journal article·2025-09Open access

Effect of low-temperature tempering on microstructure and mechanical behavior of ultra-high-strength medium-Mn steel

Wei Liu, Zhiqiang Wu, Tao Li, Hongang Zhou, Zhihui Cai, Kui Chen

Abstract

This study comprehensively examined the effects of low-temperature tempering on the microstructure and tensile properties of cold-rolled medium Mn steel. The initial microstructure contained blocky and film-like retained austenite (RA) along with banded, blocky, and lath martensite. After tempering, the microstructure was primarily composed of banded and blocky martensite, along with some granular and blocky RA. During tempering, migration of the austenite/martensite interface into the austenite phase resulted in the transformation of 18 vol.% of the blocky and film-like austenite into martensite. The tempering process relieved residual stresses from cold rolling. Carbon segregation at the martensite/austenite interfaces and the precipitation of nano-carbides increased the yield strength of the tempered samples by 554 MPa. The harder martensitic matrix enhanced RA stability, and stress–strain accumulation induced a staged martensitic transformation in the RA, reflected by more pronounced serrations in the strain hardening rate curve (S2). The improved RA stability contributed to strain hardening, raising the tensile strength by 282 MPa.
Source: openalex_inverted_index · Quality: baseline

Research context

OpenAlex topics: Microstructure and Mechanical Properties of Steels · Metallurgy and Material Forming · Metal Alloys Wear and Properties

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (61)

Show source-provided references
1. Strain rate effect on tensile flow behavior and anisotropy of a medium-manganese TRIP steel10.1007/s11837-018-2830-3 ↗
2. Heterogeneous nano/ultrafine-grained medium Mn austenitic stainless steel with high strength and ductility10.1016/j.msea.2018.04.022 ↗
3. Effect of intercritical annealing time on hydrogen embrittlement of warm-rolled medium Mn steel10.1016/j.msea.2018.04.100 ↗
4. Precipitation strengthening of Cu/NiAl co-precipitates in a martensite-austenite dual-phase steel10.1016/j.matchar.2021.111589 ↗
5. Mechanical properties and deformation mechanisms of a novel austenite-martensite dual phase steel10.1016/j.ijplas.2020.102677 ↗
6. Tailoring retained austenite and mechanical property improvement in Al–Si–V containing medium Mn steel via direct intercritical rolling10.1016/j.msea.2022.143904 ↗
7. Significance of control of austenite stability and three-stage work-hardening behavior of an ultrahigh strength–high ductility combination transformation-induced plasticity steel10.1016/j.scriptamat.2013.02.010 ↗
8. Recent progress in medium-Mn steels made with new designing strategies, a review10.1016/j.jmst.2017.06.017 ↗
9. Microstructure and mechanical properties of hot-rolled medium-Mn steel containing 3% aluminum10.1016/j.msea.2016.11.036 ↗
10. Medium Mn transformation-induced plasticity steels: recent progress and challenges10.1016/j.scriptamat.2016.07.013 ↗
11. Enhanced work-hardening behavior and mechanical properties in ultrafine-grained steels with large-fractioned metastable austenite10.1016/j.scriptamat.2010.06.023 ↗
12. Deformation and fracture in martensitic carbon steels tempered at low temperatures10.1007/s11663-001-0044-4 ↗
13. Effect of tempering on the microstructure and tensile properties of a martensitic Medium-Mn lightweight steel10.1007/s11661-019-05190-4 ↗
14. The impact of periodic distribution of alloying elements during tempering in a multistep partitioned manganese steels on mechanical behavior: experiments, simulation and analysis10.1016/j.msea.2019.138357 ↗
15. Strong and ductile medium manganese steel processed by low-temperature partitioning10.1080/02670836.2022.2163748 ↗
16. Influence of carbon partitioning kinetics on final austenite fraction during quenching and partitioning10.1016/j.scriptamat.2009.03.021 ↗
17. Interface migration between martensite and austenite during quenching and partitioning (Q&P) process
18. Potential significance of low tempering treatment in improving the mechanical properties of a cold‐rolled and intercritical annealed medium Mn steel10.1002/srin.202100814 ↗
19. The influence of tempering temperature on the reversed austenite formation and tensile properties in Fe–13%Cr–4%Ni–Mo low carbon martensite stainless steels10.1016/j.msea.2011.01.078 ↗
20. Calculation method for dislocation density in TWIP steel based on neutron diffraction and synchrotron radiation X-ray diffraction
21. The contrast factors of dislocations in cubic crystals: the dislocation model of strain anisotropy in practice10.1107/S0021889899009334 ↗
22. Microstructure-mechanical properties relationships for quenching and partitioning (Q&P) processed steel10.1016/j.actamat.2016.04.048 ↗
23. Achieving high ductility in a 1.4 GPa grade medium Mn lightweight TRIP/TWIP steel with hierarchical lamellar structure10.1016/j.msea.2022.144118 ↗
24. Strong and ductile medium-Mn steel achieved via controlled martensite tempering10.1080/02670836.2023.2207371 ↗
25. Effect of partitioning temperature on the microstructure and evolution of medium manganese steel10.1080/03019233.2023.2216097 ↗
26. Microstructure evolution and yield strength improvement of a low carbon medium manganese steel experienced intercritical annealing, pre-straining and tempering10.1016/j.matchar.2022.112439 ↗
27. Tempering and intercritical annealing of air-hardening 4 wt% medium manganese steels10.1002/srin.202100180 ↗
28. 0.1C–11Mn medium manganese steel treated by quenching and tempering process10.1080/02670836.2022.2087027 ↗
29. Transformation-induced ductility of reverse austenite evolved by low-temperature tempering of martensite
30. Tempering and austempering of double soaked medium manganese steels10.3389/fmats.2020.622131 ↗
31. Enhanced strength-ductility of medium Mn steel by quenching, partitioning and tempering10.1080/02670836.2020.1719305 ↗
32. Model for the interaction between interface migration and carbon diffusion during annealing of martensite–austenite microstructures in steels10.1016/j.scriptamat.2008.02.045 ↗
33. Effect of cryogenic treatment on internal residual stresses of hydrogen-resistant steel10.3390/mi12101179 ↗
34. Ultrahigh tensile strength achieved in a lightweight medium Mn steel via prominent work hardening10.1016/j.jmst.2022.11.009 ↗
35. Plastic yielding in lath martensites – an alternative viewpoint10.1016/j.actamat.2018.04.039 ↗
36. Accurate measurement of the orientation relationship of lath martensite and bainite by electron backscatter diffraction analysis10.1016/j.scriptamat.2009.02.053 ↗
37. The morphology and crystallography of lath martensite in Fe-C alloys10.1016/S1359-6454(02)00577-3 ↗
38. Crystallographic features of lath martensite in low-carbon steel10.1016/j.actamat.2005.11.001 ↗
39. Controllable selection of martensitic variant enables concurrent enhancement of strength and ductility in a low-carbon steel
40. Nanoscale precipitation and its influence on strengthening mechanisms in an ultra-high strength low-carbon steel10.1016/j.ijplas.2018.09.009 ↗
41. Effect of microstructure on retained austenite stability and work hardening of TRIP steels10.1016/j.msea.2011.02.032 ↗
42. On the influence of interactions between phases on the mechanical stability of retained austenite in transformation-induced plasticity multiphase steels10.1007/s11661-001-1027-4 ↗
43. Transmission electron microscopy analysis of yielding in ultrafine-grained medium Mn transformation-induced plasticity steel10.1007/s11661-013-1638-6 ↗
44. On the microstructural characteristics influencing the yielding behavior of ultra-fine grained medium-Mn steels10.1016/j.actamat.2017.07.056 ↗
45. Microstructure refinement and mechanical properties of severely deformed Al–Mg–Li alloys10.1016/S0921-5093(01)01681-1 ↗
46. Partitioning of C and Mn during intercritical annealing and transformation of retained austenite during deformation in medium Mn steel10.1002/srin.202200731 ↗
47. Heterostructured materials: superior properties from hetero-zone interaction
48. Perspective on hetero-deformation induced (HDI) hardening and back stress
49. Understanding the factors controlling the hardness in martensitic steels10.1016/j.scriptamat.2015.08.010 ↗
50. Micromechanical finite element analysis of strain partitioning in multiphase medium manganese TWIP+TRIP steel10.1016/j.actamat.2016.02.001 ↗
51. Computational design of nanostructured steels employing irreversible thermodynamics10.1179/1743284712Y.0000000179 ↗
52. Microstructures and hardness of as-quenched martensites (0.1–0.5%C)10.1016/j.actamat.2011.05.061 ↗
53. Martensite in steel: strength and structure10.1016/S0921-5093(99)00288-9 ↗
54. Effect of chemical composition on work hardening of Fe-Mn-C TWIP steels10.1179/026708309X12535382371852 ↗
55. Influence of carbon content on the microstructure, martensitic transformation and mechanical properties in austenite/ε-martensite dual-phase fe–mn–c steels10.1016/j.actamat.2012.09.078 ↗
56. The dislocation distribution, flow stress, and stored energy in cold-worked polycrystalline silver10.1080/14786436008238300 ↗
57. Work hardening and deformation sub-structure in iron single crystals deformed in tension at 298°k10.1080/14786436508224942 ↗
58. Surface and grain boundary segregation on and in iron and steels10.2355/isijinternational.29.529 ↗
59. Phase boundary segregation-induced strengthening and discontinuous yielding in ultrafine-grained duplex medium-Mn steels10.1016/j.actamat.2020.09.007 ↗
60. Microstructure-mechanical properties evolution of hot-rolled medium Mn steel: effects of short-time holding and low-temperature tempering following ultrafast heating
61. Effect of prestrain and tempering on the residual stress of low‐carbon microalloyed steel