journal article·2025-05Open access

Simultaneous improvement of strength and ductility in Fe–Mn–Al–C steel realized by cold rolling plus aging treatment

Ziyuan Gao, Qing Yin, Qingfeng Kang, Hui Wang, Haifeng Xu, Zhengdong Liu, Wenquan Cao

Abstract

In the Fe–Mn–Al–C low-density steels, aging treatment is generally employed to strengthen the steels through the formation of κ-carbides, which however results in a reduced strain-hardening rate and ductility due to the shearable nature of the κ-carbides. Here, we report an aging-induced unprecedented improvement in both the strength and ductility of a cold-rolled Fe–Mn–Al–C steel. Specifically, the aging treatment at 550 °C for 10 h results in an increment in ultimate tensile strength from 1176 MPa to 1251 MPa and uniform elongation from 5.00 % to 12.11 % compared to the cold-rolled specimen at 30 % rolling reduction. Microstructural examination revealed that the aging treatment resulted in preferential precipitation of κ-carbides within the existing dislocation structures formed during cold-rolling. The pinning effect of the κ-carbides suppressed the activity of dislocation cross-slip and prevented the further development of these dislocation structures that could lead to the local strain softening. Moreover, new slip bands were generated owing to the shearing of κ-carbides, stimulating the activation of dislocation planar slip. These combined mechanisms enhanced the dislocation storage capacity in cold-rolled specimens, thereby improving both strain-hardening rates and uniform elongation. Additionally, the influence of cold-rolling reduction on the aging-induced variation in the strain-hardening behavior was also explored. This study provides a novel strategy to simultaneously enhance the strength and ductility of the cold-rolled Fe–Mn–Al–C low-density steel by simple aging treatment.
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Research context

OpenAlex topics: Microstructure and Mechanical Properties of Steels · Metal Alloys Wear and Properties · Metallurgy and Material Forming

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References (40)

Show source-provided references
1. Fe–Al–Mn–C lightweight structural alloys: a review on the microstructures and mechanical properties10.1088/1468-6996/14/1/014205 ↗
2. High manganese and Aluminum steels for the military and transportation industry
3. Low-density steels: complex metallurgy for automotive applications
4. Current state of Fe-Mn-Al-C low density steels10.1016/j.pmatsci.2017.05.002 ↗
5. Influence of Al content and precipitation state on the mechanical behavior of austenitic high-Mn low-density steels10.1016/j.scriptamat.2012.08.038 ↗
6. Novel ultra-high-strength (ferrite + austenite) duplex lightweight steels achieved by fine dislocation substructures (Taylor lattices), grain refinement, and partial recrystallization10.1016/j.actamat.2015.06.024 ↗
7. Designing duplex, ultrafine-grained Fe-Mn-Al-C steels by tuning phase transformation and recrystallization kinetics10.1016/j.actamat.2017.09.026 ↗
8. Evolution of the microstructure and mechanical properties of an austenite–ferrite Fe–Mn–Al–C steel10.1016/j.msea.2015.07.043 ↗
9. Relationship between microstructures and tensile properties of an Fe-30Mn-8.5Al-2.0C alloy10.2320/matertrans.M2010013 ↗
10. Multistage strain hardening through dislocation substructure and twinning in a high strength and ductile weight-reduced Fe–Mn–Al–C steel10.1016/j.actamat.2012.07.018 ↗
11. Research status and development prospect of Fe–Mn–C–Al system low-density steels10.1016/j.jmrt.2023.06.037 ↗
12. Alloy design, combinatorial synthesis, and microstructure–property relations for low-density Fe-Mn-Al-C austenitic steels
13. Effect of aging treatment on microstructure and intrinsic mechanical behavior of Fe–31.4Mn–11.4Al–0.89C lightweight steel10.1016/j.jallcom.2015.10.016 ↗
14. Microstructure evolution and mechanical behavior of Fe–Mn–Al–C low-density steel upon aging10.1016/j.msea.2023.145109 ↗
15. Diagram of phase transformations in the austenite of hardened alloy Fe-28% Mn-8.5% Al-1% C-1.25% Si as a result of aging due to isothermal heating10.1007/s11041-006-0133-8 ↗
16. Effect of aging on the microstructure and deformation behavior of austenite base lightweight Fe–28Mn–9Al–0.8C steel10.1016/j.scriptamat.2010.07.036 ↗
17. Strengthening and strain hardening mechanisms in a precipitation-hardened high-Mn lightweight steel10.1016/j.actamat.2017.08.049 ↗
18. Microband-induced plasticity in a high Mn–Al–C light steel10.1016/j.msea.2008.05.042 ↗
19. Strain hardening by dynamic slip band refinement in a high-Mn lightweight steel10.1016/j.actamat.2016.06.037 ↗
20. Origin of extended tensile ductility of a Fe-28Mn-10Al-1C steel10.1007/s11661-009-9862-9 ↗
21. Brittle intermetallic compound makes ultrastrong low-density steel with large ductility10.1038/nature14144 ↗
22. Intragranular brittle precipitates improve strain hardening capability of Fe–30Mn–11Al–1.2C low-density steel10.1016/j.msea.2020.138984 ↗
23. X-ray line broadening from filed aluminium and wolfram10.1016/0001-6160(53)90006-6 ↗
24. β-Mn formation and aging effect on the fracture behavior of high-Mn low-density steels10.1016/j.scriptamat.2016.04.040 ↗
25. Direct observation of dislocation plasticity in high-Mn lightweight steel by in-situ TEM
26. An atom probe study of Kappa carbide precipitation and the effect of Silicon addition10.1007/s11661-014-2187-3 ↗
27. Linear complexions: confined chemical and structural states at dislocations10.1126/science.aab2633 ↗
28. Phase transitions in an Fe–9Al–30Mn–2.0C alloy10.1016/j.scriptamat.2007.07.007 ↗
29. Combined atom probe tomography and density functional theory investigation of the Al off-stoichiometry of κ-carbides in an austenitic Fe–Mn–Al–C low density steel10.1016/j.actamat.2016.01.007 ↗
30. Excellent combination of strength and ductility in an Fe–9Al–28Mn–1.8C alloy10.1016/j.scriptamat.2010.03.038 ↗
31. Aging hardening response and β-Mn transformation behavior of high carbon high manganese austenitic low-density Fe-30Mn-10Al-2C steel10.1016/j.msea.2017.07.055 ↗
32. Atomic and magnetic short-range order in Cu-17 at.% Mn10.1016/1359-6462(96)00010-3 ↗
33. Activation of dislocation sources in γ-phases of nickel-base superalloys studied by use of atomic-force microscopy and transmission electron microscopy10.1016/j.msea.2004.02.084 ↗
34. Enhanced mechanical properties of a Fe-Mn-Al-C austenitic low-density steel by increasing hot-rolling reduction10.1016/j.matchar.2023.113237 ↗
35. Microbanding mechanism in an Fe–Mn–C high-Mn twinning-induced plasticity steel10.1016/j.scriptamat.2013.03.010 ↗
36. Microstructural study of microbands in a Fe-30Mn-6.5Al-0.3C low-density steel deformed at cryogenic temperature by combined electron channeling contrast imaging and electron backscatter diffraction10.1016/j.actamat.2022.117980 ↗
37. Microstructural evolution in a non-cell forming metal: Al–Mg10.1016/0956-7151(93)90251-M ↗
38. Formation mechanism of κ-carbides and deformation behavior in Si-alloyed FeMnAlC lightweight steels10.1016/j.actamat.2020.08.003 ↗
39. Constriction energy in the presence of a solute field10.1063/1.372161 ↗
40. Atomistic study of nano-sized κ-carbide formation and its interaction with dislocations in a cast Si added FeMnAlC lightweight steel10.1016/j.msea.2016.07.029 ↗