journal article·2023-09

Investigation on Microstructure Evolution and Visible-Infrared Property of Vacuum-Heat-Treated TiN Film

Linlin Lu, Jie Xu, Jie Dong, Xiaolei Su, Jia Liu

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Abstract

TiN films were prepared by direct current (DC) reactive magnetron sputtering technique and then vacuum-heat-treated at different temperatures (400, 600 and 800 °C) for 3600 s to improve their properties through increasing the crystallinity and eliminating the lattice defects of the films. Optical properties in the visible-infrared region of TiN films after vacuum heat treatment were investigated. Results revealed that optical reflectance of TiN films first increased and then decreased after the vacuum heat treatment. The reflectance of all the films was below 14%. With the heat treatment temperature rising from 400 to 600 °C, infrared emissivity of TiN films first dropped and then went up at 800 °C. As the heat treatment temperature was 600 °C, the infrared emissivity of TiN films could be reduced to 0.488 and was the lowest. Results showed that vacuum heat treatment could reduce the infrared emissivity of TiN films.
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Research context

OpenAlex topics: Metal and Thin Film Mechanics · GaN-based semiconductor devices and materials · ZnO doping and properties

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (34)

Show source-provided references
1. D. Qi, X. Wang, Y.Z. Cheng, R.Z. Gong, and B.W. Li, Design and Characterization of One-Dimensional Photonic Crystals Based on ZnS/Ge for Infrared-Visible Compatible Stealth Applications, Opt. Mater., 2016, 62, p 52–56.10.1016/j.optmat.2016.09.024 ↗
2. Y. Shen, J.Q. Zhang, Y.Q. Pang, J.F. Wang, H. Ma, and S.B. Qu, Transparent Broadband Metamaterial Absorber Enhanced by Water-Substrate Incorporation, Opt. Express, 2018, 26, p 15665–15674.10.1364/OE.26.015665 ↗
3. C. Ji, Y. Liu, J. Xu, Y.Y. Li, Y.D. Shang, and X.L. Su, Enhanced Microwave Absorption Properties of Biomass-Derived Carbon Decorated with Transition Metal Alloy at Improved Graphitization Degree, J. Alloy. Compd., 2021, 890, p 161834.10.1016/j.jallcom.2021.161834 ↗
4. L.P. Chen, Z.Y. Ren, X.M. Liu, K. Wang, and Q. Wang, Infrared-Visible Compatible Stealth Based on Al-SiO2 Nanoparticle Composite Film, Opt. Commun., 2021, 482, p 126608.10.1016/j.optcom.2020.126608 ↗
5. K.W. Sun, X.F. Tang, C.L. Yang, and D. Jin, Preparation and Performance of Low Emissivityal-Doped ZnO Films for Energy-Saving Glass, Ceram. Int., 2018, 44, p 19597–19602.10.1016/j.ceramint.2018.07.207 ↗
6. M. Yuste, R.E. Galindo, S. Carvalho, J.M. Albella, and O. Sanchez, Improving the Visible Transmittance of Low-E Titanium Nitride Based Coatings for Solar Thermal Applications, Appl. Surf. Sci., 2011, 258, p 1784–1788.10.1016/j.apsusc.2011.10.046 ↗
7. Z.B. Huang, W.C. Zhou, X.Y. Tang, F. Luo, and D.M. Zhou, High-Temperature Application of the Low-Emissivity Au/Ni Films on Alloys, Appl. Surf. Sci., 2010, 256, p 6893–6898.10.1016/j.apsusc.2010.04.107 ↗
8. Z.L. Zhang, A. Ghasemi, N. Koutná, Z. Xu, T. Grünstäudl, K.X. Song, D. Holec, Y.B. He, P.H. Mayrhofer, and M. Bartosik, Correlating Point Defects with Mechanical Properties in Nanocrystalline TiN Thin Films, Mater. Des., 2021, 207, p 109844.10.1016/j.matdes.2021.109844 ↗
9. G. Xian, J. Xiong, H.Y. Fan, F. Jiang, H.B. Zhao, L.J. Xian, and Z.H. Qin, Mechanical and Wear Properties of TiN Films on Differently Pretreated TiCN-Based Cermets, Appl. Surf. Sci., 2021, 570, p 151180.10.1016/j.apsusc.2021.151180 ↗
10. L.L. Lu, F. Luo, Z.B. Huang, W.C. Zhou, and D.M. Zhu, Influence of the Nitrogen Flow Rate on the Infrared Emissivity of TiNx Films, Infrared Phys. Technol., 2018, 88, p 144–148.10.1016/j.infrared.2017.11.015 ↗
11. W.Y. Ge, Z. Chang, A. Siddique, B. Shi, and C. Liu, Large-Area Fabrication of TiN Thin Films with Photothermal Effect via PECVD, Ceram. Int., 2020, 46, p 7355–7361.10.1016/j.ceramint.2019.11.231 ↗
12. S. Khan, S.N. Chen, Y.C. Ma, M. Haq, Y.D. Li, M. Nisar, R. Khan, Y. Liu, J.X. Wang, and G.R. Han, Structural and Hydrophilic Properties of TiN Films Prepared by Ultrasonic Atomization Assisted Spray Method Under Low Temperature, Surf. Coat. Technol., 2020, 393, p 125824.10.1016/j.surfcoat.2020.125824 ↗
13. S. Udaiyappan, P. Kuppusami, R. Ramaseshan, and S. Dhanalakshmi, Structural, Nanomechanical and Electrochemical Properties of TiC and TiN Films Prepared by Pulsed DC Magnetron Sputtering Technique, Mater. Today., 2021, 47, p 1091–1098.10.1016/j.matpr.2021.07.124 ↗
14. S. Chowdhury, R. Gupta, S. Prakash, L. Behera, D.M. Phase, and M. Gupta, Synthesis and Study of Highly Dense and Smooth TiN Thin Films, Mater. Chem. Phys., 2021, 267, p 124648.10.1016/j.matchemphys.2021.124648 ↗
15. H. Liang, J. Xu, D. Zhou, X. Sun, S.C. Chua, and Y.Z. Bai, Thickness Dependent Microstructural and Electrical Properties of TiN Thin Films Prepared by DC Reactive Magnetron Sputtering, Ceram. Int., 2016, 42, p 2642–2647.10.1016/j.ceramint.2015.10.070 ↗
16. M. Maarouf, M.B. Haider, M.F. Al-Kuhaili, A. Aljaafari, and J.Y. Khan, Negative Magnetoresistance in Iron Doped TiN Thin Films Prepared by Reactive Magnetron Sputtering, J. Magn. Magn. Mater., 2020, 514, p 167235.10.1016/j.jmmm.2020.167235 ↗
17. F. Vaz, J. Ferreira, E. Ribeiro, L. Rebouta, S. Lanceros-Méndez, J.A. Mendes, E. Alves, Ph. Goudeau, J.P. Rivière, F. Ribeiro, I. Moutinho, K. Pischow, and J. de Rijk, Influence of Nitrogen Content on the Structural, Mechanical and Electrical Properties of TiN Thin Films, Surf. Coat. Technol., 2005, 191, p 317–323.10.1016/j.surfcoat.2004.01.033 ↗
18. Y.C. Yang, C.H. Tsau, J.W. Yeh, and S.K. Chen, Low-Resistivity Oxides in TixFeCoNi Thin Films After Vacuum Annealing, Surf. Eng., 2018, 34, p 667–673.10.1080/02670844.2017.1373975 ↗
19. L. Radjehi, L. Aissani, A. Djelloul, S. Lamri, K. Nomenyo, S. Achache, G. Lerondel, and F. Sanchette, Effect of Vacuum Annealing on the Structural and Optical Properties of Sputtered Cu4O3 Thin Films, Surf. Eng., 2021, 37, p 422.10.1080/02670844.2020.1753397 ↗
20. B.T. Kearney, B. Jugdersuren, J.C. Culbertson, P.A. Desario, and X. Liu, Substrate and Annealing Temperature Dependent Electrical Resistivity of Sputtered Titanium Nitride Thin Films, Thin Solid Films, 2018, 661, p 78–83.10.1016/j.tsf.2018.07.001 ↗
21. Z. Cheng, H.R. Peng, G.W. Xie, and Y.L. Shi, Annealing Studies of TiN Films Deposited by Plasma-Assisted CVD, Surf. Coat. Technol., 2001, 138, p 237–241.10.1016/S0257-8972(00)01138-5 ↗
22. N.K. Ponon, D.J.R. Appleby, E. Arac, P.J. King, S. Ganti, K.S.K. Kwa, and A. O’Neill, Effect of Deposition Conditions and Post Deposition Anneal on Reactively Sputtered Titanium Nitride Thin Films, Thin Solid Films, 2015, 578, p 31–37.10.1016/j.tsf.2015.02.009 ↗
23. Y.X. Xi, H.Q. Fan, and W.G. Liu, The Effect of Annealing Treatment on Microstructure and Properties of TiN Films Prepared by Unbalanced Magnetron Sputtering, J. Alloy. Compd., 2010, 496, p 695–698.10.1016/j.jallcom.2010.02.176 ↗
24. J. Pelleg, L.Z. Zevin, S. Lungo, and N. Croitoru, Reactive-Sputter-Deposited TiN Films on Glass Substrates, Thin Solid Films, 1991, 197, p 117–128.10.1016/0040-6090(91)90225-M ↗
25. U.C. Oh and J.H. Je, Effects of Strain Energy on the Preferred Orientation of TiN Thin Films, J. Appl. Phys., 1993, 74, p 1692.10.1063/1.355297 ↗
26. H.L. Liang, J. Xu, D.Y. Zhou, X. Sun, S.C. Chu, and Y.Z. Bai, Thickness Dependent Microstructural and Electrical Properties of TiN Thin Films Prepared by DC Reactive Magnetron Sputtering, Ceram. Int., 2016, 42, p 2642–2647.10.1016/j.ceramint.2015.10.070 ↗
27. S.K. Mishra, R. Kumar, M. Soni, L.C. Sreemany, and Pathak, Ultrathin to Nano Thickness TiN Coatings: Processing, Structural, Mechanical Behavior, J. Mater. Eng. Perform., 2015, 24, p 5013–5021.10.1007/s11665-015-1754-0 ↗
28. C. Gebauer, P. Fischer, M. Wassner, T. Diemant, Z. Jusys, N. Husing, and R.J. Behm, Performance of Titanium Oxynitrides in the Electrocatalytic Oxygen Evolution Reaction, Nano Energy, 2016, 29, p 136–148.10.1016/j.nanoen.2016.05.034 ↗
29. P. Osiceanu, An XPS Study on Ion Beam Induced Oxidation of Titanium Silicide, Appl. Surf. Sci., 2006, 253, p 381–384.10.1016/j.apsusc.2006.06.018 ↗
30. S. Logothetidis, E.I. Meletis, G. Stergioudis, and A.A. Adjaottor, Room Temperature Oxidation Behavior of TiN Thin Films, Thin Solid Films, 1999, 338, p 304–313.10.1016/S0040-6090(98)00975-4 ↗
31. L.Y. Sheng, Y.N. Xiao, C. Jiao, B.N. Du, Y.M. Li, Z.Z. Wu, and L.Q. Shao, Influence of Layer Number on Microstructure, Mechanical Properties and Wear Behavior of the TiN/Ti Multilayer Coatings Fabricated by High-Power Magnetron Sputtering Deposition, J. Manuf. Process., 2021, 70, p 529.10.1016/j.jmapro.2021.09.002 ↗
32. A. Mumtaz and W.H. Class, Color of Titanium Nitride Prepared by Reactive dc Magnetron Sputtering, J. Vac. Sci. Technol., 1982, 20, p 345–348.10.1116/1.571461 ↗
33. N. Kumar, J.T. Mcginn, K. Pourrezaei, B. Lee, and E.C. Douglas, Transmission Electron Microscopy Studies of Brown and Golden Titanium Nitride Thin Films as Diffusion Barriers in Very Largescale Integrated Circuits, J. Vac. Sci. Technol. A, 1988, 6, p 1602–1608.10.1116/1.575335 ↗
34. Z.M. Zhang, X.H. Wu, and C.J. Fu, Validity of Kirchhoff’s Law for Semitransparent Films Made of Anisotropic Materials, J. Quant. Spectrosc. Radiat., 2020, 245, p 106904.10.1016/j.jqsrt.2020.106904 ↗