journal article·2025-11Open access

A comparative study of thermal aging behavior of CF8M cast austenitic stainless steel and ER316L austenitic stainless steel weld

Shoaib Mehboob, Byeong Seo Kong, Hyun Joon Eom, Taejeong An, Chaewon Jeong, Changheui Jang

Abstract

Cast austenitic stainless steels (CASSs) and austenitic stainless steel welds (ASSWs) are susceptible to thermal aging embrittlement due to hardening of δ-ferrite during long-term exposure to high temperature of nuclear power plants. This study focused on comparison of thermal aging behavior of CF8M CASS and ER316L ASSW, with similar ferrite content. To simulate the thermal aging embrittlement observed during light water reactor operations, CF8M and ER316L weld were thermally aged at 343 °C, 375 °C and 400 °C for up to 20,000 h. The microstructural analysis revealed that thermal aging induced spinodal decomposition of δ-ferrite was observed in both CF8M and ER316L weld. In CF8M, G-phase and ω-phase precipitates appeared after 5000 h of aging at 400 °C while in ER316L weld, Ni-clusters appeared after 5000 h and G-phase precipitates formed after 10,000 h and 20,000 h of thermal aging. The mechanical properties such as nanohardness of δ-ferrite, tensile strength and fracture toughness were compared for unaged and aged CF8M and ER316L weld. The kinetics of thermal aging embrittlement was evaluated by determining the activation energy based on δ-ferrite hardening and fracture toughness degradation. While the hardening of δ-ferrite exhibited slightly faster kinetics for CF8M, the loss of fracture toughness exhibited comparable kinetics for both CF8M and ER316L weld.
Source: openalex_inverted_index · Quality: baseline

Research context

OpenAlex topics: Hydrogen embrittlement and corrosion behaviors in metals · Microstructure and Mechanical Properties of Steels · High Temperature Alloys and Creep

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (38)

Show source-provided references
1. Mechanical property degradation and microstructural evolution of cast austenitic stainless steels under short-term thermal aging10.1016/j.jnucmat.2017.07.059 ↗
2. Effect of microstructure evolution at the interphase boundary on the thermal ageing embrittlement of CF8M cast austenitic stainless steel10.1016/j.ijpvp.2022.104679 ↗
3. Influence of δ-Ferrite content on thermal aging induced mechanical property degradation in cast stainless steels
4. Microstructure and deformation behavior of thermally aged cast austenitic stainless steels
5. Low temperature thermal aging of austenitic stainless steel welds: kinetics and effects on mechanical properties10.1016/j.msea.2011.11.055 ↗
6. Thermal aging effect on elevated temperature deformation mechanisms of 316L stainless steel weld metal by small punch test10.1016/j.msea.2025.148005 ↗
7. Chopra · 2016
8. Materials challenges in nuclear energy10.1016/j.actamat.2012.11.004 ↗
9. Poehler · 2024
10. Effects of ferrite content and concentrations of carbon and silicon on weld solidification cracking susceptibility of stainless steels10.1016/j.jmrt.2023.06.018 ↗
11. Correlation of mechanics degradation and thermal aging damage defects in Z3CN20.09M cast austenitic stainless steels10.1016/j.jnucmat.2024.155558 ↗
12. Thermal aging behaviors of duplex stainless steels used in nuclear power plant: a review10.1016/j.jnucmat.2020.152693 ↗
13. A comprehensive study of the effects of long-term thermal aging on the fracture resistance of cast austenitic stainless steels10.1016/j.net.2021.08.022 ↗
14. Microstructures and mechanical properties of cast austenite stainless steels after long-term thermal aging at low temperature10.1016/j.matdes.2013.02.061 ↗
15. Effect of Ni, Mo and Mn content on spinodal decomposition kinetics and G-phase precipitation of aged model cast austenitic stainless steels10.1016/j.jnucmat.2021.153123 ↗
16. Evaluation of the thermal ageing of austenitic stainless steel welds with 10 % of δ-ferrites10.1016/j.ijpvp.2018.10.006 ↗
17. Effects of ferrite content on the mechanical properties of thermal aged duplex stainless steels10.1016/j.msea.2014.11.065 ↗
18. Thermal aging effect on fracture toughness of GTAW/SMAW of 316L stainless steel: experiments and applicability of existing CASS models10.1016/j.net.2020.10.007 ↗
19. P. Noga, T. Skrzekut, M. Wędrychowicz, M. S. Węglowski, and M. Wiewióra, "The influence of various welding methods on the microstructure and mechanical properties of 316Ti steel," Materials, vol. 17, no. 7, doi: 10.3390/ma17071681.10.3390/ma17071681 ↗
20. Effects of prior solution treatment on thermal aging behavior of duplex stainless steels
21. Long-term thermal aging performance of welding structures in primary coolant pipes for nuclear power plants10.1016/j.anucene.2020.107793 ↗
22. Spinodal decomposition in functionally graded super duplex stainless steel and weld metal10.1007/s11661-018-4600-9 ↗
23. Stability and strengthening effect of aging induced-nanofeatures in δ-ferrite in an austenitic stainless-steel weld10.1016/j.jmrt.2023.02.112 ↗
24. Evaluation of thermal ageing activation energy of δ-ferrite in an austenitic stainless steel weld using nanopillar compression test10.1016/j.scriptamat.2020.05.046 ↗
25. Evaluation of the thermal aging of δ-ferrite in austenitic stainless steel welds by electrochemical analysis10.1038/s41598-018-33422-x ↗
26. Long-term thermal aging of austenitic stainless-steel weld: microstructure evolution in δ-ferrite and δ/γ phase boundary and apparent recovery of mechanical properties10.1016/j.jmrt.2024.07.144 ↗
27. Evaluation of thermal aging activation energies based on multi-scale mechanical property tests for an austenitic stainless steel weld beads10.1016/j.msea.2022.142629 ↗
28. Short communication: characterization of Mo-rich precipitates in δ-ferrite of thermally aged Mo-bearing cast austenitic stainless steel10.1016/j.jnucmat.2025.155747 ↗
29. Effect of proton irradiation on δ-ferrite in the thermally aged austenitic stainless steel weld: precipitation of G-phase and additional hardening10.1016/j.jnucmat.2020.152656 ↗
30. Measurement of hardness and elastic modulus by instrumented indentation: advances in understanding and refinements to methodology10.1557/jmr.2004.19.1.3 ↗
31. ASTM E8/E8M-22, standard test methods for tension testing of metallic materials
32. ASTM E1820-22, standard test method for measurement of fracture toughness
33. Using automated J-R curve analysis software to simplify testing and save time
34. Degradation of impact toughness in cast stainless steels during long-term thermal aging10.1016/j.jnucmat.2020.152524 ↗
35. Evolution of nano-sized precipitates in δ-ferrite of high-Cu CF8M with thermal aging and their stability against reversion heat treatment10.1016/j.jmrt.2025.05.135 ↗
36. Precipitation sequence of nanoscale precipitates in δ-ferrite of CF8M during short-term thermal aging: role of Ni and Cu
37. Effect of external stress on the Fe–Cr phase separation in 15-5 PH and Fe–15Cr–5Ni alloys10.1016/j.ultramic.2012.12.004 ↗
38. Effects of long-term thermal aging on bulk and local mechanical behavior of ferritic-austenitic duplex stainless steels10.1016/j.msea.2018.02.058 ↗