journal article·2021-09-28

Additive manufacturing of NiZnCu-ferrite soft magnetic composites

Caleb E. Andrews, Megan P. Chatham, Samantha F. Dorman, Ian D. McCue, Joseph J. Sopcisak, Mitra L. Taheri

Journal of Materials Research· Volume 36· Issue 18
Publisher page

Abstract

Soft magnetic composites (SMCs) are a class of magnetic materials that have the potential to create lighter and more efficient electronic devices. SMCs provide high electrical resistivity while providing high magnetic permeability, consisting of a magnetically conductive core and an insulating coating traditionally made via powder metallurgy. Until recent advances, devices needing materials with these magnetic properties have been made by complex and geometrically limited laminations or press and sinter methods; both possessing issues. This paper establishes that a multi-material system incorporating NiZnCu-ferrite and high purity iron processed via additive manufacturing (AM) can serve as a manufacturing route for SMCs, with as-built samples showing high maximum relative permeability (~ 200,000). The results demonstrate the viability of laser powder bed fusion (L-PBF) AM to produce SMCs with higher permeability than press and sinter SMCs utilizing the same powder system and chemistry while also indicating new challenges that must be overcome to produce a fully dense SMC via additive manufacturing.
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Research context

OpenAlex topics: Additive Manufacturing Materials and Processes · Additive Manufacturing and 3D Printing Technologies · Metallic Glasses and Amorphous Alloys

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (53)

Show source-provided references
1. L. Ferraris, New Soft Magnetic Composites for electromagnetic applications with improved mechanical properties, 056209 (2018). https://doi.org/10.1063/1.494341310.1063/1.4943413 ↗
2. L. Gelinas, C; Pelletier, S; Lemieux, P; Azzi, PROPERTIES AND PROCESSING OF IMPROVED SMC MATERIALS, in: Proc. 2005 Int. Conf. Powder Metall. Part. Mater., 2005.
3. J.A. Bas, J.A. Calero, M.J. Dougan, Sintered soft magnetic materials. Properties and applications, J. Magn. Magn. Mater. 254 (2003) 391–398. https://doi.org/10.1016/S0304-8853(02)00934-410.1016/S0304-8853(02)00934-4 ↗
4. AK Steel, DI-MAX HF-10X COLD ROLLED FULLY PROCESSED Non-Oriented Electrical Steel Material, (n.d.) 0–3.
5. C. Magnussen, F; Svechkarenko, D; Thelin, P; Sadaragani, Analysis of a PM Machine with Soft Magnetic Composites Core, in: KTH Royal Institute of Technology, 2004
6. H.B. Bayramli, E; Olgelioglu, O; Ertan, Powder metal development forelectrical motor applications. J. Mater. Process. Technol. 161, 83–88 (2005)10.1016/j.jmatprotec.2004.07.070 ↗
7. A. Hamler, A; Gorican, V; Sustarsic, B; Sirc, The use of soft magneticcomposite materials in synchronous electric motor, J. Magn. Magn. Mater. 304 (2006)10.1016/j.jmmm.2006.03.003 ↗
8. G.A.V. Sowter, Soft Magnetic Materials for Audio Transformers: History, Production, and Applications. J. Audio Eng. Soc. 35, 760–777 (1987)
9. K.J. Sunday, M.L. Taheri, Soft magnetic composites: recent advancements in the technology. Met. Powder Rep. 72, 425–429 (2017). https://doi.org/10.1016/j.mprp.2016.08.00310.1016/j.mprp.2016.08.003 ↗
10. H. Shokrollahi, K. Janghorban, Soft magnetic composite materials (SMCs). J. Mater. Process. Technol. 189, 1–12 (2007). https://doi.org/10.1016/j.jmatprotec.2007.02.03410.1016/j.jmatprotec.2007.02.034 ↗
11. M. Persson, G. Nord, A.G. Jack, Soft Magnetic Iron Powder Materials AC Properties and their Application in Electrical Machines. Euro PM 2003, 1–7 (2003)
12. K.J. Sunday, F.G. Hanejko, M.L. Taheri, Magnetic and microstructural properties of Fe3O4-coated Fe powder soft magnetic composites. J. Magn. Magn. Mater. 423, 164–170 (2017). https://doi.org/10.1016/j.jmmm.2016.09.02410.1016/j.jmmm.2016.09.024 ↗
13. S. Wu, A. Sun, F. Zhai, J. Wang, Q. Zhang, W. Xu, P. Logan, A.A. Volinsky, Journal of Magnetism and Magnetic Materials Annealing effects on magnetic properties of silicone-coated iron-based soft magnetic composites. J. Magn. Magn. Mater. 324, 818–822 (2012). https://doi.org/10.1016/j.jmmm.2011.09.02610.1016/j.jmmm.2011.09.026 ↗
14. A.H. Taghvaei, H. Shokrollahi, K. Janghorban, Structural studies, magnetic properties and loss separation in iron – phenolicsilane soft magnetic composites. Mater. Des. 31, 142–148 (2010). https://doi.org/10.1016/j.matdes.2009.06.04410.1016/j.matdes.2009.06.044 ↗
15. J. Li, X. Peng, Y. Yang, H. Ge, Preparation and characterization of MnZn / FeSiAl soft magnetic composites. J. Magn. Magn. Mater. 426, 132–136 (2017). https://doi.org/10.1016/j.jmmm.2016.11.06810.1016/j.jmmm.2016.11.068 ↗
16. J. Azadmanjiri, Preparation of Mn – Zn ferrite nanoparticles from chemical sol – gel combustion method and the magnetic properties after sintering, 353 (2007) 4170–4173. https://doi.org/10.1016/j.jnoncrysol.2007.06.046.10.1016/j.jnoncrysol.2007.06.046 ↗
17. S. Wu, A. Sun, W. Xu, Q. Zhang, F. Zhai, P. Logan, A.A. Volinsky, Iron-based soft magnetic composites with Mn – Zn ferrite nanoparticles coating obtained by sol – gel method. J. Magn. Magn. Mater. 324, 3899–3905 (2012). https://doi.org/10.1016/j.jmmm.2012.06.04210.1016/j.jmmm.2012.06.042 ↗
18. Y. Peng, Y. Yi, L. Li, H. Ai, X. Wang, L. Chen, Fe-based soft magnetic composites coated with NiZn ferrite prepared by a co-precipitation method 428, 148–153 (2017). https://doi.org/10.1016/j.jmmm.2016.12.02410.1016/j.jmmm.2016.12.024 ↗
19. M.C. Dimri, A. Verma, S.C. Kashyap, D.C. Dube, O.P. Thakur, C. Prakash, Structural , dielectric and magnetic properties of NiCuZn ferrite grown by citrate precursor method, 133 (2006) 42–48. https://doi.org/10.1016/j.mseb.2006.04.04310.1016/j.mseb.2006.04.043 ↗
20. K.J. Sunday, M.L. Taheri, NiZnCu-ferrite coated iron powder for soft magnetic composite applications. J. Magn. Magn. Mater. 463, 1–6 (2018). https://doi.org/10.1016/j.jmmm.2018.05.03010.1016/j.jmmm.2018.05.030 ↗
21. M. Yaghtin, A.H. Taghvaei, B. Hashemi, K. Janghorban, Effect of heat treatment on magnetic properties of iron-based soft magnetic composites with Al 2 O 3 insulation coating produced by sol – gel method. J. Alloys Compd. 581, 293–297 (2013). https://doi.org/10.1016/j.jallcom.2013.07.00810.1016/j.jallcom.2013.07.008 ↗
22. N. Kang, M. El Mansori, F. Guittonneau, H. Liao, Y. Fu, E. Aubry, Controllable mesostructure, magnetic properties of soft magnetic Fe-Ni-Si by using selective laser melting from nickel coated high silicon steel powder. Appl. Surf. Sci. 455, 736–741 (2018). https://doi.org/10.1016/j.apsusc.2018.06.04510.1016/j.apsusc.2018.06.045 ↗
23. N.C. Benack, T. Wang, K. Matthews, M.L. Taheri, Additive Manufacturing Methods for Soft Magnetic Composites (SMCs). Microsc. Microanal. 24, 1066–1067 (2018). https://doi.org/10.1017/s143192761800581010.1017/s1431927618005810 ↗
24. A. Plotkowski, J. Pries, F. List, P. Nandwana, B. Stump, K. Carver, R.R. Deho, In fl uence of scan pattern and geometry on the microstructure and soft- magnetic performance of additively manufactured Fe-Si, 29 (2019). https://doi.org/10.1016/j.addma.2019.10078110.1016/j.addma.2019.100781 ↗
25. T. Tiismus, Hans; Kallaste, Ants; Rassolkin, Anton; Vaimann, Preliminary Analysis of Soft Magnetic Material Properties for Additive Manufacturing of Electrical Machines. Key Eng. Mater. 799, 270–275 (2019)10.4028/www.scientific.net/KEM.799.270 ↗
26. C. Gerada, R. Hague, Free-Form Design of Electrical Machine Rotor Cores for Production Using Additive Manufacturing 141, 1–13 (2019). https://doi.org/10.1115/1.404262110.1115/1.4042621 ↗
27. H. Tiismus, S. Member, A. Kallaste, M. Ieee, T. Vaimann, M. Ieee, Technologies for Additive Manufacturing of Electrical Machines, (2019) 651–65510.1109/DEMPED.2019.8864850 ↗
28. T.F. Babuska, M.A. Wilson, K.L. Johnson, S.R. Whetten, J.F. Curry, J.M. Rodelas, C. Atkinson, P. Lu, M. Chandross, B.A. Krick, J.R. Michael, N. Argibay, D.F. Susan, A.B. Kustas, Achieving high strength and ductility in traditionally brittle soft magnetic intermetallics via additive manufacturing. Acta Mater. 180, 149–157 (2019). https://doi.org/10.1016/j.actamat.2019.08.04410.1016/j.actamat.2019.08.044 ↗
29. D. Goll, D. Schuller, G. Martinek, T. Kunert, J. Schurr, C. Sinz, T. Schubert, T. Bernthaler, H. Riegel, G. Schneider, Additive manufacturing of soft magnetic materials and components. Addit. Manuf. 27, 428–439 (2019). https://doi.org/10.1016/j.addma.2019.02.02110.1016/j.addma.2019.02.021 ↗
30. M. Garibaldi, I. Ashcroft, J.N. Lemke, M. Simonelli, R. Hague, Effect of annealing on the microstructure and magnetic properties of soft magnetic Fe-Si produced via laser additive manufacturing. Scr. Mater. 142, 121–125 (2018). https://doi.org/10.1016/j.scriptamat.2017.08.04210.1016/j.scriptamat.2017.08.042 ↗
31. H. Schönrath, M. Spasova, S.O. Kilian, R. Meckenstock, G. Witt, J.T. Sehrt, M. Farle, Additive manufacturing of soft magnetic permalloy from Fe and Ni powders : Control of magnetic anisotropy. J. Magn. Magn. Mater. 478, 274–278 (2019). https://doi.org/10.1016/j.jmmm.2018.11.08410.1016/j.jmmm.2018.11.084 ↗
32. S. Sundaram, M. Skouras, D.S. Kim, L. Van Den Heuvel, W. Matusik, Topology optimization and 3D printing of multimaterial magnetic actuators and displays, Sci. Adv. (2019) 1–15.10.1126/sciadv.aaw1160 ↗
33. Z. Ji, C. Yan, B. Yu, X. Wang, F. Zhou, Multimaterials 3D Printing for Free Assembly Manufacturing of Magnetic Driving Soft Actuator. Adv. Mater. Interfaces. 4, 1–6 (2017). https://doi.org/10.1002/admi.20170062910.1002/admi.201700629 ↗
34. L. Li, K. Jones, B. Sales, J.L. Pries, I.C. Nlebedim, K. Jin, H. Bei, B.K. Post, M.S. Kesler, O. Rios, V. Kunc, R. Fredette, J. Ormerod, A. Williams, T.A. Lograsso, M.P. Paranthaman, Fabrication of highly dense isotropic Nd-Fe-B nylon bonded magnets via extrusion-based additive manufacturing. Addit. Manuf. 21, 495–500 (2018). https://doi.org/10.1016/j.addma.2018.04.00110.1016/j.addma.2018.04.001 ↗
35. L. Li, A. Tirado, I.C. Nlebedim, O. Rios, B. Post, V. Kunc, R.R. Lowden, E. Lara-curzio, R. Fredette, J. Ormerod, T.A. Lograsso, M.P. Paranthaman, Big Area Additive Manufacturing of High Performance Bonded NdFeB Magnets, Nat. Publ. Gr. (2016) 1–7. https://doi.org/10.1038/srep3621210.1038/srep36212 ↗
36. E.B. Joyee, Y. Pan, Multi-material additive manufacturing of functional soft robot. Procedia Manuf. 34, 566–573 (2019). https://doi.org/10.1016/j.promfg.2019.06.22110.1016/j.promfg.2019.06.221 ↗
37. E.B. Joyee, Y. Pan, A fully three-dimensional printed inchworm-inspired soft robot with magnetic actuation. Soft Robot. 6, 333–345 (2019). https://doi.org/10.1089/soro.2018.008210.1089/soro.2018.0082 ↗
38. W. Pantleon, Resolving the geometrically necessary dislocation content by conventional electron backscattering diffraction. Scr. Mater. 58, 994–997 (2008). https://doi.org/10.1016/j.scriptamat.2008.01.05010.1016/j.scriptamat.2008.01.050 ↗
39. GNK Hoeganaes, Ancorsteel© 1000/1000B/1000C, (n.d.) 1–5.
40. N.A. Castro, F.J.G. Landgraf, Porosity and Magnetic Losses in Soft Magnetic Composites, Proc. 16 - Soft Magn. Mater. Conf. (2003) 767–772
41. Y. Yan, K.D.T. Ngo, D. Hou, M. Mu, Y. Mei, G.Q. Lu, Effect of Sintering Temperature on Magnetic Core-Loss Properties of a NiCuZn Ferrite for High-Frequency Power Converters. J. Electron. Mater. 44, 3788–3794 (2015). https://doi.org/10.1007/s11664-015-3836-z10.1007/s11664-015-3836-z ↗
42. T. Kamiyama, Y. Minonishi, T. Shinohara, H. Yamamoto, Dislocations and their relation to the magnetic properties of Pd2MnSn Heusler alloy, Philos. Mag. A. 52 (1985) 43–47. https://doi.org/10.1080/0141861850824213410.1080/01418618508242134 ↗
43. M. Sablik, Modeling the effect of grain size and dislocation density on hysteretic magnetic properties in steels. J. Appl. Phys. 89, 5610–5613 (2001)10.1063/1.1359167 ↗
44. R. Ranhan, O. Buck, R.B. Thompson, A study on the effect of dislocation on the magnetic properties of nickel using magnetic NDE methods, J. Appl. Phys. 61 (1987). https://doi.org/10.1063/1.33889910.1063/1.338899 ↗
45. K. Eloot, A. De Paepe, J. Dilewijns, C. Standaert, Relation between magnetic properties and changes in dislocation and cell structure due to cold deformation, J. Magn. Magn. Mater. 157–158 (1996) 459–460. https://doi.org/10.1016/0304-8853(95)01061-010.1016/0304-8853(95)01061-0 ↗
46. K.A. Small, M.L. Taheri, Role of processing in microstructural evolution in inconel 625: a comparison of three additive manufacturing techniques. Metall. Mater. Trans. A. 52, 2811–2820 (2021)10.1007/s11661-021-06273-x ↗
47. Y. Liu, Y. Yang, D. Wang, A study on the residual stress during selective laser melting (SLM) of metallic powder. Int. J. Adv. Manuf. Technol. (2016). https://doi.org/10.1007/s00170-016-8466-y10.1007/s00170-016-8466-y ↗
48. K.A. Small, Z. Clayburn, R. DeMott, S. Primig, D. Fullwood, M.L. Taheri, Interplay of dislocation substructures and elastic strain evolution in an additively manufactured nickel superalloy, Mat. Sci. Eng. A. (2020)10.1016/j.msea.2020.139380 ↗
49. M. Bayat, A. Thanki, S. Mohanty, A. Witvrouw, S. Yang, J. Thorborg, N.S. Tiedje, J.H. Hattel, Keyhole-induced porosities in Laser-based Powder Bed Fusion (L-PBF) of Ti6Al4V: High-fidelity modelling and experimental validation, Addit. Manuf. 30 (2019)10.1016/j.addma.2019.100835 ↗
50. Y. Lee, W. Zhang, Modeling of heat transfer, fluid flow and solidification microstructure of nickel-base superalloy fabricated by laser powder bed fusio. Addit. Manuf. 12, 178–188 (2019)
51. Y.-C. Wu, C.-H. San, C.-H. Chang, H.-J. Lin, R. Marwan, S. Baba, W.-S. Hwang, Numerical modeling of melt-pool behavior in selective laser melting with random powder distribution and experimental validation. J. Mater. Process. Technol. 254, 72–78 (2018)10.1016/j.jmatprotec.2017.11.032 ↗
52. S.A. Khairallah, A.T. Anderson, A. Rubenchik, W.E. King, Laser powder-bed fusion additive manufacturing: Physics of complex melt flow and formation mechanisms of pores, spatter, and denudation zones. Acta Mater. 108, 36–45 (2016)10.1016/j.actamat.2016.02.014 ↗
53. W.E. King, H.D. Barth, V.M. Castillo, G.F. Gallegos, J.W. Gibbs, D.E. Hahn, C. Kamath, A.M. Rubenchik, Observation of keyhole-mode laser melting in laser powder-bed fusion additive manufacturing. J. Mater. Process. Technol. 214, 2915–2925 (2014)10.1016/j.jmatprotec.2014.06.005 ↗