Evaluation Methods for Non-contact Bend and Free Recovery Tests of Thin NiTi Wires and Their Effects on Measured Transformation Temperatures
Source abstract
Abstract
Abstract Non-contact evaluation of transformation temperatures via bend and free recovery tests requires precise optical evaluation of shape changes of NiTi components. A variety of experimental setups is documented in the literature, but the influence of the evaluation method on the transformation temperatures is rarely assessed in detail. In the present work, the reverse transformation of bent wires is evaluated comparing the tracking of the lowest wire point and the tracking of the curvature. For calculating curvatures, different approaches of fitting the wire outline were applied. Fourth degree polynomials and ellipse segment fits were found to cause high noise toward the end of the reverse transformation, second degree polynomials and circle segment fits led to increased sensitivity in that region. Accordingly, the evaluation of curvature allowed to resolve a two-stage reverse transformation, which was otherwise obscured. The reasons for this effect are discussed comparing curvatures as determined by the different evaluation methods.
Source: crossref · Quality: baseline
Research context
OpenAlex topics: Shape Memory Alloy Transformations · High Entropy Alloys Studies · Intermetallics and Advanced Alloy Properties
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (18)
Show source-provided references
1. T.W. Duerig, A.R. Pelton, and D. Stöckel, The Utility of Superelasticity in Medicine, Bio-Med. Mater. Eng., 1996, 6(4), p 255–26610.3233/BME-1996-6404 ↗
2. A.R. Pelton, J. Dicello, and S. Miyazaki, Optimisation of Processing and Properties of Medical Grade Nitinol Wire, Min. lnvasive Ther. Allied Technol., 2000, 9(2), p 107–11810.3109/13645700009063057 ↗
3. K. Otsuka and X. Ren, Physical Metallurgy of Ti-Ni-Based Shape Memory Alloys, Prog. Mater. Sci., 2005, 50(5), p 511–67810.1016/j.pmatsci.2004.10.001 ↗
4. S. Miyazaki and K. Otsuka, Deformation and Transition Behavior Associated with the R-Phase in Ti-Ni Alloys, Metall. Trans. A, 1986, 17(1), p 53–6310.1007/BF02644442 ↗
5. Standard Test Method for Transformation Temperature of Nickel-Titanium Alloys by Thermal Analysis, F2004-17, ASTM International, 2017
6. Standard Test Method for Determination of Transformation Temperature of Nickel-Titanium Shape Memory Alloys by Bend and Free Recovery, F2082/F2082M-16, ASTM International, 2016
7. A. Nespoli, E. Villa, F. Passaretti, F. Albertini, R. Cabassi, M. Pasquale, C.P. Sasso, and M. Coïsson, Non-conventional Techniques for the Study of Phase Transitions in NiTi-Based Alloys, J. Mater. Eng. Perform., 2014, 23(7), p 2491–249710.1007/s11665-014-1105-6 ↗
8. M.H. Wu, M. Polinsky, and N. Webb, What Is The Big Deal About The Af Temperature?, in SMST 2006: Proceedings of the International Conference on Shape Memory and Superelastic Technologies, B. Berg, M.R. Mitchell, and J. Proft, Ed., May 7–11, 2006 (Pacific Grove, CA, USA), SMST, 2008, p 143–154
9. J. Pache, A. Kastrati, J. Mehilli, H. Schühlen, F. Dotzer, J. Hausleiter, M. Fleckenstein, F.-J. Neumann, U. Sattelberger, C. Schmitt, M. Müller, J. Dirschinger, and A. Schömig, Intracoronary Stenting and Angiographic Results: Strut Thickness Effect on Restenosis Outcome (ISAR-STEREO-2) Trial, J. Am. Coll. Cardiol., 2003, 41(8), p 1283–128810.1016/S0735-1097(03)00119-0 ↗
10. S. Zende, K.E. Freiberg, F. Dorner, N.-A. Feth, and A. Undisz, Corrosion Resistance of Nitinol Wires After Deformation, Shape Mem. Superelast., 2019, 5(4), p 346–35110.1007/s40830-019-00243-4 ↗
11. A. Undisz, M. Fink, and M. Rettenmayr, Response of Austenite Finish Temperature and Phase Transformation Characteristics of Thin Medical-Grade Ni-Ti Wire to Short-Time Annealing, Scr. Mater., 2008, 59(9), p 979–98210.1016/j.scriptamat.2008.06.057 ↗
12. A. Undisz, M. Fink, and M. Rettenmayr, Determination of Transformation Properties of Thin Medical Grade Ni-Ti Wire by High-Resolution Bend and Free Recovery Testing, J. Mater. Eng. Perform., 2009, 18(5), p 814–81710.1007/s11665-009-9451-5 ↗
13. M. Bartning and J. Simpson, Design and Performance of a Non-Contact AF Tester, in SMST 2003: Proceedings of the International Conference on Shape Memory and Superelastic Technologies, A.R. Pelton and T. Duerig, Ed., May 5–8, 2003 (Pacific Grove, CA, USA), SMST, 2004, p 53–58
14. N. Suzaly, M.C. Keller, S. Hügl, T. Lenarz, T.S. Rau, and E. Karsten, Characterization of a Measurement Setup for the Thermomechanical Characterization of Curved Shape Memory Alloy Actuators, Curr. Direct. Biomed. Eng., 2019, 5(1), p 445–44710.1515/cdbme-2019-0112 ↗
15. R. Rizzoni, M. Merlin, and D. Casari, Shape Recovery Behaviour of NiTi Strips in Bending: Experiments and Modelling, Continu. Mech. Thermodyn., 2013, 25(2), p 207–22710.1007/s00161-012-0242-0 ↗
16. MATLAB and Image Processing Toolbox Release 2017b, The MathWorks, Inc., Natick
17. M. Kline, Calculus: An Intuitive and Physical Approach, 2nd ed., Dover, New York, 1998, p 457–461
18. M. Drexel, J. Proft, and S. Russell, Characterization of Transformation Temperatures with the Bend and Free Recovery Technique: Parameters and Effects, J. Mater. Eng. Perform., 2009, 18(5), p 620–62510.1007/s11665-009-9434-6 ↗