journal article·2005-09Open access

Assessment of Geometrical and Transport Properties of a Fibrous C/C Composite Preform Using x-ray Computerized Micro-tomography: Part I. Image Acquisition and Geometrical Properties

Olivia Coindreau, Gérard L. Vignoles

Journal of Materials Research· Volume 20· Issue 9

Abstract

Raw and partially infiltrated carbon–carbon composite preforms have been scanned by high-resolution synchrotron radiation x-ray computerized micro-tomography. Three dimensional high-quality images of the pore space have been produced at two distinct resolutions and have been used for the computation of geometrical quantities: porosity, internal surface area, pore sizes, and their distributions, as well as local and average fiber directions. Determination of the latter property makes use of an original algorithm. All quantities have been compared to experimental data with good results. Structural models appropriate for ideal families of cylinders are shown to represent adequately the actual pore space.
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Research context

OpenAlex topics: Composite Material Mechanics · Advanced ceramic materials synthesis · Thermal properties of materials

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (49)

Show source-provided references
1. 10.1080/0098644860891169810.1080/00986448608911698 ↗
2. 10.1109/34.911410.1109/34.9114 ↗
3. Characterization of internal damage in an MMCp using x-ray synchrotron phase contrast microtomography.10.1016/S1359-6454(99)00024-5 ↗
4. Baruchel · 2000
5. 10.1111/j.1365-246X.1991.tb06730.x10.1111/j.1365-246X.1991.tb06730.x ↗
6. 10.1002/aic.69038010610.1002/aic.690380106 ↗
7. 10.1016/0020-7225(86)90097-210.1016/0020-7225(86)90097-2 ↗
8. 10.1088/0305-4470/23/9/00810.1088/0305-4470/23/9/008 ↗
9. 10.1149/1.183693310.1149/1.1836933 ↗
10. 10.1023/A:101525151833310.1023/A:1015251518333 ↗
11. 5 Reuge N. and Vignoles G.L. : Global modelling of I-CVI: Effects of reactor control parameters on a densification. J. Mater. Proc. Technol. (2004, in press).
12. Starr · 1988 · 243
13. 10.1016/0009-2509(89)85189-910.1016/0009-2509(89)85189-9 ↗
14. 10.1063/1.47135610.1063/1.471356 ↗
15. 10.1002/aic.69037080710.1002/aic.690370807 ↗
16. 10.1063/1.33778610.1063/1.337786 ↗
17. 10.1145/37401.3742210.1145/37401.37422 ↗
18. Kak · Classics in Applied Math. · 2001 · 33
19. Jonard · 2001
20. 48 Satterfield C.N. Mass transfer in heterogenous catalysis, Technical Report MA-41 (MIT Press, Cambridge, MA, 1970).
21. 10.1063/1.33907410.1063/1.339074 ↗
22. 10.1126/science.260.5109.78910.1126/science.260.5109.789 ↗
23. 35 Baruchel J. and Härtwig J. : ID 19 Topography and High-Resolution Diffraction Handbook. http://www.esrf.fr/exp facilities/ID19/handbook/handbook.html (2004).
24. Vignoles · 2000 · 10 · Pr2-9
25. 10.1063/1.46460410.1063/1.464604 ↗
26. Starr · 1992 · 250 · 207
27. 10.1016/0301-9322(82)90029-510.1016/0301-9322(82)90029-5 ↗
28. 10.1109/34.8566810.1109/34.85668 ↗
29. Baruchel · 1995 · 115
30. X-ray microtomography of ceramic and metal matrix composites.
31. 10.1063/1.44896610.1063/1.448966 ↗
32. 10.1002/aic.69037010710.1002/aic.690370107 ↗
33. 10.1098/rspa.1979.016010.1098/rspa.1979.0160 ↗
34. 10.1016/S0165-1684(03)00064-110.1016/S0165-1684(03)00064-1 ↗
35. 10.1063/1.32938610.1063/1.329386 ↗
36. Kim · 1997 · 18 · 287
37. Fundamental and practical aspects of the chemical vapor infiltration of porous substrates.
38. Modelling binary, Knudsen, and transition regime diffusion inside complex porous media.
39. FReLON camera: Fast readout low noise.
40. 10.1016/0021-9797(85)90246-210.1016/0021-9797(85)90246-2 ↗
41. 10.1016/S0008-6223(00)00103-210.1016/S0008-6223(00)00103-2 ↗
42. 10.1002/aic.69039030410.1002/aic.690390304 ↗
43. 10.1063/1.34627610.1063/1.346276 ↗
44. 10.1063/1.43744010.1063/1.437440 ↗
45. And · 1972 · 63
46. 10.1002/aic.69039071110.1002/aic.690390711 ↗
47. 10.1063/1.36437410.1063/1.364374 ↗
48. 10.1002/aic.69035120510.1002/aic.690351205 ↗
49. 10.1557/JMR.1998.017210.1557/JMR.1998.0172 ↗