journal article·2022-03

Precipitation Behavior and Strengthening Mechanism of Extruded 2196 Al-Cu-Li Alloy Plate during Multi-Step Age-Hardening Treatment

Xiaoxue Chen, Haotian Zhang, Guoqun Zhao

Publisher page

Abstract

In order to reveal the precipitation behavior and strengthening mechanism of extruded 2196 Al-Cu-Li alloy plate during aging treatment, one-step and two-step age-hardening treatment with different temperatures and time were conducted. According to the mechanical property tests and microstructure observation, it was found that the strengthening effect of two-step age-hardening treatment is better than that of one-step aging, and the plasticity of the alloy is also improved. This is because the Guinier–Preston zones precipitated during low-temperature pre-aging can provide nucleation particles for T1 phases in the second-stage aging process, thus promoting the uniform precipitation of fine acicular T1 phases. In addition, the size of θ' phase and grain boundary precipitates in the two-step aged alloy is small, and the width of precipitated free zone is also narrow, which promotes the improvement of mechanical properties of the plate. The optimal two-step age-hardening treatment of 2196 alloy is finally determined as 125 °C×8 h+165 °C×32 h, the yield stress reached 455 MPa, and the fracture mechanism of the corresponding alloy shows a combination of intergranular fracture and cleavage fracture.
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Aluminum Alloy Microstructure Properties · Aluminum Alloys Composites Properties · Metallurgy and Material Forming

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (34)

Show source-provided references
1. R.K. Gupta, N. Nayan, G. Nagasireesha and S.C. Sharma, Development and Characterization of Al–Li Alloys, Mater. Sci. Eng. A, 2006, 420, p 228–234.10.1016/j.msea.2006.01.045 ↗
2. R.J. Rioja and J. Liu, The Evolution of Al-Li Base Products for Aerospace and Space Applications, Metall. Mater. Trans. A, 2012, 43A, p 3325–3337.10.1007/s11661-012-1155-z ↗
3. J.C. Williams and E.A. Starke Jr., Progress in Structural Materials for Aerospace Systems, Acta Mater., 2003, 51, p 5775–5799.10.1016/j.actamat.2003.08.023 ↗
4. A.A. El-Aty, Y. Xu, X.Z. Guo, S.H. Zhang, Y. Ma and D.Y. Chen, Strengthening Mechanisms, Deformation Behavior, and Anisotropic Mechanical Properties of Al-Li Alloys: A Review, J. Adv. Res., 2018, 10, p 49–67.10.1016/j.jare.2017.12.004 ↗
5. Y.X. Wang and G.Q. Zhao, Hot Extrusion Processing of Al–Li Alloy Profiles and Related Issues: A Review, Chin. J. Mech. Eng., 2020, 33, p 64.10.1186/s10033-020-00479-7 ↗
6. X.S. Zhang, Y.J. Chen and J.L. Hu, Recent Advances in the Development of Aerospace Materials, Prog. Aerosp. Sci., 2018, 97, p 22–34.10.1016/j.paerosci.2018.01.001 ↗
7. A. Medjahed, A. Henniche, M. Derradji, T.F. Yu, Y. Wang, R.Z. Wu, L.G. Hou, J.H. Zhang, X.L. Li and M.L. Zhang, Effects of Cu/Mg Ratio on the Microstructure, Mechanical and Corrosion Properties of Al-Li-Cu-Mg-X Alloys, Mater. Sci. Eng. A, 2018, 718, p 241–249.10.1016/j.msea.2018.01.118 ↗
8. P. Donnadieu, Y. Shao, F.D. Geuser, G.A. Botton, S. Lazar, M. Cheynet, M.D. Boissieu and A. Deschamps, Atomic Structure of T1 Precipitates in Al–Li–Cu Alloys Revisited with HAADF-STEM Imaging and Small-Angle X-ray Scattering, Acta Mater., 2011, 59, p 462–472.10.1016/j.actamat.2010.09.044 ↗
9. E. Gumbmann, F.D. Geuser, C. Sigli and A. Deschamps, Influence of Mg, Ag and Zn Minor Solute Additions on the Precipitation Kinetics and Strengthening of an Al-Cu-Li Alloy, Acta Mater., 2017, 133, p 172–185.10.1016/j.actamat.2017.05.029 ↗
10. X.L. Zhang, L. Zhang, G.H. Wu, J.W. Sun, M. Rong, C.C. Hsieh and Y.X. Yu, Influence of Sc Content on the Microstructure and Mechanical Properties of Cast Al-2Li-2Cu-0.5Mg-0.2Zr Alloy, Mater. Charact., 2018, 142, p 223–236.10.1016/j.matchar.2018.05.046 ↗
11. J.W. Sun, G.H. Wu, L. Zhang, X.L. Zhang, L.L. Liu and J.S. Zhang, Microstructure Characteristics of an Ultra-high Strength Extruded Al-4.7Cu-1Li-0.5Mg-0.1Zr-1Zn Alloy During Heat Treatment, J. Alloys Compd., 2020, 813, p 152216.10.1016/j.jallcom.2019.152216 ↗
12. J.S. Tao, L. Zhang, G.H. Wu, A.T. Chen, X.L. Zhang and C.C. Shi, Effect of Heat Treatment on the Microstructure and Mechanical Properties of Extruded Al–4Cu–1Li–0.4Mg–0.4Ag–0.18Zr Alloy, Mater. Sci. Eng. A, 2018, 717, p 11–19.10.1016/j.msea.2018.01.063 ↗
13. A. Hekmat-Ardakan, E.M. Elgallad, F. Ajersch and X.G. Chen, Microstructural Evolution and Mechanical Properties of As-Cast and T6-Treated AA2195 DC Cast Alloy, Mater. Sci. Eng. A, 2012, 558, p 76–81.10.1016/j.msea.2012.07.075 ↗
14. J.J. Xu, Y.L. Deng, J.Q. Chen, Y.K. Xie and X.B. Guo, Effect of Ageing Treatments on the Precipitation Behavior and Mechanical Properties of Al–Cu–Li Alloys, Mater. Sci. Eng. A, 2020, 773, p 138885.10.1016/j.msea.2019.138885 ↗
15. M. Suresh, R. Kalsar, A.M. More, A. Bisht, N. Nayan and S. Suwas, Evolution of Microstructure and Texture in the Third Generation Al-Li Alloy AA2195 During Warm Hybrid Processing, J. Alloys Compd., 2021, 855, p 156750.10.1016/j.jallcom.2020.156750 ↗
16. Y.X. Wang, X.W. Ma, H.K. Xi, G.Q. Zhao, X. Xu and X.X. Chen, Effects of Pre-stretching and Aging Treatments on Microstructure, Mechanical Properties, and Corrosion Behavior of Spray-Formed Al-Li Alloy 2195, J. Mater. Eng. Perform., 2020, 29, p 6960–6973.10.1007/s11665-020-05142-9 ↗
17. H.Y. Li, D.S. Huang, W. Kang, J.J. Liu, Y.X. Ou and D.W. Li, Effect of Different Aging Processes on the Microstructure and Mechanical Properties of a Novel Al–Cu–Li Alloy, J. Mater. Sci. Technol., 2016, 32, p 1049–1053.10.1016/j.jmst.2016.01.018 ↗
18. S.F. Zhang, W.D. Zeng, W.H. Yang, C.L. Shi and H.J. Wang, Ageing Response of a Al–Cu–Li 2198 Alloy, Mater. Des., 2014, 63, p 368–374.10.1016/j.matdes.2014.04.063 ↗
19. F.S. Qureshi, A.K. Sheikh and M. Rashid, A Mathematical Model to Predict the Strength of Aluminum Alloys Subjected to Precipitation Hardening, J. Mater. Eng. Perform., 1999, 29, p 353–360.10.1361/105994999770346918 ↗
20. T. Dorin, F.D. Geuser, W. Lefebvre, C. Sigli and A. Deschamps, Strengthening Mechanisms of T1 Precipitates and Their Influence on the Plasticity of an Al–Cu–Li Alloy, Mater. Sci. Eng. A, 2014, 605, p 119–126.10.1016/j.msea.2014.03.024 ↗
21. X.H. Zhu, Y.C. Lin, Q. Wu and Y.Q. Jiang, Effects of Aging on Precipitation Behavior and Mechanical Properties of a Tensile Deformed Al-Cu Alloy, J. Alloys Compd., 2020, 843, p 155975.10.1016/j.jallcom.2020.155975 ↗
22. Y.Z. Hou, L. Chen, Z.G. Li, G.Q. Zhao and C.S. Zhang, Effects of Artificial Aging on Microstructure, Mechanical Properties and Stress Corrosion Cracking of a Novel High Strength 7A99 Al alloy, Mater. Sci. Eng. A, 2020, 780, p 139217.10.1016/j.msea.2020.139217 ↗
23. Y. Lin, C. Lu, C.Y. Wei and Z.Q. Zheng, Effect of Aging Treatment on Microstructures, Tensile Properties and Intergranular Corrosion Behavior of Al–Cu–Li Alloy, Mater. Charact., 2018, 141, p 163–168.10.1016/j.matchar.2018.04.043 ↗
24. N. Nayan, S.V.S.N. Murty, A.K. Jha, B. Pant, S.C. Sharma, K.M. George and G.V.S. Sastry, Processing and Characterization of Al–Cu–Li Alloy AA2195 Undergoing Scale up Production Through the Vacuum Induction Melting Technique, Mater. Sci. Eng. A, 2013, 576, p 21–28.10.1016/j.msea.2013.03.054 ↗
25. X.X. Chen, X.W. Ma, H.K. Xi, G.Q. Zhao, Y.X. Wang and X. Xu, Effects of Heat Treatment on the Microstructure and Mechanical Properties of Extruded 2196 Al-Cu-Li Alloy, Mater. Des., 2020, 192, p 108746.10.1016/j.matdes.2020.108746 ↗
26. A. Deschamps, M. Garcia, J. Chevy, B. Davo and F.D. Geuser, Influence of Mg and Li Content on the Microstructure Evolution of Al-Cu-Li Alloys During Long-Term Ageing, Acta Mater., 2017, 122, p 32–46.10.1016/j.actamat.2016.09.036 ↗
27. R. Yoshimura, T.J. Konno, E. Abe and K. Hiraga, Transmission Electron Microscopy Study of the Early Stage of Precipitates in Aged Al–Li–Cu Alloys, Acta Mater., 2003, 51, p 2891–2903.10.1016/S1359-6454(03)00104-6 ↗
28. M. Romios, R. Tiraschi, C. Parrish, H.W. Babel, J.R. Ogren and O.S. Es-Said, Design of Multistep Aging Treatments of 2099 (C458) Al-Li Alloy, J. Mater. Eng. Perform., 2005, 14, p 641–646.10.1361/105994905X64594 ↗
29. B. Decreus, A. Deschamps, F.D. Geuser, P. Donnadieu, C. Sigli and M. Weyland, The Influence of Cu/Li Ratio on Precipitation in Al-Cu-Li-x Alloys, Acta Mater., 2013, 61, p 2207–2218.10.1016/j.actamat.2012.12.041 ↗
30. X.L. Zhang, L. Zhang, G.H. Wu, W.C. Liu, C.C. Shi, J.S. Tao and J.W. Sun, Microstructural Evolution and Mechanical Properties of Cast Al-2Li-2Cu-0.5Mg-0.2Zr Alloy During Heat Treatment, Mater. Charact., 2017, 132, p 312–319.10.1016/j.matchar.2017.08.027 ↗
31. Z. Gao, J.Z. Liu, J.H. Chen, S.Y. Duan, Z.R. Liu, W.Q. Ming and C.L. Wu, Formation Mechanism of Precipitate T1 in AlCuLi Alloys, J. Alloys Compd., 2015, 624, p 22–26.10.1016/j.jallcom.2014.10.208 ↗
32. P. Khanikar, Y. Liu and M.A. Zikry, Experimental and Computational Investigation of the Dynamic Behavior of Al–Cu–Li Alloys, Mater. Sci. Eng. A, 2014, 604, p 67–77.10.1016/j.msea.2014.02.089 ↗
33. Y. Lin, Z.Q. Zheng, S.C. Li, X. Kong and Y. Han, Microstructures and Properties of 2099 Al-Li Alloy, Mater. Charact., 2013, 84, p 88–99.10.1016/j.matchar.2013.07.015 ↗
34. E. Balducci, L. Ceschini, S. Messieri, S. Wenner and R. Holmestad, Thermal Stability of the Lightweight 2099 Al-Cu- Li Alloy: Tensile Tests and Microstructural Investigations after Overaging, Mater. Des., 2017, 119, p 54–64.10.1016/j.matdes.2017.01.058 ↗