the mechanical properties of the two alloys negligible. Therefore, the difference in mechanical properties of the two alloys is mainly related to the texture intensity and the content of the second phase precipitated by different additions of rare earth elements.
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Research context

OpenAlex topics: Magnesium Alloys: Properties and Applications · Aluminum Alloys Composites Properties · Advanced Welding Techniques Analysis

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (50)

Show source-provided references
1. Latest research advances on magnesium and magnesium alloys worldwide10.1016/j.jma.2020.02.003 ↗
2. Recent advances of high strength Mg-RE alloys: alloy development, forming and application10.1016/j.jmrt.2023.08.055 ↗
3. Drag effects of solute and second phase distributions on the grain growth kinetics of pre-extruded Mg-6Zn alloy10.1016/j.jmst.2016.06.025 ↗
4. Effect of Sb additions on the microstructural stability and mechanical properties of cast Mg-4Zn alloy10.1016/j.msea.2010.05.029 ↗
5. In vitro and in vivo assessment of squeeze-cast Mg-Zn-Ca-Mn alloys for biomedical applications10.1016/j.actbio.2022.07.040 ↗
6. Effect of Mn addition on grain refinement of biodegradable Mg-4Zn-0.5Ca alloy10.1016/j.jallcom.2016.03.182 ↗
7. Mechanical and in vitro corrosion properties of a heat-treated Mg-Zn-Ca-Mn alloy as a potential bioresorbable material10.36959/508/392 ↗
8. Mechanism of Mn on inhibiting Fe-caused magnesium corrosion10.1016/j.jma.2020.09.015 ↗
9. Determining critical Zn/Ca atomic ratio and its role in mechanical and corrosion properties of biodegradable Mg-Ca-Zn-Mn alloys10.1016/j.mtla.2024.102203 ↗
10. Microstructure and mechanical properties of extruded Mg-Zn-Mn-Ca alloys10.1016/j.jmrt.2024.08.001 ↗
11. High temperature mechanical behaviour of Mg-6Zn-1Y alloy with 1 wt.% calcium addition: reinforcing effect due to I-(Mg3Zn6Y1) and Mg6Zn3Ca2 phases10.1016/j.jma.2020.08.007 ↗
12. Development of dilute Mg-Zn-Ca-Mn alloy with high performance via extrusion10.1016/j.jallcom.2016.01.195 ↗
13. High-speed extrusion of dilute Mg-Zn-Ca-Mn alloys and its effect on microstructure, texture and mechanical properties10.1016/j.msea.2016.10.007 ↗
14. Extruded Mg-Zn-Ca-Mn alloys with low yield anisotropy10.1016/j.msea.2012.08.012 ↗
15. The effects of Ca and Mn on the microstructure, texture and mechanical properties of Mg-4Zn alloy10.1016/j.jma.2020.03.012 ↗
16. Recent developments in rare-earth free wrought magnesium alloys having high strength: a review10.1016/j.jallcom.2015.12.057 ↗
17. Effects of rare-earth elements Gd and Y on the solid solution strengthening of Mg alloys10.1016/j.jallcom.2009.02.131 ↗
18. Effects of cerium addition on the microstructure, mechanical properties and hot workability of ZK60 alloy10.1016/j.msea.2012.09.026 ↗
19. Effects of extrusion speed on the microstructure and mechanical properties of ZK60 alloys with and without 1wt% cerium addition10.1016/j.msea.2013.06.073 ↗
20. Influence of Nd on microstructure and bio-corrosion rsistance of Mg-Zn-Mn-Ca alloy10.1016/S1875-5372(13)60052-1 ↗
21. Study on the low mechanical anisotropy of extruded Mg-Zn-Mn-Ce-Ca alloy tube in the compression process10.1016/j.jma.2022.07.001 ↗
22. Study on microstructure evolution and deformation behavior of Mg-Zn base alloy pipes during hot bending10.1016/j.jmrt.2024.08.034 ↗
23. Improving tensile properties and corrosion resistance of Mg-Zn-Ca-Mn alloy via Gd addition10.1016/j.intermet.2023.108000 ↗
24. Role of RE in the deformation and recrystallization of Mg alloy and a new alloy design concept for Mg-RE alloys10.1016/j.scriptamat.2014.12.010 ↗
25. In-situ isothermal aging TEM analysis of a micro Cu/ENIG/Sn solder joint for flexible interconnects10.1016/j.jmst.2023.06.020 ↗
26. Bo-LSTM based cross-sectional profile sequence progressive prediction method for metal tube rotate draw bending10.1016/j.aei.2023.102152 ↗
27. Enhancing impact resistance of hybrid structures designed with triply periodic minimal surfaces10.1016/j.compscitech.2023.110365 ↗
28. Microstructure classification of steel samples with different heat-treatment processes based on laser-induced breakdown spectroscopy (LIBS)10.1039/D3JA00453H ↗
29. In-situ SEM and EBSD investigation of the deformation behavior of extruded Mg-6Al-1Zn-1.1Sc alloy10.1088/2053-1591/acf190 ↗
30. An investigation of the deformation and cracking mechanism of Mg-1Al-12Y alloys based on in-situ SEM/EBSD slip trace analysis10.1016/j.msea.2022.144016 ↗
31. The hot deformation behavior and microstructural evolution of as-cast Mg-2Zn-0.5Mn-0.2Ca-0.3Nd-0.7La alloy10.1016/j.jmrt.2022.12.027 ↗
32. Heterogeneous bimodal microstructure and its formation mechanism of Mg-Gd-Y-Zn-Zr alloy during isothermal compression10.1016/j.jallcom.2023.169523 ↗
33. Revealing the deformation behavior and microstructure evolution in Mg-12Y-1Al alloy during hot compression10.1016/j.jallcom.2023.169462 ↗
34. Hot deformation behavior and resultant microstructural evolution of dilute Mg-Bi-Sn-Mn alloy during hot compression10.1016/j.jmrt.2023.08.093 ↗
35. Slip, twinning, and fracture in hexagonal close-packed metals10.1007/BF02648537 ↗
36. Hardening evolution of AZ31B Mg sheet10.1016/j.ijplas.2006.03.005 ↗
37. Grain refinement, texture, and mechanical properties of a magnesium alloy after radial-shear rolling10.1016/j.jallcom.2018.09.065 ↗
38. Quasi in-situ EBSD analysis of twinning-detwinning and slip behaviors in textured AZ31 magnesium alloy subjected to compressive-tensile loading10.1016/j.jma.2021.08.025 ↗
39. Dislocation behavior in a polycrystalline Mg-Y alloy using multi-scale characterization and VPSC simulation10.1016/j.jmst.2021.03.087 ↗
40. Improving ductility of a Mg alloy via non-basal slip induced by Ca addition10.1016/j.ijplas.2019.04.020 ↗
41. Effect of grain size on slip activity in pure magnesium polycrystals10.1016/j.actamat.2014.10.001 ↗
42. Effects of cryogenic treatment on microstructures and mechanical properties of Mg-2Nd-4Zn alloy10.1016/j.matlet.2021.130699 ↗
43. Evolutions of CuZn5 and Mg2Zn11 phases during ECAP and their impact on mechanical properties of Zn-Cu-Mg alloys10.1016/j.jmrt.2022.11.095 ↗
44. An Orowan precipitate strengthening equation for mechanical twinning in Mg10.1016/j.ijplas.2018.08.010 ↗
45. Microstructure evolution and coercivity enhancement in Nd-Zn alloy-doped Nd-Fe-B powders10.1016/j.jmmm.2022.169427 ↗
46. The transformation of slip dislocations during twinning of copper-aluminum alloy crystals
47. Twins as barriers to basal slip in hexagonal-close-packed metals10.1007/s11661-002-0149-7 ↗
48. Effect of dislocation-twin boundary interaction on deformation by twin boundary migration10.1016/j.msea.2016.03.061 ↗
49. Extension twin variant selection during uniaxial compression of a magnesium alloy10.1016/j.msea.2012.04.046 ↗
50. Strain compatibility effect on the variant selection of connected twins in magnesium10.1016/j.matdes.2015.03.041 ↗