journal article·1999-11

A solvothermal decomposition process for fabrication and particle sizes control of Bi2S3 nanowires

Shu-Hong Yu, Lei Shu, Jian Yang, Zhao-Hui Han, Yi-Tai Qian, Yu-Heng Zhang

Journal of Materials Research· Volume 14· Issue 11
Publisher page

Abstract

A novel one-step solvothermal decomposition process (SDP) was successfully developed for fabrication of Bi2S3 nanowires via a reaction between BiCl3 and thiourea in polar solvents at 140 °C for 6–12 h. The influence of solvents, reaction temperature, and reaction time on the formation of Bi2S3 nanowires was investigated. The yield was as high as 98%. The particle sizes of Bi2S3 nanowires are controlled by the choice of solvents. The possible formation mechanism of Bi2S3 nanowires via the so-called SDP method is proposed. The present technique is expected to synthesize other nanostructural metal chalcogenides under mild conditions.
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Research context

OpenAlex topics: Chalcogenide Semiconductor Thin Films · Quantum Dots Synthesis And Properties · Advanced Thermoelectric Materials and Devices

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