journal article·2019-07

Deformation Behavior and Microstructure Evolution of Powder Metallurgy Ti6Al4V Alloy During Hot Compression

Ronge Liu, Baoyu Wang, Junling Li, Weiping Ma, Shushan Hu

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Abstract

In order to determine appropriate workability parameters for cross-wedge rolling products of powder metallurgy (PM) Ti6Al4V alloys, thermal compression experiments were carried out within the temperature range of 850-1050 °C, the strain rate range of 0.1-10 s−1, and with a height decrease of 60%. The compression deformation behavior was investigated. A strain-compensated constitutive model was established based on the flow stress curves corrected by the friction, which can predict the flow behaviors under the entirety of the experimental deformation conditions. Moreover, the processing map was developed, and stable and unstable deformation regimes were established. The microstructure analysis illustrated that globularization and dynamic recrystallization were the main deformation mechanisms. The porosity of the compressed samples was greatly reduced and influenced by the temperature and strain rate. Considering the material flow stress, hot processing map, microstructure and porosity, the appropriate hot deformation parameters for PM Ti6Al4V alloy preforms are suggested.
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Titanium Alloys Microstructure and Properties · Metallurgy and Material Forming · Advanced materials and composites

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References (49)

Show source-provided references
1. C.X. Cui, B.M. Hu, L.C. Zhao, and S.J. Liu, Titanium Alloy Production Technology, Market Prospects and Industry Development, Mater. Des., 2011, 32(3), p 1684–1691 (in English)10.1016/j.matdes.2010.09.011 ↗
2. F.H. Froes and D. Eylon, Powder Metallurgy of Titanium Alloys, Metall. Rev., 2013, 35(1), p 162–184 (in English)10.1179/095066090790323984 ↗
3. W. Chen, Y. Yamamoto, W.H. Peter, M.B. Clark, S.D. Nunn, J.O. Kiggans, T.R. Muth, C.A. Blue, J.C. Williams, and K. Akhtar, The Investigation of Die-Pressing and Sintering Behavior of ITP CP-Ti and Ti-6Al-4V Powders, J. Alloys Compd., 2012, 541, p 440–447 (in English)10.1016/j.jallcom.2012.06.131 ↗
4. Y. Kim, Y.B. Song, S.H. Lee, and Y.S. Kwon, Characterization of the Hot Deformation Behavior and Microstructural Evolution of Ti-6Al-4V Sintered Preforms Using Materials Modeling Techniques, J. Alloys Compd., 2016, 676, p 15–25 (in English)10.1016/j.jallcom.2016.03.146 ↗
5. Y. Kim, E.P. Kim, Y.B. Song, S.H. Lee, and Y.S. Kwon, Microstructure and Mechanical Properties of Hot Isostatically Pressed Ti-6Al-4V Alloy, J. Alloys Compd., 2014, 603, p 207–212 (in English)10.1016/j.jallcom.2014.03.022 ↗
6. J.W. Qiu, Y. Liu, Y.B. Liu, B. Liu, B. Wang, E. Ryba, and H.P. Tang, Microstructures and Mechanical Properties of Titanium Alloy Connecting Rod Made By Powder Forging Process, Mater. Des., 2012, 33, p 213–219 (in English)10.1016/j.matdes.2011.07.034 ↗
7. Y.J. Feng, W.C. Zhang, G.R. Cui, J.P. Wu, and W.Z. Chen, Effects of the Extrusion Temperature on the Microstructure and Mechanical Properties of TiBw/Ti6Al4V Composites Fabricated by Pre-sintering and Canned Extrusion, J. Alloys Compd., 2017, 721, p 383–391 (in English)10.1016/j.jallcom.2017.05.309 ↗
8. V.V. Joshi, C. Lavender, V. Moxson, V. Duz, E. Nyberg, and K.S. Weil, Development of Ti-6Al-4V and Ti-1Al-8V-5Fe Alloys Using Low-Cost TiH2 Powder Feedstock, JMEPEG, 2013, 22(4), p 995–1003 (in English)10.1007/s11665-012-0386-x ↗
9. L. Bolzoni, P.G. Esteban, E.M. Ruiz-Navas, and E. Gordo, Influence of Powder Characteristics on Sintering Behaviour and Properties of PM Ti Alloys Produced from Prealloyed Powder and Master Alloy, Powder Metall., 2011, 54(4), p 543–550 (in English)10.1179/003258910X12827272082623 ↗
10. C. Liang, M.X. Ma, M.T. Jia, S. Raynova, J.Q. Yan, and D.L. Zhang, Microstructures and Tensile Mechanical Properties of Ti-6Al-4V Bar/Disk Fabricated by Powder Compact Extrusion/Forging, Mater. Sci. Eng. A, 2014, 619, p 290–299 (in English)10.1016/j.msea.2014.09.083 ↗
11. F. Yang, D.L. Zhang, B. Gabbitas, H.Y. Lu, and C.F. Wang, Microstructural Evolution During Extrusion of a Ti/Al/Al35V65 (Ti-6Al-4V) Powder Compact and the Mechanical Properties of the Extruded Rod, Mater. Sci. Eng. A, 2014, 598, p 360–367 (in English)10.1016/j.msea.2014.01.055 ↗
12. H.C. Ji, J.P. Liu, B.Y. Wang, Z.H. Zheng, J.H. Huang, and Z.H. Hu, Cross-Wedge Rolling of a 4Cr9Si2 Hollow Valve: Explorative Experiment and Finite Element Simulation, Int. J. Adv. Manuf. Technol., 2015, 77(1-4), p 15–26 (in English)10.1007/s00170-014-6363-9 ↗
13. Z. Pater, T. Bulzak, and J. Tomczak, Cross-Wedge Rolling of Driving Shaft from Titanium Alloy Ti6Al4V, Key Eng. Mater., 2016, 687(8), p 125–132 (in English)10.4028/www.scientific.net/KEM.687.125 ↗
14. A. Tofil, J. Tomczak, and T. Bulzak, Comparative Analysis of Forging Rolling and Cross-Wedge Rolling of Forgings from Titanium Alloy Ti6Al4V, Key Eng. Mater., 2016, 687(8), p 141–148 (in English)10.4028/www.scientific.net/KEM.687.141 ↗
15. J.L. Li, B.Y. Wang, H.C. Ji, J. Zhou, X.B. Fu, and X. Huang, Numerical and Experimental Investigation on the Cross-Wedge Rolling of Powder Sintering TC4 Alloy, Int. J. Adv. Manuf. Technol., 2018, 94(5-8), p 2149–2162 (in English)10.1007/s00170-017-0992-8 ↗
16. Y.V.R.K. Prasad and T. Seshacharyulu, Modelling of Hot Deformation for Microstructural Control, Int. Mater. Rev., 1998, 43(6), p 243–258 (in English)10.1179/imr.1998.43.6.243 ↗
17. Y.H. Duan, L.S. Ma, H.R. Qi, R.Y. Li, and P. Li, Developed Constitutive Models, Processing Maps and Microstructural Evolution of Pb-Mg-10Al-0.5B Alloy, Mater. Charact., 2017, 129, p 353–366 (in English)10.1016/j.matchar.2017.05.026 ↗
18. R.Y. Li, Y.H. Duan, L.S. Ma, and S. Chen, Flow Behavior, Dynamic Recrystallization and Processing Map of Mg-20Pb-1.6Al-0.4B Alloy, J. Mater. Eng. Perform., 2017, 26(5), p 2439–2451 (in English)10.1007/s11665-017-2681-z ↗
19. Z.W. Yuan, F.G. Li, H.J. Qiao, M.L. Xiao, J. Cai, and J. Li, A Modified Constitutive Equation for Elevated Temperature Flow Behavior of Ti-6Al-4V Alloy Based on Double Multiple Nonlinear Regression, Mater. Sci. Eng. A, 2013, 578, p 260–270 (in English)10.1016/j.msea.2013.04.091 ↗
20. P.M. Souza, H. Beladi, R.P. Singh, P.D. Hodgson, and B. Rolfe, An Analysis on the Constitutive Models for Forging of Ti6Al4V Alloy Considering the Softening Behavior, JMEPEG, 2018, 27(7), p 3545–3558 (in English)10.1007/s11665-018-3402-y ↗
21. Y. Sun, L.X. Hu, and J.S. Ren, Modeling the Constitutive Relationship of Powder Metallurgy Ti-47Al-2Nb-2Cr Alloy During Hot Deformation, J. Mater. Eng. Perform., 2015, 24(3), p 1313–1321 (in English)10.1007/s11665-015-1397-1 ↗
22. A. Hajari, M. Morakabati, S.M. Abbasi, and H. Badri, Constitutive Modeling for High-Temperature Flow Behavior of Ti-6242S Alloy, Mater. Sci. Eng. A, 2017, 681, p 103–113 (in English)10.1016/j.msea.2016.11.002 ↗
23. Y.V.R.K. Prasad and T. Seshacharyulu, Modelling of Hot Deformation for Microstructural Control, Int. Metall. Rev., 1998, 43(6), p 243–258 (in English)10.1179/imr.1998.43.6.243 ↗
24. Y. Sun, Z.P. Wan, L.X. Hu, and J.S. Ren, Characterization of Hot Processing Parameters of Powder Metallurgy TiAl-Based Alloy Based on the Activation Energy Map and Processing Map, Mater. Des., 2015, 86, p 922–932 (in English)10.1016/j.matdes.2015.07.140 ↗
25. V.S. Sokolovsky, N.D. Stepanov, S.V. Zherebtsov, N.A. Nochovnaya, P.V. Panin, M.A. Zhilyakova, A.A. Popov, and G.A. Salishchev, Hot Deformation Behavior and Processing Maps of B and Gd Containing β-Solidified TiAl Based Alloy, Intermetallics, 2018, 94, p 138–151 (in English)10.1016/j.intermet.2018.01.004 ↗
26. K.P. Rao and Y.V.R.K. Prasad, Processing Map and Hot Working Mechanisms in a P/M TiAl Alloy Composite with In Situ Carbide and Silicide Dispersions, Mater. Sci. Eng. A, 2010, 527(24), p 6589–6595 (in English)10.1016/j.msea.2010.06.064 ↗
27. Y. Xue, Y. Du, Z.M. Zhang, Y.W. Huang, and L.F. Guo, Processing Map of Powder Metallurgy Al-W Alloys at Elevated Temperatures, JMEPEG, 2017, 26(7), p 3216–3225 (in English)10.1007/s11665-017-2750-3 ↗
28. Y.H. Duan, P. Li, L.S. Ma, and R.Y. Li, Dynamic Recrystallization and Processing Map of Pb-30 Mg-9Al-1B Alloy During Hot Compression, Metall. Mater. Trans. A, 2017, 48A, p 3419–3431 (in English)10.1007/s11661-017-4090-1 ↗
29. F.C. Ren, F. Chen, J. Chen, and X.Y. Tang, Hot Deformation Behavior and Processing Maps of AISI, 420 Martensitic Stainless Steel, JMP, 2018, 31, p 640–649 (in English)
30. L.J. Huang, Y.Z. Zhang, L. Geng, B. Wang, and W. Ren, Hot Compression Characteristics of TiBw/Ti6Al4V Composites with Novel Network Microstructure Using Processing Maps, Mater. Sci. Eng. A, 2013, 580, p 242–249 (in English)10.1016/j.msea.2013.05.039 ↗
31. B.Q. Guo, C. Aranas, Jr., B.H. Sun, X.K. Ji, and J.J. Jonas, Reverse Transformation Behavior of Ti-6Al-4V After Deformation in the Two-Phase Region, Metall. Mater. Trans. A, 2018, 49A, p 22–2710.1007/s11661-017-4403-4 ↗
32. B.Q. Guo, C. Aranas, Jr., A. Foul, X.K. Ji, A. Fall, M. Jahazi, and J.J. Jonas, Effect of Multipass Deformation at Elevated Temperatures on the Flow Behavior and Microstructural Evolution in Ti-6Al-4V, Mater. Sci. Eng. A, 2018, 729, p 119–124 (in English)10.1016/j.msea.2018.05.058 ↗
33. S.L. Semiatin, V. Seetharaman, and I. Weiss, Flow Behavior and Globularization Kinetics During Hot Working of Ti-6Al-4V with a Colony Alpha Microstructure, Mater. Sci. Eng. A, 1999, 263(2), p 257–271 (in English)10.1016/S0921-5093(98)01156-3 ↗
34. L.G. Guo, X.G. Fan, G.F. Yu, and H. Yang, Microstructure Control Techniques in Primary Hot Working of Titanium Alloy Bars: A Review, Chin. J. Aeronaut., 2016, 29(1), p 30–40 (in English)10.1016/j.cja.2015.07.011 ↗
35. M. Kopec, K.H. Wang, D.J. Politis, Y.Q. Wang, L.L. Wang, and J.G. Lin, Formability and Microstructure Evolution Mechanisms of Ti6Al4V Alloy During a Novel Hot Stamping Process, Mater. Sci. Eng. A, 2018, 719, p 72–81 (in English)10.1016/j.msea.2018.02.038 ↗
36. R. Ebrahimi and A. Najafizadeh, A New Method for Evaluation of Friction in Bulk Metal Forming, J. Mater. Process. Technol., 2004, 152(2), p 136–143 (in English)10.1016/j.jmatprotec.2004.03.029 ↗
37. T. Seshacharyulu, S.C. Medeiros, J.T. Morgan, J.C. Malas, W.G. Frazier, and Y.V.R.K. Prasad, Hot Deformation and Microstructural Damage Mechanisms in Extra-Low Interstitial (ELI) Grade Ti-6Al-4V, Mater. Sci. Eng. A, 2000, 279(1), p 289–299 (in English)10.1016/S0921-5093(99)00173-2 ↗
38. J.J. Jonas, C.M. Sellars, and W.J.M. Tegart, Strength and Structure Under Hot-Working Conditions, Metall. Rev., 1969, 14(1), p 1–24 (in English)10.1179/095066069790138056 ↗
39. R.M. Miller, T.R. Bieler, and S.L. Semiatin, Flow Softening During Hot Working of Ti-6Al-4V with a Lamellar Colony Microstructure, Scr. Mater., 1999, 40(12), p 1387–1393 (in English)10.1016/S1359-6462(99)00061-5 ↗
40. Y. Kim, Y.B. Song, S.H. Lee, and Y.S. Kwon, Characterization of the Hot Deformation Behavior and Microstructural Evolution of Ti-6Al-4V Sintered Preforms Using Materials Modeling Techniques, J. Alloys Compd., 2016, 676, p 15–25 (in English)10.1016/j.jallcom.2016.03.146 ↗
41. G.F. Liu, S.Z. Zhang, L.Q. Chen, and J.X. Qiu, Deformation Behavior and Microstructural Evolution During Hot Compression of an α + β Ti-6.5Al-3.5Mo-1.5Zr-0.3Si Alloy, Int. J. Miner. Metall. Mater., 2011, 18(3), p 344–351 (in English)10.1007/s12613-011-0445-6 ↗
42. N. Kotkunde, H.N. Krishnamurthy, P. Puranik, A.K. Gupta, and S.K. Singh, Microstructure Study and Constitutive Modeling of Ti-6Al-4V Alloy at Elevated Temperatures, Mater. Des., 2014, 54(2), p 96–103 (in English)10.1016/j.matdes.2013.08.006 ↗
43. Q. Bai, J. Lin, T.A. Dean, D.S. Bailint, T. Gao, and Z. Zhang, Modelling of Dominant Softening Mechanisms for Ti-6Al-4V in Steady State Hot Forming Conditions, Mater. Sci. Eng. A, 2013, 559, p 352–358 (in English)10.1016/j.msea.2012.08.110 ↗
44. I. Weiss, F.H. Froes, D. Eylon, and G.E. Welsch, Modification of Alpha Morphology in Ti-6Al-4V by Thermomechanical Processing, Metall. Trans. A, 1986, 17(11), p 1935–1947 (in English)10.1007/BF02644991 ↗
45. Y. Kim, Y.B. Song, S.H. Lee, and Y.S. Kwon, Characterization of the Hot Deformation Behavior and Microstructural Evolution of Ti-6Al-4V Sintered Preforms Using Materials Modeling Techniques, J. Alloys Compd., 2016, 676, p 15–25 (in English)10.1016/j.jallcom.2016.03.146 ↗
46. P. Kumar, K.S.R. Chandran, F. Cao, M. Koopman, and Z.Z. Fang, The Nature of Tensile Ductility as Controlled by Extreme-Sized Pores in Powder Metallurgy Ti-6Al-4V Alloy, Metall. Mater. Trans. A, 2016, 47(5), p 2150–2161 (in English)10.1007/s11661-016-3419-5 ↗
47. F. Cao, K.S.R. Chandran, P. Kumar, P. Sun, Z.Z. Fang, and M. Koopman, New Powder Metallurgical Approach to Achieve High Fatigue Strength in Ti-6Al-4V Alloy, Metall. Mater. Trans. A, 2016, 47(5), p 2335–2345 (in English)10.1007/s11661-016-3409-7 ↗
48. Y. Wang, S.Q. Zhang, X.J. Tian, and H.M. Wang, High-Cycle Fatigue Crack Initiation and Propagation in Laser Melting Deposited TC18 Titanium Alloy, Int. J. Miner. Metall. Mater., 2013, 20(7), p 665–670 (in English)10.1007/s12613-013-0781-9 ↗
49. I. Weiss, D. Eylon, M.W. Toaz, and F.H. Froes, Effect of Isothermal Forging on Microstructure and Fatigue Behavior of Blended Elemental Ti-6Al-4V Powder Compacts, Metall. Mater. Trans. A, 1986, 17(3), p 549–559 (in English)10.1007/BF02643962 ↗