Occurrence of plastic instabilities in dynamic microhardness testing

Plastic instabilities were observed to appear during dynamic ultramicrohardness testing of a solid solution Al–3.3 wt.% Mg alloy. The tests were carried out at room temperature with a Vickers hardness indenter in a computer-controlled dynamic ultramicrohardness testing machine. During the tests the applied load was increased from 0 to 2000 mN at constant loading rate. The instabilities appear as characteristic steps in the continuously recorded load-indentation depth curves. The physical basis for the occurrence of the instabilities is the interaction between moving dislocations and solute atoms, a phenomenon termed in the literature as serrated yielding, jerky flow, or Portevin-Le Châtelier effect. The instabilities start at a critical load, F_c, in the depth-load curve. Varying the loading rate, μ, by two orders of magnitude F_c was found to increase linearly with the loading rate.