journal article·2015-06

Mechanical Property of Pure Magnesium: From Orientation Perspective Pertaining to Deviation from Basal Orientation

S. K. Sahoo, R. K. Sabat, S. Panda, S. C. Mishra, S. Suwas

Publisher page

Abstract

Pure magnesium is subjected to cold rolling followed by annealing at 200 °C to obtain near-equiaxed grains of average grain size ~15 µm. The hardness of different grains/orientations of the annealed samples is estimated through consecutive characterization by nanoindentation and electron backscattered diffraction. It is observed that an increase in deviation from basal orientation decreases the hardness of an orientation. Orientations <14° from basal orientation have higher hardness compared to orientations at 14° to 28° from basal orientations. Subsequently, the texture and microstructure of pure magnesium are tailored to examine the correlation between volume fractions of basal orientations with the bulk hardness of the samples. A direct relationship of hardness with the volume fraction of basal orientations is observed. Magnesium with higher volume fraction of basal orientations has higher hardness.
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Magnesium Alloys: Properties and Applications · Metal and Thin Film Mechanics · Microstructure and mechanical properties

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (36)

Show source-provided references
1. B.L. Mordike and T. Ebert, Magnesium: Properties—Applications—Potential, Mater. Sci. Eng. A, 2001, 302, p 37–4510.1016/S0921-5093(00)01351-4 ↗
2. J. Xing, X. Yang, H. Miuna, and T. Sakai, Superplasticity of Magnesium Alloy AZ31 Processes by Severe Plastic Deformation, Mater. Trans., 2007, 48, p 1406–141110.2320/matertrans.L-MRA2007839 ↗
3. T. Mukai, H. Watanabe, K. Ishikawa, and K. Higashi, Guide for Enhancement of Room Temperature Ductility in Mg Alloys at High Strain Rates, Mater. Sci. Forum, 2003, 419–422, p 171–17610.4028/www.scientific.net/MSF.419-422.171 ↗
4. S.R. Agnew, P. Mehrotra, T.M. Lillo, G.M. Stoica, and P.K. Liaw, Texture Evolution of Five Wrought Magnesium Alloys during Route A Equal Channel Angular Extrusion: Experiments and Simulations, Acta Mater., 2005, 53, p 3135–314610.1016/j.actamat.2005.02.019 ↗
5. S. Sandlobes, S. Zaefferer, I. Schestakow, S. Yi, and R. Gonzalez-Martinez, On the Role of Non-basal Deformation Mechanisms for the Ductility of Mg and Mg-Y Alloys, Acta Mater., 2011, 59, p 429–43910.1016/j.actamat.2010.08.031 ↗
6. S. Suwas, G. Gottstein, and R. Kumar, Evolution of Crystallographic Texture during Equal Channel Angular Extrusion (ECAE) and Its Effect on Secondary Processing of Magnesium, Mater. Sci. Eng. A, 2007, 471, p 1–1410.1016/j.msea.2007.05.030 ↗
7. L. Capolungo, I.J. Beyerlein, and C.N. Tome, Slip-Assisted Twin Growth in Hexagonal Close-Packed Metals, Scripta Mater., 2009, 60, p 32–3510.1016/j.scriptamat.2008.08.044 ↗
8. S.R. Agnew, J.A. Horton, and M.H. Yoo, TEM Invesitgation of Dislocation Structures in Mg and Mg-Li a-Solid Solution Alloys, Metall. Mater. Trans. A, 2002, 33, p 851–85810.1007/s11661-002-0154-x ↗
9. M.H. Yoo and J.K. Lee, Deformation Twinning in h.c.p Metals and Alloys, Philos. Mag. A, 1991, 63, p 987–100010.1080/01418619108213931 ↗
10. A. Jain and S.R. Agnew, Modeling the Temperature Dependent Effect of Twinning on the Behavior of Magnesium Alloy AZ31B Sheet, Mater. Sci. Eng. A, 2007, 462, p 29–3610.1016/j.msea.2006.03.160 ↗
11. A. Chapuis and J.H. Driver, Temperature Dependency of Slip and Twinning in Plane Strain Compressed Magnesium Single Crystals, Acta Mater., 2011, 59, p 1986–199410.1016/j.actamat.2010.11.064 ↗
12. L.L. Chang, Y.N. Wang, X. Zhao, and J.C. Huang, Microstructure and Mechanical Properties in an AZ31 Magnesium Alloy Sheet Fabricated by Asymmetric Hot Extrusion, Mater. Sci. Eng. A, 2008, 496, p 512–51610.1016/j.msea.2008.06.015 ↗
13. N. Stanford and M.R. Barnett, The Origin of “Rare Earth” Texture Development in Extruded Mg-Based Alloys and its Effect on Tensile Ductility, Mater. Sci. Eng. A, 2008, 496, p 399–40810.1016/j.msea.2008.05.045 ↗
14. J. Koike, T. Kobayashi, T. Mukai, H. Watanabe, M. Suzuki, K. Maruyama, and K. Higashi, The Activity of Non-basal Slip Systems and Dynamic Recovery at Room Temperature in Fine-Grained AZ31B Magnesium Alloys, Acta Mater., 2003, 51, p 2055–206510.1016/S1359-6454(03)00005-3 ↗
15. B. Beausir, S. Suwas, L.S. Tóth, K.W. Neale, and J.J. Fundenberger, Analysis of Texture Evolution in Magnesium During Equal Channel Angular Extrusion, Acta Mater., 2008, 56, p 200–21410.1016/j.actamat.2007.09.032 ↗
16. S.H. Kim, B.S. You, C.D. Yim, and Y.M. Seo, Texture and Microstructure Changes in Asymmetrically Hot Rolled AZ31 Magnesium Alloy Sheets, Mater. Lett., 2005, 59, p 3876–388010.1016/j.matlet.2005.07.024 ↗
17. B. Beausir, S. Biswas, D. Kim, L.S. Toth, and S. Suwas, Analysis of Microstructure and Texture Evolution in Pure Magnesium During Symmetric and Asymmetric Rolling, Acta Mater., 2009, 57, p 5061–507710.1016/j.actamat.2009.07.008 ↗
18. X. Gong, H. Li, S.B. Kang, J.H. Cho, and S. Li, Microstructure and Mechanical Properties of Twin-Roll Cast Mg-4.5Al-1.0Zn Sheets Processed by Differential Speed Rolling, Mater. Des., 2010, 31, p 1581–158710.1016/j.matdes.2009.09.021 ↗
19. S.E. Ion, F.J. Humphreys, and S.H. White, Dynamic Recrystallization and the Development of Microstructure During the High Temperature Deformation of Magnesium, Acta. Mater., 1982, 30, p 1909–191910.1016/0001-6160(82)90031-1 ↗
20. Y. Qiao, X. Wang, Z. Liu, and E. Wang, Effect of Temperature on Microstructures, Texture and Mechanical Properties of Hot Rolled Pure Mg Sheets, Mater. Sci. Eng. A, 2013, 568, p 202–20510.1016/j.msea.2013.01.036 ↗
21. K. Pawlik and P. Ozga, LaboTex: The Texture Analysis Software, Göttinger Arbeiten zur Geologie und Paläontologie, SB4, 1999.
22. I. Groma and F. Szekely, Analysis of the Asymptotic Properties of X-ray Line Broadening Caused by Dislocations, J. Appl. Cryst., 2000, 33, p 1329–133410.1107/S002188980001058X ↗
23. N. Rajmohan, Y. Hayakawa, J.A. Szpunar, and J.H. Root, Neutron Diffraction Method for Stored Energy Measurement in Interstitial Free Steel, Acta Mater., 1997, 45, p 2485–249410.1016/S1359-6454(96)00371-0 ↗
24. T. Mura, Micromechanics of Defects in Solids, Matrinus Nijhoff Publishers, Dordrecht, 1987, p 421–43910.1007/978-94-009-3489-4 ↗
25. Z. Zeng, Y. Zhang, and S. Jonsson, Microstructure and Texture Evolution of Commercial Pure Titanium Deformed at Elevated Temperatures, Mater. Sci. Eng. A, 2009, 513–514, p 83–9010.1016/j.msea.2009.01.065 ↗
26. T.B. Britton, H. Liang, F.P.E. Dunne, and A.J. Wilkinson, The Effect of Crystal Orientation on the Indentation Response of Commercially Pure Titanium: Experiments and Simulations, Proc. R. Soc. A, 2010, 466, p 695–71910.1098/rspa.2009.0455 ↗
27. G.B. Viswanathan, E. Lee, D.M. Maher, S. Banerjee, and H.L. Fraser, Direct Observations and Analyses of Dislocation Substructures in the α Phase of an α/β Ti-Alloy Formed by Nanoindentation, Acta Mater., 2005, 53, p 5101–511510.1016/j.actamat.2005.07.030 ↗
28. F.K. Mante, G.R. Baran, and B. Lucas, Nanoindentation Studies of Titanium Single Crystals, Biomaterials, 1999, 20, p 1051–105510.1016/S0142-9612(98)00257-9 ↗
29. G. Nayyeri, W. J. Poole and C. W. Sinclair, Proc. 9th Int. Conf. Mg Alloys Appl., eds. W. J. Poole and K. U. Kainer, Vancouver, 2012, p 1325–1330.
30. R. Sanchez-Martin, M.T. Perez-Prado, J. Segurado, J. Bohlen, I. Gutierrez-Urrutia, J. Llorca, and J.M. Molina-Aldareguia, Measuring the Critical Resolved Shear Stresses in Mg Alloys by Instrumented Nanoindentation, Acta Mater., 2014, 71, p 283–29210.1016/j.actamat.2014.03.014 ↗
31. B. Selvarajou, J.H. Shin, T.K. Ha, I. Choi, S.P. Joshi, and H.N. Han, Orientation-Dependent Indentation Response of Magnesium Single Crystals: Modeling and Experiments, Acta Mater., 2014, 81, p 358–37610.1016/j.actamat.2014.08.042 ↗
32. H. Yoshinaga and R. Horiuchi, Deformation Mechanism in Magnesium Single Crystals Compressed in the Direction Parallel to Hexagonal Axis, Trans. JIM, 1963, 4, p 1–810.2320/matertrans1960.4.1 ↗
33. M.R. Barnett, Twinning and the Ductility of Magnesium Alloys: Part I, “Contraction” Twins, Mater. Sci. Eng. A, 2007, 464, p 1–710.1016/j.msea.2006.12.037 ↗
34. M.R. Barnett, Twinning and the Ductility of Magnesium Alloys: Part II, “Contraction” Twins, Mater. Sci. Eng. A, 2007, 464, p 8–1610.1016/j.msea.2007.02.109 ↗
35. L. Meng, P. Yang, Q. Xie, and W. Mao, Analyses on Compression Twins in Magnesium, Mater. Trans., 2008, 49, p 710–71410.2320/matertrans.MRA2007242 ↗
36. S. Biswas, S.S. Dhinwal, and S. Suwas, Room-Temperature Equal Channel Angular Extrusion of Pure Magnesium, Acta Mater., 2010, 58, p 3247–326110.1016/j.actamat.2010.01.051 ↗