journal article·2022-01

Effect of Heat Treatment on the Microstructure and Properties of Inconel 718 Alloy Fabricated by Selective Laser Melting

Rongxia Zhao, Zhanyong Zhao, Peikang Bai, Wenbo Du, Lizheng Zhang, Hongqiao Qu

Publisher page

Abstract

Inconel 718 alloy was fabricated by selective laser melting (SLM) and treated with different solutions and two-stage aging heat treatments (H1-H4). The microstructure evolution of the alloy under four different heat treatments was analyzed, and the influence of the size and quantity of precipitates on the mechanical properties of the alloy under different aging mechanisms was explored. The results showed that after solution treatment at 1020 °C, the structural segregation at the boundaries of columnar and equiaxed crystals disappeared, the Nb-rich Laves phase and carbides were dissolved into the matrix. After aging treatment, γ′ and γ″ strengthening phases were precipitated in the matrix, and the fine needle-like γ″ phase was uniformly distributed, which played the role of dispersion strengthening and significantly improved the strength of the alloy. Under the double aging system of 720 °C + 620 °C (H4), the average size of precipitates was 26.47 nm, and the properties of the alloy tend to be isotropic. After H4 heat-treated, the σUTS and σ0.2 of the sample reached 1520 MPa and 1272 MPa, respectively. There was no obvious fracture and spalling on the worn surface of the alloy, thus it showed good friction and wear resistance. At the same time, it was proved that the temperature change at the first stage of double aging had a greater influence on the precipitation of the strengthening phase than that at the second stage.
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Additive Manufacturing Materials and Processes · High Entropy Alloys Studies · Additive Manufacturing and 3D Printing Technologies

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (39)

Show source-provided references
1. A. Chamanfar, L. Sarrat, M. Jahazi, M. Asadi, A. Weck and A.K. Koul, Microstructural Characteristics of Forged and Heat Treated Inconel-718 Disks, Mater. Des., 2013, 52, p 791–800.10.1016/j.matdes.2013.06.004 ↗
2. L.E. Murr, S.M. Gaytan, D.A. Ramirez, E. Martinez, J. Hernandez, K.N. Amato, P.W. Shindo, F.R. Medina and R.B. Wicker, Metal Fabrication by Additive Manufacturing Using Laser and Electron Beam Melting Technologies, Mater. Sci. Technol., 2012, 28, p 1–14.10.1016/S1005-0302(12)60016-4 ↗
3. D.D. Gu, W. Meiners, K. Wissenbach and R. Poprawe, Laser Additive Manufacturing of Metallic Components: Materials, Processes and Mechanisms, Int. Mater. Rev., 2012, 57(3), p 133–164.10.1179/1743280411Y.0000000014 ↗
4. T. DebRoy, H.L. Wei, J.S. Zuback, T. Mukherjee, J.W. Elmer, J.O. Milewski, A.M. Beese, A. Wilson-Heid, A. De and W. Zhang, Additive Manufacturing of Metallic Components – Process, Structure and Properties, Mater. Sci., 2018, 92, p 112–224.
5. D. Herzog, V. Seyda, E. Wycisk and C. Emmelmann, Additive Manufacturing of Metals, Acta Mater., 2016, 117, p 371–392.10.1016/j.actamat.2016.07.019 ↗
6. E.C. Santos, M. Shiomi, K. Osakada and T. Laoui, Rapid Manufacturing of Metal Components by Laser Forming, Int. J. Mach. Tools Manuf., 2006, 46, p 1459–1468.10.1016/j.ijmachtools.2005.09.005 ↗
7. I. Yadroitsev and I. Smurov, Selective Laser Melting Technology: From the Single Laser Melted Track Stability to 3D Parts of Complex Shape, Phys. Procedia, 2010, 5, p 551–560.10.1016/j.phpro.2010.08.083 ↗
8. M. Ni, C. Chen, X. Wang, P. Wang, R. Li, X. Zhang and K. Zhou, Anisotropic Tensile Behavior of In Situ Precipitation Strengthened Inconel 718 Fabricated by Additive Manufacturing, Mater. Sci. Eng., 2017, 701, p 344–351.10.1016/j.msea.2017.06.098 ↗
9. K.N. Amato, S.M. Gaytan, L.E. Murr, E. Martinez, P.W. Shindo, J. Hernandez, S. Collins and F. Medina, Microstructures and Mechanical Behavior of Inconel 718 Fabricated by Selective Laser Melting, Acta Mater., 2012, 60, p 2229–2239.10.1016/j.actamat.2011.12.032 ↗
10. C.M. Kuo, Y.T. Yang, H.Y. Bor, C.N. Wei and C.C. Tai, Aging Effects on the Microstructure and Creep Behavior of Inconel 718 Superalloy, Mater. Sci. Eng. A, 2009, 510, p 289–294.10.1016/j.msea.2008.04.097 ↗
11. J. Zhang, J. Gao, B. Song, L. Zhang, C. Han, C. Cai, K. Zhou and Y. Shi, A Novel Crack-Free Ti-Modified Al-Cu-Mg Alloy Designed for Selective Laser Melting, Addit. Manuf., 2021, 38, p 101829.
12. K. Kulawik, P.A. Buffat, A. Kruk, A.M. Wusatowska-Sarnek and A. Czyrska-Filemonowicz, Imaging and Characterization of γ′ and γ″ Nanoparticles in Inconel 718 by EDX Elemental Mapping and FIB–SEM Tomography, Mater. Charact., 2015, 100, p 74–80.10.1016/j.matchar.2014.12.012 ↗
13. Z.Y. Zhao, R.G. Guan, Y.F. Shen and P.K. Bai, Grain Refinement Mechanism of Mg-3Sn-1Mn-1La Alloy During Accumulative Hot Rolling, J. Mater. Sci. Technol., 2021, 91, p 251–261.10.1016/j.jmst.2021.02.052 ↗
14. Y. Lu, S. Wu, Y. Gan, T. Huang, C. Yang, L. Junjie and J. Lin, Study on the Microstructure, Mechanical Property and Residual Stress of SLM Inconel-718 Alloy Manufactured by Differing Island Scanning Strategy, Opt. Laser Technol., 2015, 75, p 197–206.10.1016/j.optlastec.2015.07.009 ↗
15. V.A. Popovich, E.V. Borisov, A.A. Popovich, V.S. Sufiiarov, D.V. Masaylo and L. Alzina, Functionally Graded Inconel 718 Processed by Additive Manufacturing: Crystallographic Texture, Anisotropy of Microstructure and Mechanical Properties, Mater. Des., 2017, 114, p 441–449.10.1016/j.matdes.2016.10.075 ↗
16. A.A. Popovich, V.S. Sufiiarov, I.A. Polozov and E.V. Borisov, Microstructure and mechanical properties of inconel 718 produced by SLM and subsequent heat treatment, Key Engineering Materials, Vol 651, Trans Tech Publications Ltd., Switzerland, 2015, p 665–670
17. W.M. Tucho, P. Cuvillier, A. Sjolyst-Kverneland and V. Hansen, Microstructure and Hardness Studies of Inconel 718 Manufactured by Selective Laser Melting Before and After Solution Heat Treatment, Mater. Sci. Eng. A., 2017, 689, p 220–232.10.1016/j.msea.2017.02.062 ↗
18. D. Zhang, W. Niu, X. Cao and Z. Liu, Effect of Standard Heat Treatment on the Microstructure and Mechanical Properties of Selective Laser Melting Manufactured Inconel 718 Superalloy, Mater. Sci. Eng. A., 2015, 644, p 32–40.10.1016/j.msea.2015.06.021 ↗
19. J. Li, Z. Zhao, P. Bai, H. Qu, B. Liu, L. Li, L. Wu, R. Guan, H. Liu and Z. Guo, Microstructural Evolution and Mechanical Properties of IN718 Alloy Fabricated by Selective Laser Melting Following Different Heat Treatments, J. Alloy Compd., 2019, 772, p 861–870.10.1016/j.jallcom.2018.09.200 ↗
20. J.-P. Choi, G.-H. Shin, S. Yang, D.-Y. Yang, J.-S. Lee, M. Brochu and J.-H. Yu, Densification and Microstructural Investigation of Inconel 718 Parts Fabricated by Selective Laser Melting, Powder Technol., 2017, 310, p 60–66.10.1016/j.powtec.2017.01.030 ↗
21. J.H. Yi, J.W. Kang, T.J. Wang, X. Wang, Y.Y. Hu, T. Feng, Y.L. Feng and P.Y. Wu, Effect of Laser Energy Density on the Microstructure, Mechanical Properties, and Deformation of Inconel 718 Samples Fabricated by Selective Laser Melting, J. Alloy Compd., 2019, 786, p 481–488.10.1016/j.jallcom.2019.01.377 ↗
22. E. Chlebus, K. Gruber, B. Kuźnicka, J. Kurzac and T. Kurzynowski, Effect of Heat Treatment on the Microstructure and Mechanical Properties of Inconel 718 Processed by Selective Laser Melting, Mater. Sci. Eng. A, 2015, 639, p 647–655.10.1016/j.msea.2015.05.035 ↗
23. S. Holland, X. Wang, X.Y. Fang, Y.B. Guo, F. Yan and L. Li, Grain Boundary Network Evolution in Inconel 718 From Selective Laser Melting to Heat Treatment, Mater. Sci. Eng. A, 2018, 725, p 406–418.10.1016/j.msea.2018.04.045 ↗
24. S. Holland, X. Wang, J. Chen, W. Cai, F. Yan and L. Li, Multiscale Characterization of Microstructures and Mechanical Properties of Inconel 718 Fabricated by Selective Laser Melting, J. Alloy Compd., 2019, 784, p 182–194.10.1016/j.jallcom.2018.12.380 ↗
25. J. Schneider, B. Lund and M. Fullen, Effect of Heat Treatment Variations on the Mechanical Properties of Inconel 718 Selective Laser Melted Specimens, Addit. Manuf., 2018, 21, p 248–254.
26. W. Huang, J. Yang, H. Yang, G. Jing, Z. Wang and X. Zeng, Heat Treatment of Inconel 718 Produced by Selective Laser Melting: Microstructure and Mechanical Properties, Mater. Sci. Eng. A, 2019, 750, p 98–107.10.1016/j.msea.2019.02.046 ↗
27. G.H. Cao, T.Y. Sun, C.H. Wang, X. Li, M. Liu, Z.X. Zhang, P.F. Hu, A.M. Russell, R. Schneider, D. Gerthsen, Z.J. Zhou, C.P. Li and G.F. Chen, Investigations of γ′, γ″ and δ Precipitates in Heat-Treated Inconel 718 Alloy Fabricated by Selective Laser Melting, Mater. Charact., 2018, 136, p 398–406.10.1016/j.matchar.2018.01.006 ↗
28. Z.Y. Zhao, P.K. Bai, W.B. Du, B. Liu, D. Pan, R. Das, C.T. Liu and Z.H. Guo, An Overview of Graphene and Its Derivatives Reinforced Metal Matrix Composites: Preparation, Properties and Applications, Carbon, 2020, 170, p 302–326.10.1016/j.carbon.2020.08.040 ↗
29. M. Oyesola, K. Mpofu and N. Mathe, A Techno-Economic Analytical Approach of Laser-Based Additive Manufacturing Processes for Aerospace Application, Procedia Manuf., 2019, 35, p 155–163.10.1016/j.promfg.2019.05.019 ↗
30. Z.Y. Zhao, L.Z. Zhang, P.K. Bai, W.B. Du, S.W. Wang, X.Y. Xu, Q.N. Dong, Y.X. Li and B. Han, Tribological Behavior of In Situ TiC/Graphene/Graphite/Ti6Al4V Matrix Composite Through Laser Cladding, Acta Metall. Sin. (Engl. Lett.), 2021, 34, p 1317–1330. https://doi.org/10.1007/s40195-021-01215-3.10.1007/s40195-021-01215-3 ↗
31. H. Qi, M. Azer and A. Ritter, Studies of Standard Heat Treatment Effects on Microstructure and Mechanical Properties of Laser Net Shape Manufactured INCONEL 718, Metall. Mater. Trans. A, 2009, 40, p 2410–2422.10.1007/s11661-009-9949-3 ↗
32. S. Ghosh, S. Yadav and G. Das, Study of Standard Heat Treatment on Mechanical Properties of Inconel 718 using Ball Indentation Technique, Mater. Lett., 2008, 62, p 2619–2622.10.1016/j.matlet.2008.01.001 ↗
33. S.D. Jadhav, S. Dadbakhsh, L. Goossens, J.P. Kruth, J. Van Humbeeck and K. Vanmeensel, Influence of Selective Laser Melting Process Parameters on Texture Evolution in Pure Copper, J. Mater. Process. Technol., 2019, 270, p 47–58.10.1016/j.jmatprotec.2019.02.022 ↗
34. P. Liu, J. Hu, S. Sun, K. Feng, Y. Zhang and M. Cao, Microstructural Evolution and Phase Transformation of Inconel 718 Alloys Fabricated by Selective Laser Melting Under Different Heat Treatment, J. Manuf. Process., 2019, 39, p 226–232.10.1016/j.jmapro.2019.02.029 ↗
35. F. Liu, X. Lin, G. Yang, M. Song, J. Chen and W. Huang, Microstructure and Residual Stress of Laser Rapid Formed Inconel 718 Nickel-Base Superalloy, Opt. Laser Technol., 2011, 43, p 208–213.10.1016/j.optlastec.2010.06.015 ↗
36. Z. Wang, K. Guan, M. Gao, X. Li, X. Chen and X. Zeng, The Microstructure and Mechanical Properties of Deposited-IN718 by Selective Laser Melting, J. Alloy Compd., 2012, 513, p 518–523.10.1016/j.jallcom.2011.10.107 ↗
37. C. Slama and M. Abdellaoui, Structural Characterization of the Aged Inconel 718, J. Alloy Compd., 2000, 306, p 277–284.10.1016/S0925-8388(00)00789-1 ↗
38. Y.C. Lin, J. Deng, Y. Jiang, D. Wen and G. Liu, Effects of Initial δ Phase on Hot Tensile Deformation Behaviors and Fracture Characteristics of a Typical Ni-Based Superalloy, Mater. Sci. Eng. A, 2014, 598, p 251–262.10.1016/j.msea.2014.01.029 ↗
39. T. Rong, D. Gu, Q. Shi, S. Cao and M. Xia, Effects of Tailored Gradient Interface on Wear Properties of WC/Inconel 718 Composites Using Selective Laser Melting, Surf. Coat. Technol., 2016, 307, p 418–427.10.1016/j.surfcoat.2016.09.011 ↗