Improved Mechanical Properties of Structural Steel via Developing Bimodal Grain Size Distribution and Intercritical Heat Treatment
Source abstract
Abstract
Intercritical annealing and tempering heat treatment combined with cold rolling were applied for improvement of tensile properties and strain-hardening rate of structural steel. Coarse dual-phase (DP) microstructure was processed via intercritical heat treatment of the ferritic–pearlitic sheet, which resulted in the increase in tensile strength and disappearance of the yield point phenomenon. However, the tensile toughness was not effectively enhanced, which is indicative of unaltered strength–ductility trade-off. A bimodal-sized ferrite structure was obtained by cold rolling of the DP microstructure followed by subcritical annealing (tempering), where its characteristic features are high yield stress and relatively poor work-hardening response. Afterward, the intercritical annealing of the bimodal steel resulted in the development of fine DP steel with excellent work-hardening capacity and pronounced enhancement of tensile toughness. Conclusively, this work demonstrates the possibility of controlling the tensile properties and work-hardening behavior of conventional steels by simple heat treatment routes with the aid of cold rolling.
Source: openaire · Quality: candidate unverified · Source record ↗
Research context
OpenAlex topics: Microstructure and Mechanical Properties of Steels · Metal Alloys Wear and Properties · High Entropy Alloys Studies
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (58)
Show source-provided references
1. C.P. Scott, B.S. Amirkhiz, I. Pushkareva, F. Fazeli, S.Y.P. Allain, and H. Azizi, New Insights into Martensite Strength and the Damage Behaviour of Dual Phase Steels, Acta Mater., 2018, 159, p 112–12210.1016/j.actamat.2018.08.010 ↗
2. T. Dutta, S. Dey, S. Datta, and D. Das, Designing Dual-Phase Steels with Improved Performance Using ANN and GA in Tandem, Comput. Mater. Sci., 2019, 157, p 6–1610.1016/j.commatsci.2018.10.020 ↗
3. S. Sahoo, N. Padmapriya, P.S. De, P.C. Chakraborti, and S.K. Ray, Ductile Tearing Resistance Indexing of Automotive Grade DP 590 Steel Sheets: EWF Testing Using DENT Specimens, J. Mater. Eng. Perform., 2018, 27, p 2018–202310.1007/s11665-018-3293-y ↗
4. C. Thomser, V. Uthaisangsuk, and W. Bleck, Influence of Martensite Distribution on the Mechanical Properties of Dual Phase Steels: Experiments and Simulation, Steel Res. Int., 2009, 80, p 582–587
5. Y. Deng, H. Di, M. Hu, J. Zhang, and R.D.K. Misra, High Strength-High Ductility Combination Ultrafine-Grained Dual-Phase Steels Through Introduction of High Degree of Strain at Room Temperature Followed by Ultrarapid Heating During Continuous Annealing of a Nb-Microalloyed Steel, J. Mater. Eng. Perform., 2017, 26, p 3007–301510.1007/s11665-017-2740-5 ↗
6. C.C. Tasan, M. Diehl, D. Yan, M. Bechtold, F. Roters, L. Schemmann, C. Zheng, N. Peranio, D. Ponge, M. Koyama, K. Tsuzaki, and D. Raabe, An Overview of Dual-Phase Steels: Advances in Microstructure-Oriented Processing and Micromechanically Guided Design, Annu. Rev. Mater. Res., 2015, 45, p 19.1–19.4110.1146/annurev-matsci-070214-021103 ↗
7. S. Sodjit and V. Uthaisangsuk, Microstructure Based Prediction of Strain Hardening Behavior of Dual Phase Steels, Mater. Des., 2012, 41, p 370–37910.1016/j.matdes.2012.05.010 ↗
8. M. Mazinani and W.J. Poole, Effect of Martensite Plasticity on the Deformation Behavior of a Low-Carbon Dual-Phase Steel, Metall. Mater. Trans. A, 2007, 38, p 328–33910.1007/s11661-006-9023-3 ↗
9. H. Mirzadeh, M. Alibeyki, and M. Najafi, Unraveling the Initial Microstructure Effects on Mechanical Properties and Work-Hardening Capacity of Dual Phase Steel, Metall. Mater. Trans. A, 2017, 48, p 4565–457310.1007/s11661-017-4246-z ↗
10. D. Das and P.P. Chattopadhyay, Influence of Martensite Morphology on the Work-Hardening Behavior of High Strength Ferrite–Martensite Dual-Phase Steel, J. Mater. Sci., 2009, 44, p 2957–296510.1007/s10853-009-3392-0 ↗
11. A. Kalhor and H. Mirzadeh, Tailoring the Microstructure and Mechanical Properties of Dual Phase Steel Based on the Initial Microstructure, Steel Res. Int., 2017, 88, p 160038510.1002/srin.201600385 ↗
12. H. Seyedrezai, A.K. Pilkey, and J.D. Boyd, Effect of Pre-IC Annealing Treatments on the Final Microstructure and Work Hardening Behavior of a Dual-Phase Steel, Mater. Sci. Eng. A, 2014, 594, p 178–18810.1016/j.msea.2013.11.034 ↗
13. A. Ramazani, S. Bruehl, M. Abbasi, W. Bleck, and U. Prahl, The Effect of Bake-Hardening Parameters on the Mechanical Properties of Dual-Phase Steels, Steel Res. Int., 2016, 87, p 1559–156510.1002/srin.201600060 ↗
14. M. Zamani, H. Mirzadeh, and M. Maleki, Enhancement of Mechanical Properties of Low Carbon Dual Phase Steel via Natural Aging, Mater. Sci. Eng. A, 2018, 734, p 178–18310.1016/j.msea.2018.07.105 ↗
15. N. Ormsuptave and V. Uthaisangsuk, Effect of Fine Grained Dual Phase Steel on Bake Hardening Properties, Steel Res. Int., 2017, 88, p 160015010.1002/srin.201600150 ↗
16. T. Waterschoot, A.K. De, S. Vandeputte, and B.C. De Cooman, Static Strain Aging Phenomena in Cold-Rolled Dual-Phase Steels, Metall. Mater. Trans. A, 2003, 34, p 781–79110.1007/s11661-003-1006-z ↗
17. N. Nakada, Y. Arakawa, K.S. Park, T. Tsuchiyama, and S. Takaki, Dual Phase Structure Formed by Partial Reversion of Cold-Deformed Martensite, Mater. Sci. Eng. A, 2012, 553, p 128–13310.1016/j.msea.2012.06.001 ↗
18. M. Alibeyki, H. Mirzadeh, and M. Najafi, Fine-Grained Dual Phase Steel via Intercritical Annealing of Cold-Rolled Martensite, Vacuum, 2018, 155, p 147–15210.1016/j.vacuum.2018.06.003 ↗
19. H. Azizi-Alizamini, M. Militzer, and W.J. Poole, Formation of Ultrafine Grained Dual Phase Steels through Rapid Heating, ISIJ Int., 2011, 51, p 958–96410.2355/isijinternational.51.958 ↗
20. M. Nouroozi, H. Mirzadeh, and M. Zamani, Effect of Microstructural Refinement and Intercritical Annealing Time on Mechanical Properties of High-Formability Dual Phase Steel, Mater. Sci. Eng. A, 2018, 736, p 22–2610.1016/j.msea.2018.08.088 ↗
21. Y. Karimi, S.H. Nedjad, H. Shirazi, M.N. Ahmadabadi, H. Zargari, and K. Ito, Cold Rolling and Intercritical Annealing of C-Mn Steel Sheets with Different Initial Microstructures, Mater. Sci. Eng. A, 2018, 736, p 392–39910.1016/j.msea.2018.09.008 ↗
22. H. Azizi-Alizamini, M. Militzer, and W.J. Poole, A Novel Technique for Developing Bimodal Grain Size Distributions in Low Carbon Steels, Scr. Mater., 2007, 57, p 1065–106810.1016/j.scriptamat.2007.08.035 ↗
23. T.S. Wang, Z. Li, B. Zhang, X.J. Zhang, J.M. Deng, and F.C. Zhang, High Tensile Ductility and High Strength in Ultrafine-Grained Low-Carbon Steel, Mater. Sci. Eng. A, 2010, 527, p 2798–280110.1016/j.msea.2010.01.072 ↗
24. A. Karmakar, A. Karani, S. Patra, and D. Chakrabarti, Development of Bimodal Ferrite-Grain Structures in Low-Carbon Steel Using Rapid Intercritical Annealing, Metall. Mater. Trans. A, 2013, 44, p 2041–205210.1007/s11661-012-1556-z ↗
25. M.P. Rao, V.S. Sarma, and S. Sankaran, Processing of Bimodal Grain-Sized Ultrafine-Grained Dual Phase Microalloyed V-Nb Steel with 1370 MPa Strength and 16 pct Uniform Elongation Through Warm Rolling and Intercritical Annealing, Metall. Mater. Trans. A, 2014, 45, p 5313–531710.1007/s11661-014-2478-8 ↗
26. M. Alibeyki, H. Mirzadeh, and M. Najafi, The Effects of Primary Thermo-mechanical Processing Routes and Intercritical Annealing on the Mechanical Properties of st37 Low Carbon Steel, Kov. Mater., 2018, 56, p 297–303
27. M.C. Zhao, F. Yin, T. Hanamura, K. Nagai, and A. Atrens, Relationship Between Yield Strength and Grain Size for a Bimodal Structural Ultrafine-Grained Ferrite/Cementite Steel, Scr. Mater., 2007, 57, p 857–86010.1016/j.scriptamat.2007.06.062 ↗
28. S. Ghaemifar and H. Mirzadeh, Refinement of Banded Structure via Thermal Cycling and Its Effects on Mechanical Properties of Dual Phase Steel, Steel Res. Int., 2018, 89, p 170053110.1002/srin.201700531 ↗
29. S. Ghaemifar and H. Mirzadeh, Enhanced Mechanical Properties of Dual Phase Steel by Repetitive Intercritical Annealing, Can. Metall. Q., 2017, 56, p 459–46310.1080/00084433.2017.1361223 ↗
30. K.T. Park, Y.K. Lee, and D.H. Shin, Fabrication of Ultrafine Grained Ferrite/Martensite Dual Phase Steel by Severe Plastic Deformation, ISIJ Int., 2005, 45, p 750–75510.2355/isijinternational.45.750 ↗
31. K. Mukherjee, S.S. Hazra, and M. Militzer, Grain Refinement in Dual-Phase Steels, Metall. Mater. Trans. A, 2009, 40, p 2145–215910.1007/s11661-009-9899-9 ↗
32. R. Ueji, N. Tsuji, Y. Minamino, and Y. Koizumi, Ultragrain Refinement of Plain Low Carbon Steel by Cold-Rolling and Annealing of Martensite, Acta Mater., 2002, 50, p 4177–418910.1016/S1359-6454(02)00260-4 ↗
33. M. Najafi, H. Mirzadeh, and M. Alibeyki, Toward Unraveling the Mechanisms Responsible for the Formation of Ultrafine Grained Microstructure During Tempering of Cold Rolled Martensite, Mater. Sci. Eng. A, 2016, 670, p 252–25510.1016/j.msea.2016.06.024 ↗
34. H.F. Lan, W.J. Liu, and X.H. Liu, Ultrafine Ferrite Grains Produced by Tempering Cold-Rolled Martensite in Low Carbon and Microalloyed Steels, ISIJ Int., 2007, 47, p 1652–165710.2355/isijinternational.47.1652 ↗
35. M. Najafi, H. Mirzadeh, and M. Alibeyki, Tempering of Deformed and As-Quenched Martensite in Structural Steel, J. Min. Metall. Sect. B., 2019, 55, p 95–9910.2298/JMMB180813002N ↗
36. Z. Nasiri and H. Mirzadeh, Enhancement of Work-Hardening Behavior of Dual Phase Steel by Heat Treatment, Materialwiss. Werkstofftech., 2018, 49, p 1081–108610.1002/mawe.201700122 ↗
37. M. Alibeyki, H. Mirzadeh, M. Najafi, and A. Kalhor, Modification of Rule of Mixtures for Estimation of the Mechanical Properties of Dual-Phase Steel, J. Mater. Eng. Perform., 2017, 26, p 2683–268810.1007/s11665-017-2687-6 ↗
38. M. Maleki, H. Mirzadeh, and M. Zamani, Effect of Intercritical Annealing on Mechanical Properties and Work-Hardening Response of High Formability Dual Phase Steel, Steel Res. Int., 2018, 89, p 170041210.1002/srin.201700412 ↗
39. M. Maleki, H. Mirzadeh, and M. Zamani, Effect of Intercritical Annealing Time at Pearlite Dissolution Finish Temperature (Ac1f) on Mechanical Properties of Low Carbon Dual Phase Steel, J. Mater. Eng. Perform., 2019, 28, p 2178–218310.1007/s11665-019-04009-y ↗
40. M. Razzaghi, H. Mirzadeh, and M. Emamy, Unraveling the Effects of Zn Addition and Hot Extrusion Process on the Microstructure and Mechanical Properties of As-Cast Mg-2Al Magnesium Alloy, Vacuum, 2019, 167, p 214–22210.1016/j.vacuum.2019.06.013 ↗
41. G. Krauss, Steels Processing, Structure, and Performance, 2nd ed., ASM International, Materials Park, 201510.31399/asm.tb.spsp2.9781627082655 ↗
42. M. Calcagnotto, D. Ponge, E. Demir, and D. Raabe, Effect of Grain Refinement to 1 μm on Strength and Toughness of Dual-Phase Steels, Mater. Sci. Eng. A, 2010, 527, p 7832–784010.1016/j.msea.2010.08.062 ↗
43. M. Calcagnotto, Y. Adachi, D. Ponge, and D. Raabe, Deformation and Fracture Mechanisms in Fine- and Ultrafine-Grained Ferrite/Martensite Dual-Phase Steels and the Effect of Aging, Acta Mater., 2011, 59, p 658–67010.1016/j.actamat.2010.10.002 ↗
44. S. Saadatkia, H. Mirzadeh, and J.M. Cabrera, Hot Deformation Behavior, Dynamic Recrystallization, and Physically-Based Constitutive Modeling of Plain Carbon Steels, Mater. Sci. Eng. A, 2015, 636, p 196–20210.1016/j.msea.2015.03.104 ↗
45. B. Pourbahari, H. Mirzadeh, M. Emamy, and R. Roumina, Enhanced Ductility of a Fine-Grained Mg-Gd-Al-Zn Magnesium Alloy by Hot Extrusion, Adv. Eng. Mater., 2018, 20, p 170117110.1002/adem.201701171 ↗
46. H. Mirzadeh, J.M. Cabrera, J.M. Prado, and A. Najafizadeh, Hot Deformation Behavior of a Medium Carbon Microalloyed Steel, Mater. Sci. Eng. A, 2011, 528, p 3876–388210.1016/j.msea.2011.01.098 ↗
47. F. Najafkhani, H. Mirzadeh, M. Zamani, Effect of Intercritical Annealing Conditions on Grain Growth Kinetics of Dual Phase Steel. Met. Mater. Int., 2019, 25, p 1039–104610.1007/s12540-019-00241-2 ↗
48. N.K. Balliger and T. Gladman, Work Hardening of Dual-Phase Steels, Met. Sci., 1981, 15, p 95–10810.1179/030634581790426615 ↗
49. S. Nikkhah, H. Mirzadeh, and M. Zamani, Improved Mechanical Properties of Mild Steel via Combination of Deformation, Intercritical Annealing, and Quench Aging, Mater. Sci. Eng. A, 2019, 756, p 268–27110.1016/j.msea.2019.04.071 ↗
50. Y.I. Son, Y.K. Lee, K.T. Park, C.S. Lee, and D.H. Shin, Ultrafine Grained Ferrite–Martensite Dual Phase Steels Fabricated via Equal Channel Angular Pressing: Microstructure and Tensile Properties, Acta Mater., 2005, 53, p 3125–313410.1016/j.actamat.2005.02.015 ↗
51. F. Jamei, H. Mirzadeh, and M. Zamani, Synergistic Effects of Holding Time at Intercritical Annealing Temperature and Initial Microstructure on the Mechanical Properties of Dual Phase Steel, Mater. Sci. Eng. A, 2019, 750, p 125–13110.1016/j.msea.2019.02.052 ↗
52. H. Seyedrezai, A.K. Pilkey, and J.D. Boyd, Effects of Martensite Particle Size and Spatial Distribution on Work Hardening Behaviour of Fine-Grained Dual-Phase Steel, Can. Metall. Q., 2018, 57, p 28–3710.1080/00084433.2017.1403105 ↗
53. R. Zamani, H. Mirzadeh, and M. Emamy, Mechanical Properties of a Hot Deformed Al-Mg2Si In-Situ Composite, Mater. Sci. Eng. A, 2018, 726, p 10–1710.1016/j.msea.2018.04.064 ↗
54. B. Pourbahari, H. Mirzadeh, and M. Emamy, Toward Unraveling the Effects of Intermetallic Compounds on the Microstructure and Mechanical Properties of Mg-Gd-Al-Zn Magnesium Alloys in the As-Cast, Homogenized, and Extruded Conditions, Mater. Sci. Eng. A, 2017, 680, p 39–4610.1016/j.msea.2016.10.084 ↗
55. S. Nikkhah, H. Mirzadeh, and M. Zamani, Fine Tuning the Mechanical Properties of Dual Phase Steel via Thermomechanical Processing of Cold Rolling and Intercritical Annealing, Mater. Chem. Phys., 2019, 230, p 1–810.1016/j.matchemphys.2019.03.053 ↗
56. N. Barri, A.R. Salasel, A. Abbasi, H. Mirzadeh, M. Emamy, and M. Malekan, A New Intermetallic Phase Formation in Mg-Si-Ni Magnesium-Based In-Situ Formed Alloys, Vacuum, 2019, 164, p 349–35410.1016/j.vacuum.2019.03.050 ↗
57. S. Kheiri, H. Mirzadeh, and M. Naghizadeh, Tailoring the Microstructure and Mechanical Properties of AISI, 316L Austenitic Stainless Steel via Cold Rolling and Reversion Annealing, Mater. Sci. Eng. A, 2019, 759, p 90–9610.1016/j.msea.2019.05.028 ↗
58. A.R. Salasel, A. Abbasi, N. Barri, H. Mirzadeh, M. Emamy, and M. Malekan, Effect of Si and Ni on Microstructure and Mechanical Properties of In-Situ Magnesium-Based Composites in the As-Cast and Extruded Conditions, Mater. Chem. Phys., 2019, 232, p 305–31010.1016/j.matchemphys.2019.04.079 ↗