journal article·2020-08

Effects of Temperature and Time on Microstructural Evolution of Semisolid 5A06 Aluminum Alloy: Preparation of Semisolid Billets in Ellipsoid Solid Phase

Jufu Jiang, Yingze Liu, Guanfei Xiao, Ying Wang, Xinquan Xiao

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Abstract

To shorten the semisolid billet process and reduce its cost, the effects of isothermal temperature and soaking time on the microstructural evolution and coarsening rate during directly heating room temperature hot-rolled 5A06 aluminum alloy to semisolid temperature were investigated. Samples cut from the hot-rolled plates were heated to semisolid temperatures ranging from 580 to 620 °C, and soaking for 5-30 min. The microstructure of samples was characterized by optical microscopy, scanning electron microscopy with energy-dispersive x-ray spectroscopy, and Image-Pro Plus software. The results showed that the microstructure contained ellipsoidal solid grains with the quantitative parameters of the average grain size of 143 µm and averaged shape factor of 0.55 under an optimal condition of 615 °C for 20 min. Recrystallization occurred within 5 min of holding time, increasing temperature can promote recrystallization, which is beneficial to spheroidization of solid phase, and it will also accelerate melting and the growth of solid particles. Extending soaking time, the liquid phase increased gradually and the change of solid particles was complicated. Abnormal accumulation of liquid phase was found, which will lead to the formation of irregular structure. The reasonable coarsening rate constants ranged from 1319 to 3454 μm3 s−1 under the desired treatment parameters. The segregation of Mg occurred at the grain boundaries, as well as around the inclusions within the grains.
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Research context

OpenAlex topics: Aluminum Alloy Microstructure Properties · Aluminum Alloys Composites Properties · Microstructure and mechanical properties

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References (43)

Show source-provided references
1. D.B. Spencer, R. Mehrabian, and M.C. Flemings, Rheological Behavior of Sn-15 pct Pb in the Crystallization Range, Metall. Trans., 1972, 3, p 1925–1932. https://doi.org/10.1007/BF0264258010.1007/BF02642580 ↗
2. M.C. Flemings, Behavior of Metal Alloys in the Semisolid State, Metall. Trans., 1991, 22, p 269–293. https://doi.org/10.1007/BF0265122710.1007/BF02651227 ↗
3. S. Janudom, J. Wannasin, J. Basem, and S. Wisumethangoon, Characterization of Flow Behavior of Semi-solid Slurries Containing Low Solid Fractions in High-pressure Die Casting, Acta Mater., 2013, 61, p 6267–6275. https://doi.org/10.1016/j.actamat.2013.07.01010.1016/j.actamat.2013.07.010 ↗
4. D. Liu, H.V. Atkinson, P. Kapranos, and H. Jones, Effect of Heat Treatment on Properties of Thixoformed High Performance 2014 and 201 Aluminium Alloys, J. Mater. Sci., 2004, 39, p 99–105. https://doi.org/10.1023/B:JMSC.0000007732.04363.8110.1023/B:JMSC.0000007732.04363.81 ↗
5. C.G. Kang, S.M. Lee, and B.M. Kim, A Study of Die Design of Semi-solid Die Casting According to Gate Shape and Solid Fraction, J. Mater. Process. Technol., 2008, 204, p 8–21. https://doi.org/10.1016/j.jmatprotec.2008.01.03810.1016/j.jmatprotec.2008.01.038 ↗
6. D.G. Eskin and L. Katgerman, Mechanical Properties in the Semi-solid State and Hot Tearing of Aluminium Alloys, Prog. Mater Sci., 2004, 49, p 629–711. https://doi.org/10.1016/S0079-6425(03)00037-910.1016/S0079-6425(03)00037-9 ↗
7. K.N. Li, Y.B. Zhang, Q. Zeng, G.H. Huang, B. Ji, and D.D. Yin, Effects of Semisolid Treatment and ECAP on the Microstructure and Mechanical Properties of Mg-6.52Zn-0.95Y Alloy with Icosahedral Phase, Mater. Sci. Eng. A, 2019, 751, p 283–291. https://doi.org/10.1016/j.msea.2019.02.08310.1016/j.msea.2019.02.083 ↗
8. Y. Wang, S. Zhao, and C. Zhang, Microstructures and Mechanical Properties of Semi-solid Squeeze Casting ZL104 Connecting Rod, Trans. Nonferrous Met. Soc. China, 2018, 28, p 235–243. https://doi.org/10.1016/S1003-6326(18)64656-410.1016/S1003-6326(18)64656-4 ↗
9. M. Cao, Z. Wang, and Q. Zhang, Microstructure-Dependent Mechanical Properties of Semi-solid Copper Alloys, J. Alloys Compd., 2017, 715, p 413–420. https://doi.org/10.1016/j.jallcom.2017.03.36010.1016/j.jallcom.2017.03.360 ↗
10. G. Xiao, J. Jiang, Y. Wang, Y. Liu, and Y. Zhang, Microstructure and Mechanical Properties of Nickel-Based Superalloy GH4037 Parts Formed by Thixoforming, Mater. Sci. Eng. A (2020) 780, Article 139196. https://doi.org/10.1016/j.msea.2020.13919610.1016/j.msea.2020.139196 ↗
11. M.S. Salleh, M.Z. Omar, J. Syarif, and M.N. Mohammed, An Overview of Semisolid Processing of Aluminium Alloys, ISRN Mater. Sci., 2013, 5, p 1–9. https://doi.org/10.1155/2013/67982010.1155/2013/679820 ↗
12. K.P. Young, C.P. Kyonka, and J.A. Fine Grained Metal Composition. US Patent, No. 4415374, 1982.
13. D.H. Kirkwood, C.M. Sellars, and L.G. Eliasboyed, Thixotropic Materials, US Patent, No. 5037489, 1991.
14. M. Kiuchi and R. Kopp, Mushy/Semi-solid Metal Forming Technology—Present and Future, CIRP Ann. Manuf. Technol., 2002, 51, p 653–670. https://doi.org/10.1016/S0007-8506(07)61705-310.1016/S0007-8506(07)61705-3 ↗
15. A. Bolouri, M. Shahmiri, and C.G. Kang, Coarsening of Equiaxed Microstructure in the Semisolid State of Aluminum 7075 Alloy Through SIMA Processing, J. Mater. Sci., 2012, 47, p 3544–3553. https://doi.org/10.1007/s10853-011-6200-610.1007/s10853-011-6200-6 ↗
16. J. Jiang, Y. Wang, X. Xiao, and X. Nie, Comparison of Microstructural Evolution of 7075 Aluminum Alloy Fabricated by SIMA and RAP, J. Mater. Process. Technol., 2016, 238, p 361–372. https://doi.org/10.1016/j.jmatprotec.2016.06.02010.1016/j.jmatprotec.2016.06.020 ↗
17. H.V. Atkinson and D. Liu, Coarsening Rate of Microstructure in Semi-solid Aluminium Alloys, Trans. Nonferrous Met. Soc. China, 2010, 20, p 1672–1676. https://doi.org/10.1016/S1003-6326(09)60356-310.1016/S1003-6326(09)60356-3 ↗
18. A. Bolouri, M. Shahmiri, and C.G. Kang, Study on the Effects of the Compression Ratio and Mushy Zone Heating on the Thixotropic Microstructure of AA 7075 Aluminum Alloy via SIMA Process, J. Alloys Compd., 2011, 509, p 402–408. https://doi.org/10.1016/j.jallcom.2010.09.04210.1016/j.jallcom.2010.09.042 ↗
19. J. Fu, S. Wang, and K. Wang, Influencing Factors of the Coarsening Behaviors for 7075 Aluminum Alloy in the Semi-solid State, J. Mater. Sci., 2018, 53, p 9790–9805. https://doi.org/10.1007/s10853-018-2246-z10.1007/s10853-018-2246-z ↗
20. J. Jiang and S. Luo, Reheating Microstructure of Refined AZ91D Magnesium Alloy in Semi-solid State, Trans. Nonferrous Met. Soc. China, 2004, 14, p 1074–1081
21. J. Jiang, Y. Wang, J. Qu, Z. Du, Y. Sun, and S. Luo, Microstructure Evolution of AM60 Magnesium Alloy Semisolid Slurry Prepared by New SIMA, J. Alloys Compd., 2010, 497, p 62–67. https://doi.org/10.1016/j.jallcom.2010.02.09910.1016/j.jallcom.2010.02.099 ↗
22. B. Binesh and M. Aghaie-Khafri, RUE-based Semi-solid Processing: Microstructure Evolution and Effective Parameters, Mater. Des., 2016, 95, p 268–286. https://doi.org/10.1016/j.matdes.2016.01.11710.1016/j.matdes.2016.01.117 ↗
23. M. Cao, Q. Zhang, and Y. Zhang, Effects of Plastic Energy on Thixotropic Microstructure of C5191 Alloys During SIMA Process, J. Alloys Compd., 2017, 721, p 220–228. https://doi.org/10.1016/j.jallcom.2017.05.24510.1016/j.jallcom.2017.05.245 ↗
24. Y. Wang, S. Zhao, and C. Zhang, Microstructural Evolution of Semisolid 6063 Aluminum Alloy Prepared by Recrystallization and Partial Melting Process, J. Mater. Eng. Perform., 2017, 26, p 4354–4363. https://doi.org/10.1007/s11665-017-2854-910.1007/s11665-017-2854-9 ↗
25. C.P. Chen and C.-Y.A. Tsao, Semi-solid Deformation of Non-dendritic Structures—I. Phenomenological Behavior, Acta Mater., 1997, 45, p 1955–1968. https://doi.org/10.1016/S1359-6454(96)00312-610.1016/S1359-6454(96)00312-6 ↗
26. E. Tzimas and A. Zavaliangos, Mechanical Behavior of Alloys with Equiaxed Microstructure in the Semisolid State at High Solid Content, Acta Mater., 1999, 47, p 517–528. https://doi.org/10.1016/S1359-6454(98)00356-510.1016/S1359-6454(98)00356-5 ↗
27. E.O. Hall, The Deformation and Ageing of Mild Steel: II, Characteristics of the Lüders Deformation, Proc. Phys. Soc. B, 1951, 64, p 747–753. https://doi.org/10.1088/0370-1301/64/9/30210.1088/0370-1301/64/9/302 ↗
28. N.J. Petch, The Cleavage Strength of Polycrystals, J. Iron Steel Inst., 1953, 174, p 25–28. https://doi.org/10.1016/0001-6160(53)90043-110.1016/0001-6160(53)90043-1 ↗
29. J. Jiang, Y. Liu, G. Xiao, Y. Wang, and X. Xiao, Effects of plastic deformation of solid phase on mechanical properties and microstructure of wrought 5A06 aluminum alloy in directly semisolid thixoforging, J. Alloys Compd. (2020) 831, Article 154748. https://doi.org/10.1016/j.jallcom.2020.15474810.1016/j.jallcom.2020.154748 ↗
30. O. Engler, K. Kuhnke, and J. Hasenclever, Development of Intermetallic Particles During Solidification and Homogenization of two AA 5xxx Series Al-Mg Alloys with Different Mg CONTENTS, J. Alloys Compd., 2017, 728, p 669–681. https://doi.org/10.1016/j.jallcom.2017.09.06010.1016/j.jallcom.2017.09.060 ↗
31. G. Peng, L. Li, J. Wang, H. Xia, S. Meng, J. Gong, Effect of subatmospheric pressures on weld formation and mechanical properties during disk laser welding of 5A06 aluminium alloy, J. Mater. Process. Technol. (2020) 277, Article 116457. https://doi.org/10.1016/j.jmatprotec.2019.11645710.1016/j.jmatprotec.2019.116457 ↗
32. Z. Wang, J.P. Oliveira, Z. Zeng, X. Bu, B. Peng, and X. Shao, Laser Beam Oscillating Welding of 5A06 Aluminum Alloys: Microstructure, Porosity and Mechanical Properties, Opt. Laser Technol., 2019, 111, p 58–65. https://doi.org/10.1016/j.optlastec.2018.09.03610.1016/j.optlastec.2018.09.036 ↗
33. N. Guo, Y. Fu, Y. Wang, Q. Meng, and Y. Zhu, Microstructure and mechanical properties in friction stir welded 5A06 aluminum alloy thick plate, Mater. Des., 2017, 113, p 273–283. https://doi.org/10.1016/j.matdes.2016.10.03010.1016/j.matdes.2016.10.030 ↗
34. N. Saklakoglu, I.E. Saklakoglu, M. Tanoglu, O. Oztas, and O. Cubukcuoglu, Mechanical Properties and Microstructural Evaluation of AA5013 Aluminum Alloy Treated in the Semi-solid State by SIMA Process, J. Mater. Process. Technol., 2004, 148, p 103–107. https://doi.org/10.1016/j.jmatprotec.2004.01.05110.1016/j.jmatprotec.2004.01.051 ↗
35. J. Jiang, G. Xiao, Y. Wang, and Y. Qi, Microstructure Evolution of Wrought Nickel Based Superalloy GH4037 in the Semi-solid State, Mater. Charact., 2018, 141, p 229–237. https://doi.org/10.1016/j.matchar.2018.04.05710.1016/j.matchar.2018.04.057 ↗
36. D. Zhang, H. Dong, and H.V. Atkinson, What is the Process Window for Semi-solid Processing?, Metall. Mater. Trans. A, 2016, 47(1), p 1–5. https://doi.org/10.1007/s11661-015-3185-910.1007/s11661-015-3185-9 ↗
37. Y. Wang, X. Zhao, and Y. Zhao, Microstructural Coarsening of 6061 Aluminum Alloy Semi-solid Billets Prepared via Recrystallization and Partial Melting, J. Mech. Sci. Technol., 2017, 31, p 3917–3923. https://doi.org/10.1007/s12206-017-0737-510.1007/s12206-017-0737-5 ↗
38. E. Tzimas and A. Zavaliangos, Evolution of Near-equiaxed Microstructure in the Semisolid State, Mater. Sci. Eng. A, 2000, 289, p 228–240. https://doi.org/10.1016/S0921-5093(00)00908-410.1016/S0921-5093(00)00908-4 ↗
39. J. Jiang, Y. Wang, and H.V. Atkinson, Microstructural Coarsening of 7005 Aluminum Alloy Semisolid Billets with High Solid Fraction, Mater. Charact., 2014, 90, p 52–61. https://doi.org/10.1016/j.matchar.2014.01.01710.1016/j.matchar.2014.01.017 ↗
40. I.M. Lifshitz and V.V. Slyozov, The Kinetics of Precipitation from Supersaturated Solid Solutions, J. Phys. Chem. Solids, 1961, 19, p 35–50. https://doi.org/10.1016/0022-3697(61)90054-310.1016/0022-3697(61)90054-3 ↗
41. C. Wagner, Theory of the Ageing of Precipitates by Redissolution (Ostwald Maturing), Electrochemistry, 1961, 65, p 581–591
42. S. Zabler, A. Rueda, A. Rack, H. Riesemeier, P. Zaslansky, I. Manke, F. Garcia-Morenod, and J. Banhart, Coarsening of Grain-Refined Semi-solid Al-Ge32 Alloy: X-ray Microtomography and In Situ Radiography, Acta Mater., 2007, 55, p 5045–5055. https://doi.org/10.1016/j.actamat.2007.05.02810.1016/j.actamat.2007.05.028 ↗
43. O. Engler and S. Miller-Jupp, Control of Second-Phase Particles in the Al-Mg-Mn Alloy AA 5083, J. Alloys Compd., 2016, 689, p 998–1010. https://doi.org/10.1016/j.jallcom.2016.08.07010.1016/j.jallcom.2016.08.070 ↗