Work-hardening stages and deformation mechanisms during tensile tests of commercially pure titanium containing α′-martensite
Source abstract
Abstract
High purity titanium usually requires thicker plates because of its limited mechanical strength on account of the low impurity content. Heterogeneous microstructures can be considered an alternative to enhance the material’s ductility and strength. This work incorporates precipitation of α′-phase trough partial recrystallization as an approach to achieving high strength-ductility in commercially pure Ti. Cold rolling and annealing were able to enhance mechanical properties and produced recovered and recrystallized constituents with different mechanisms of deformation. Tensile tests identified three work-hardening stages. Ti CP deformed plastically without significant mechanical twinning. Annealing at 400–500 °C achieved the most noteworthy increase in mechanical strength, achieving up to 600 MPa with a total elongation of 23%. Dislocations glide dominated the deformation process. Recrystallization resulted in grain growth, mostly to annealing temperatures of 700 to 900 °C, and in the increase of tensile strength, also enhanced by high volume fraction of α′-martensite.Graphical abstract
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Research context
OpenAlex topics: Titanium Alloys Microstructure and Properties · Advanced materials and composites · Intermetallics and Advanced Alloy Properties
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (41)
Show source-provided references
1. D. Banerjee, J.C. Williams, Perspectives on titanium science and technology. Acta Mater. 61, 844–879 (2013)10.1016/j.actamat.2012.10.043 ↗
2. X. Huang, K. Suzuki, M. Yuasa, Y. Chino, Microstructural and textural evolution of pure titanium during differential speed rolling and subsequent annealing. J. Mater. Sci. 49, 3166–3176 (2014)10.1007/s10853-014-8019-4 ↗
3. P. Singha, H. Pungotra, N.S. Kalsi, On the characteristics of titanium alloys for the aircraft applications. Mater. Today Proc. 4, 8971–8982 (2017)10.1016/j.matpr.2017.07.249 ↗
4. B.D. Bishoyia, R.K. Sabatb, S.K. Sahoo, Effect of temperature on microstructure and texture evolutions during uniaxial compression of commercially pure titanium. Mater. Sci. Eng. A 718, 398–411 (2018)10.1016/j.msea.2018.01.128 ↗
5. Y. Ma, M. Yang, F. Yuan, X. Wu, A review on heterogeneous nanostructures: a strategy for superior mechanical properties in metals. Metals 9(5), 14–17 (2019)10.3390/met9050598 ↗
6. D.K. Yang, P.D. Hodgson, C.E. Wen, Simultaneously enhanced strength and ductility of titanium via multimodal grain structure. Scripta Mater. 63, 941–944 (2010)10.1016/j.scriptamat.2010.07.010 ↗
7. J.L. Zhang, C.C. Tasan, M.J. Lai, D. Yan, D. Raabe, Partial recrystallization of gum metal to achieve enhanced strength and ductility. Acta Mater. 135, 400–410 (2017)10.1016/j.actamat.2017.06.051 ↗
8. P. Rostami, G. Faraji, A. Sadeghi, M. Baghani, Microstructure and mechanical properties of CP-titanium processed by ECAP followed by warm caliber rolling. Trans. Indian Inst. Met. 71(5), 1083–1090 (2018)10.1007/s12666-017-1243-2 ↗
9. A. Fattah-alhosseini, M.K. Keshavarz, Y. Mazaheri, A.R. Ansari, M. Karimi, Strengthening mechanisms of nano-grained commercial pure titanium processed by accumulative roll bonding. Mater. Sci. Eng. A 693, 164–169 (2017)10.1016/j.msea.2017.03.070 ↗
10. X. Zhao, W. Fu, X. Yang, T.G. Langdon, Microstructure and properties of pure titanium processed by equal-channel angular pressing at room temperature. Scripta Mater. 59, 542–545 (2008)10.1016/j.scriptamat.2008.05.001 ↗
11. V.K. Sahu, S. Gupta, N.P. Gurao, Effect of initial texture on the evolution of microstructure and texture during rolling of commercially pure titanium at room and cryogenic temperature. Metall. Mater. Trans. A 51(11), 5848–5860 (2020)10.1007/s11661-020-05979-8 ↗
12. K. Majchrowicz, A. Sotniczuk, B. Adamczyk-Cieślak, W. Chromiński, P. Jóźwik, Z. Pakieła et al., The influence of microstructure and texture on the hardening by annealing effect in cold-rolled titanium. J. Alloys Compd. 948, 169791 (2023)10.1016/j.jallcom.2023.169791 ↗
13. Q. Chao, P.D. Hodgson, H. Beladi, Ultrafine grain formation in a Ti-6Al-4V alloy by thermomechanical processing of a martensitic microstructure. Metall. Mater. Trans. A 45, 2659–2671 (2014)10.1007/s11661-014-2205-5 ↗
14. N. Bozzolo, N. Dewobroto, H.R. Wenk, F. Wagner, Microstructure and microtexture of highly cold-rolled commercially pure titanium. J. Mater. Sci. 42, 2405–2416 (2007)10.1007/s10853-006-1302-2 ↗
15. Y.J. Chen, Y.J. Li, J.C. Walmsley, S. Dumoulin, H.J. Roven, Deformation structures of pure titanium during shear deformation. Metall. Mater. Trans. A 41(4), 787–794 (2010)10.1007/s11661-009-0040-x ↗
16. G.S. Dyakonov, S. Mironov, N. Enikeev, I.P. Semenova, I.P. Semenova, R.Z. Valiev, S.L. Semiatin, Annealing behavior of severely deformed titanium grade 4. Mater. Sci. Eng. A 742, 89–101 (2019)10.1016/j.msea.2018.10.122 ↗
17. S. Sandlöbes, S. Korte-Kerzel, D. Raabe, On the influence of the heat treatment on microstructure formation and mechanical properties of near-α Ti–Fe alloys. Mater. Sci. Eng. A 748, 301–312 (2019)10.1016/j.msea.2018.12.071 ↗
18. N. Liu, Y. Wang, W.J. He, J. Li, A. Chapuis, B.F. Luan, Q. Liu, Microstructure and textural evolution during cold rolling and annealing of commercially pure titanium sheet. Trans. Nonferrous Met. Soc. China 28, 1123–1131 (2018)10.1016/S1003-6326(18)64748-X ↗
19. AJCPM. de Oliveira, A.B. Sakai, I.G. Oliveira, S.C. Souza, R.O. Correia, A.C. de Jesus, D.B. Santos. Efeito da laminação a frio e recozimento na microestrutura do titânio comercialmente puro de grau II contendo martensita-α′ 22º. ENEMET - ABM WEEK SP. 91–104 (2024)10.5151/2594-4711-40651 ↗
20. D.K. Yang, P. Cizek, P.D. Hodgson, C.E. Wen, Microstructure evolution and nanograin formation during shear localization in cold-rolled titanium. Acta Mater. 58, 4536–4548 (2010)10.1016/j.actamat.2010.05.007 ↗
21. Y. Gu, A. Ma, J. Jiang, H. Li, D. Song, H. Wu, Y. Yuan, Simultaneously improving mechanical properties and corrosion resistance of pure Ti by continuous ECAP plus short-duration annealing. Mater Charact 138, 38–47 (2018)10.1016/j.matchar.2018.01.050 ↗
22. J.C. Williams, R. Taggart, D.H. Polonis, The morphology and substructure of Ti-Cu martensite. Metall. Trans. 1, 2265–2270 (1970)10.1007/BF02643444 ↗
23. Z. Nishiyama, M. Oka, H. Nakagawa, The electron microscopic structure and lattice defects of the martensite in commercially pure titanium. Trans JIM 7, 168–173 (1996)10.2320/matertrans1960.7.168 ↗
24. S.K. Kim, J.K. Park, In-Situ measurement of continuous cooling β→α transformation behavior of CP-Ti. Metall. Mater. Trans. A 33(40), 1051–1056 (2002)10.1007/s11661-002-0206-2 ↗
25. T. Ahmed, H.J. Rack, Phase transformations during cooling in α+β titanium alloys. Mater. Sci. Eng. A 243, 206–211 (1988)10.1016/S0921-5093(97)00802-2 ↗
26. S. Zhao, Y. Wang, L. Peng, Y. Zhang, R. Ran, G. Yuan, Effect of annealing temperature on microstructure and mechanical properties of cold-rolled commercially pure titanium sheets. Trans. Nonferrous Met. Soc. China 32(8), 2587–2597 (2022)10.1016/S1003-6326(22)65968-5 ↗
27. B. Zhu, X. Wu, M. Wan, X. Cui, H. Li, X. Li et al., Effect of cold deformation on microstructure and mechanical behavior of commercially pure grade 4 titanium strip. Metals 12, 1166 (2022)10.3390/met12071166 ↗
28. G.E. Dieter, Mechanical metallurgy (McGraw-Hill Book Company, London, 1988), pp.337–346
29. S.N. Monteiro, R.E. Heed-Hill, An empirical analysis of titanium stress-strain curve. Met. Trans. 4, 1011–1015 (1973)10.1007/BF02645603 ↗
30. Z. Fan, H. Ming-zhi, S. De-ke, The relationship between the strain-hardening exponent n and the microstructure of metals. Mater. Sci. Eng. A 122(2), 211–213 (1989)10.1016/0921-5093(89)90632-1 ↗
31. U.F. Kocks, H. Mecking, Physics and phenomenology of strain hardening: the FCC case. Prog. Mater. Sci. 48, 171–273 (2003)10.1016/S0079-6425(02)00003-8 ↗
32. E.V. Legostaeva, A.Y. Eroshenko, I.A. Glukhov, Y.P. Sharkeev, O.A. Belyavskaya, A.Y. Zhilyakov et al., Ultrafine-grained microstructure and thermal properties of titanium at different stages of plastic deformation. Russ. Phys. J. 64(10), 1941–1948 (2022)10.1007/s11182-022-02545-0 ↗
33. H. Becker, W. Pantleon, Work-hardening stages and deformation mechanism maps during tensile deformation of commercially pure titanium. Comput. Mater. Sci. 76, 52–59 (2013)10.1016/j.commatsci.2013.03.028 ↗
34. D. Kang, K. Lee, E. Kwon, T. Tsuchiyama, S. Takaki, Variation of work hardening rate by oxygen contents in pure titanium alloy. Mater. Sci. Eng. A 632, 120–126 (2015)10.1016/j.msea.2015.02.074 ↗
35. Y.G. Ko, D.H. Shin, K.-T. Park, C.S. Lee, An analysis of the strain hardening behavior of ultra-fine grain pure titanium. Scripta Mater. 54, 1785–1789 (2006)10.1016/j.scriptamat.2006.01.034 ↗
36. K. Ahn, H. Huh, J. Yoon, Strain hardening model of pure titanium considering effects of deformation twinning. Met. Mater. Int. 19(4), 749–758 (2013)10.1007/s12540-013-4014-6 ↗
37. Z. Li, L. Fu, B. Fu, A. Shan, Yield point elongation in fine-grained titanium. Mater. Lett. 96, 1–4 (2013)10.1016/j.matlet.2012.12.115 ↗
38. X. Shi, Z. Cao, Z. Fan, R. Guo, J. Qiao, Probing into the yield plateau phenomenon in commercially pure titanium during tensile tests. Acta Metall. Sinica 34, 701–709 (2021)10.1007/s40195-020-01165-2 ↗
39. L.J. Wu, K.Y. Luo, Y. Liu, C.Y. Cui, W. Xue, J.Z. Lu, Effects of laser shock peening on the micro-hardness, tensile properties, and fracture morphologies of CP-Ti alloy at different temperatures. Appl. Surf. Sci. 431, 122–134 (2018)10.1016/j.apsusc.2017.05.202 ↗
40. S.W. Choi, C.L. Li, J.W. Won, J.T. Yeom, Y.S. Choi, J.K. Hong, Deformation heterogeneity and its effect on recrystallization behavior in commercially pure titanium: comparative study on initial microstructures. Mater. Sci. Eng. A 764, 138211 (2019)10.1016/j.msea.2019.138211 ↗
41. M. Klinger, A. Jäger, Crystallographic tool box (CrysTBox): automated tools for transmission electron microscopists and crystallographers. J. Appl. Cryst. 48, 2012–2018 (2015)10.1107/S1600576715017252 ↗