Assessment of Microstructural Evolution and Mechanical Properties of Laser Metal Deposited 316L Stainless Steel
Source abstract
Abstract
Laser metal deposition (LMD) method is considered as a promising additive manufacturing technique owing to its advanced features. This includes printing complex shaped structures via three-dimensional computer-aided-designs, laser cladding and rapid prototyping. In the present study, detailed microstructure-property correlation is pursued for a block of 316L stainless steel alloy, manufactured by LMD. Presence of fully austenitic phase with corresponding residual stresses in the as-built structure is observed through x-ray diffraction analysis. At the first hand, detailed microstructural analysis is done at the bottom and top sections of the block along the build direction. Presence of hatch structures, variation in the layer thickness along with non-uniformity in the grain size and morphology are noted at these sections. An enhancement in the layer thickness and residual stress along with coarsened grain size is noted to exist towards the top section. This is particularly reflected in achieving highest localized hardness at the bottom section, which progressively decreases towards the top, as characterized through nano-indentation. The LMD-manufactured 316L SS alloy however, exhibits strong indentation size effect along with higher global hardness and strengths with respect to the as-cast alloys. This is primarily related to the complex thermal history of the AM technique. Standard solution heat treatment of the LMD-manufactured 316L SS alloy although coarsens the grain size, minimizes the microstructural non-uniformities and residual stress. Such increment in grain size however, leads to reduction in hardness at the macro, micro- and nano-levels, in comparison to the as-built counterparts. Tensile tests of the solutionized 316L alloys reveal a reduction in yield and ultimate tensile strength along with increased ductility and toughness, thereby suggesting solution treatment as a useful measure to optimize the combination of properties. Importantly, the properties are noted to supersede those of the wrought alloys.
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Research context
OpenAlex topics: Additive Manufacturing Materials and Processes · High Entropy Alloys Studies · Welding Techniques and Residual Stresses
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References (68)
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1. M. Odnobokova, A. Kipelova, A. Belyakov and R. Kaibyshev, Microstructure Evolution in a 316L Stainless Steel Subjected to Multidirectional Forging and Unidirectional Bar Rolling, IOP Conf. Ser Mater. Sci. Eng., 2014, 63(1), p 012060.10.1088/1757-899X/63/1/012060 ↗
2. R.B. Song, J.Y. Xiang and D.P. Hou, Characteristics of Mechanical Properties and Microstructure for 316L Austenitic Stainless Steel, J. Iron Steel Res. Int., 2011, 18(11), p 53–59.10.1016/S1006-706X(11)60117-9 ↗
3. F.P. De Moraes, S.F. Alves, R.L. Plaut and A.F. Padilha, Degradation of Microstructure and Properties of an AISI 316L Steel Pipe after More than 100,000 Hours Usage at 640°C in a Petrochemical Industry, Procedia Struct. Integr., 2019, 17, p 131–137.10.1016/j.prostr.2019.08.018 ↗
4. T. Hryniewicz, K. Rokosz and M. Filippi, Biomaterial Studies on AISI 316L Stainless Steel After Magnetoelectropolishing, Materials (Basel), 2009, 2(1), p 129–145.10.3390/ma2010129 ↗
5. W.E. Frazier, Metal Additive Manufacturing: A Review, J. Mater. Eng. Perform., 2014, 23(6), p 1917–1928.10.1007/s11665-014-0958-z ↗
6. A. Ramakrishnan and G.P. Dinda, Microstructure and Mechanical Properties of Direct Laser Metal Deposited Haynes 282 Superalloy, Mater. Sci. Eng. A, 2019, 748, p 347–356.10.1016/j.msea.2019.01.101 ↗
7. N. Shamsaei, A. Yadollahi, L. Bian and S.M. Thompson, An Overview of Direct Laser Deposition for Additive Manufacturing; Part II: Mechanical Behavior, Process Parameter Optimization and Control, Addit. Manuf., 2015, 8, p 12–35.
8. A.K. Matta, D. Ranga Raju and K.N.S. Suman, The Integration of CAD/CAM and Rapid Prototyping in Product Development: A Review, Mater. Today Proc., 2015, 2(4–5), p 3438–3445.10.1016/j.matpr.2015.07.319 ↗
9. P. Sreeramagiri, A. Bhagavatam, A. Ramakrishnan, H. Alrehaili and G.P. Dinda, Design and Development of a High-Performance Ni-Based Superalloy WSU 150 for Additive Manufacturing, J. Mater. Sci. Technol., 2020, 47, p 20–28.10.1016/j.jmst.2020.01.041 ↗
10. P. Guo, B. Zou, C. Huang and H. Gao, Study on Microstructure, Mechanical Properties and Machinability of Efficiently Additive Manufactured AISI 316L Stainless Steel by High-Power Direct Laser Deposition, J. Mater. Process. Technol., 2017, 240, p 12–22.10.1016/j.jmatprotec.2016.09.005 ↗
11. M. Mukherjee, Effect of Build Geometry and Orientation on Microstructure and Properties of Additively Manufactured 316L Stainless Steel by Laser Metal Deposition, Materialia, 2019, 7, p 100359.10.1016/j.mtla.2019.100359 ↗
12. E. Salsi, M. Chiumenti and M. Cervera, Modeling of Microstructure Evolution of Ti6Al4V for Additive Manufacturing, Metals (Basel), 2018, 8(8), p 633.10.3390/met8080633 ↗
13. D.R. Feenstra, V. Cruz, X. Gao, A. Molotnikov and N. Birbilis, Effect of Build Height on the Properties of Large Format Stainless Steel 316L Fabricated via Directed Energy Deposition, Addit. Manuf., 2020, 34, p 101205.
14. M.J. Zhan, G.F. Sun, Z.D. Wang, X.T. Shen, Y. Yan and Z.H. Ni, Numerical and Experimental Investigation on Laser Metal Deposition as Repair Technology for 316L Stainless Steel, Opt. Laser Technol., 2019, 118, p 84–92.10.1016/j.optlastec.2019.05.011 ↗
15. P.J. Withers and H.K.D.H. Bhadeshia, Residual Stress Part 2—Nature and Origins, Mater. Sci. Technol., 2001, 17(4), p 366–375.10.1179/026708301101510087 ↗
16. A. Saboori, G. Piscopo, M. Lai, A. Salmi and S. Biamino, An Investigation on the Effect of Deposition Pattern on the Microstructure, Mechanical Properties and Residual Stress of 316L Produced by Directed Energy Deposition, Mater. Sci. Eng. A, 2020, 780, p 139179.10.1016/j.msea.2020.139179 ↗
17. W. Chen, T. Voisin, Y. Zhang, J. Florien, C.M. Spadaccini, D.L. Mcdowell, T. Zhu and Y.M. Wang, Microscale Residual Stresses in Additively Manufactured Stainless Steel, Nat. Commun., 2019, 10(1), p 1–12.10.1038/s41467-018-07882-8 ↗
18. D. Kong, C. Dong, X. Ni, L. Zhang, J. Yao, C. Man, X. Cheng, K. Xiao and X. Li, Mechanical Properties and Corrosion Behavior of Selective Laser Melted 316L Stainless Steel after Different Heat Treatment Processes, J. Mater. Sci. Technol., 2019, 35(7), p 1499–1507.10.1016/j.jmst.2019.03.003 ↗
19. A. Leicht, U. Klement and E. Hryha, Effect of Build Geometry on the Microstructural Development of 316L Parts Produced by Additive Manufacturing, Mater. Charact., 2018, 143, p 137–143.10.1016/j.matchar.2018.04.040 ↗
20. E. Yasa and J.P. Kruth, Microstructural Investigation of Selective Laser Melting 316L Stainless Steel Parts Exposed to Laser Re-melting, Procedia Eng., 2011, 19, p 389–395.10.1016/j.proeng.2011.11.130 ↗
21. D.J. Rowenhorst, L. Nguyen, A.D. Murphy-Leonard and R.W. Fonda, Characterization of Microstructure in Additively Manufactured 316L Using Automated Serial Sectioning, Curr. Opin. Solid State Mater. Sci., 2020, 24(3), p 100819.10.1016/j.cossms.2020.100819 ↗
22. N. Kurgan, Effect of Porosity and Density on the Mechanical and Microstructural Properties of Sintered 316L Stainless Steel Implant Materials, Mater. Des., 2014, 55, p 235–241.10.1016/j.matdes.2013.09.058 ↗
23. F. Bartolomeu, M. Buciumeanu, E. Pinto, N. Alves, O. Carvalho, F.S. Silva and G. Miranda, 316L Stainless Steel Mechanical and Tribological Behavior—A Comparison between Selective Laser Melting, Hot Pressing and Conventional Casting, Addit. Manuf., 2017, 16, p 81–89.
24. S. Kheiri, H. Mirzadeh and M. Naghizadeh, Tailoring the Microstructure and Mechanical Properties of AISI 316L Austenitic Stainless Steel via Cold Rolling and Reversion Annealing, Mater. Sci. Eng. A, 2019, 759, p 90–96.10.1016/j.msea.2019.05.028 ↗
25. A. Ascari, A.H.A. Lutey, E. Liverani and A. Fortunato, Laser Directed Energy Deposition of Bulk 316L Stainless Steel, Lasers Manuf. Mater. Process., 2020, 7(4), p 426–448.10.1007/s40516-020-00128-w ↗
26. Q. Porter, J. Morrow and C. Ma, Selective Laser Melting of 316L Stainless Steel: Homogeneity of Thermal History, Microstructure, and Mechanical Properties, Int. J. Adv. Manuf. Technol., 2020, 111(11–12), p 3343–3350.10.1007/s00170-020-06308-4 ↗
27. T. Simson, A. Emmel, A. Dwars and J. Böhm, Residual Stress Measurements on AISI 316L Samples Manufactured by Selective Laser Melting, Addit. Manuf., 2017, 17, p 183–189.
28. B. Blinn, M. Klein, C. Gläßner, M. Smaga, J.C. Aurich and T. Beck, An Investigation of the Microstructure and Fatigue Behavior of Additively Manufactured AISI 316L Stainless Steel with Regard to the Influence of Heat Treatment, Metals (Basel), 2018, 8(4), p 220.10.3390/met8040220 ↗
29. O.O. Salman, C. Gammer, A.K. Chaubey, J. Eckert and S. Scudino, Effect of Heat Treatment on Microstructure and Mechanical Properties of 316L Steel Synthesized by Selective Laser Melting, Mater. Sci. Eng. A, 2019, 748, p 205–212.10.1016/j.msea.2019.01.110 ↗
30. A. Yadollahi, N. Shamsaei, S.M. Thompson and D.W. Seely, Effects of Process Time Interval and Heat Treatment on the Mechanical and Microstructural Properties of Direct Laser Deposited 316L Stainless Steel, Mater. Sci. Eng. A, 2015, 644, p 171–183.10.1016/j.msea.2015.07.056 ↗
31. X. Zhang, M.D. McMurtrey, L. Wang, R.C. O’Brien, C.H. Shiau, Y. Wang, R. Scott, Y. Ren and C. Sun, Evolution of Microstructure, Residual Stress, and Tensile Properties of Additively Manufactured Stainless Steel Under Heat Treatments, JOM, 2020, 72(12), p 4167–4177.10.1007/s11837-020-04433-9 ↗
32. ASTM E3–95, Standard Practice for Preparation of Metallographic Specimens, ASTM Int., 2016, 82(C), p 1–15.
33. ASTM E8, ASTM E8/E8M Standard Test Methods for Tension Testing of Metallic Materials, Annu. B. ASTM Stand., 2010, 4(C), p 1–27.
34. R. Casati, J. Lemke and M. Vedani, Microstructure and Fracture Behavior of 316L Austenitic Stainless Steel Produced by Selective Laser Melting, J. Mater. Sci. Technol., 2016, 32(8), p 738–744.10.1016/j.jmst.2016.06.016 ↗
35. G.F. Sun, X.T. Shen, Z.D. Wang, M.J. Zhan, S. Yao, R. Zhou and Z.H. Ni, Laser Metal Deposition as Repair Technology for 316L Stainless Steel: Influence of Feeding Powder Compositions on Microstructure and Mechanical Properties, Opt. Laser Technol., 2019, 109, p 71–83.10.1016/j.optlastec.2018.07.051 ↗
36. Y. Zhong, L. Liu, S. Wikman, D. Cui and Z. Shen, Intragranular Cellular Segregation Network Structure Strengthening 316L Stainless Steel Prepared by Selective Laser Melting, J. Nucl. Mater., 2016, 470, p 170–178.10.1016/j.jnucmat.2015.12.034 ↗
37. T. Voisin, J.P. Monchoux, M. Hantcherli, S. Mayer, H. Clemens and A. Couret, Microstructures and Mechanical Properties of a Multi-Phase β-Solidifying TiAl Alloy Densified by Spark Plasma Sintering, Acta Mater., 2014, 73, p 107–115.10.1016/j.actamat.2014.03.058 ↗
38. J.P. Monchoux, A. Couret, L. Durand, T. Voisin, Z. Trzaska and M. Thomas, Elaboration of Metallic Materials by SPS: Processing, Microstructures, Properties, and Shaping, Metals (Basel), 2021, 11(2), p 1–20.10.3390/met11020322 ↗
39. T. Voisin, J.B. Forien, A. Perron, S. Aubry, N. Bertin, A. Samanta, A. Baker and Y.M. Wang, New Insights on Cellular Structures Strengthening Mechanisms and Thermal Stability of an Austenitic Stainless Steel Fabricated by Laser Powder-Bed-Fusion, Acta Mater., 2021, 203, p 116476.10.1016/j.actamat.2020.11.018 ↗
40. R.M. Mahamood, Laser Metal Deposition of Metals and Alloys, Laser Metal Deposition Process of Metals Alloys, and Composite Materials. R.M. Mahamood Ed., Springer, Cham, 2018, p 93–11810.1007/978-3-319-64985-6_5 ↗
41. C. Li, Z.Y. Liu, X.Y. Fang and Y.B. Guo, Residual Stress in Metal Additive Manufacturing, Procedia CIRP, 2018, 71, p 348–353.10.1016/j.procir.2018.05.039 ↗
42. V.I. Monine, J. Da Cruz Payão Filho, R.S. Gonzaga, E.K.D. Passos and J.T. De Assis, X-Ray Diffraction Technique for Residual Stress Measurement in NiCrMo Alloy Weld Metal, Adv. Mater. Sci. Eng., 2018, 2018, p 1–10.10.1155/2018/8986423 ↗
43. D. Benjamin and C.W. Kirkpatrick, Properties and Selection: Stainless Steels, Tool Materials and Special Purpose Metals, ASM Int., 1980, 2, p 144.
44. W. Woo, D. Kim, E.J. Kingston, V. Luzin, F. Salvemini and M.R. Hill, Effect of Interlayers and Scanning Strategies on Through-Thickness Residual Stress Distributions in Additive Manufactured Ferritic-Austenitic Steel, Structure, 2019, 744, p 618–629.
45. R.J. Moat, A.J. Pinkerton, L. Li, P.J. Withers and M. Preuss, Residual Stresses in Laser Direct Metal Deposited Waspaloy, Mater. Sci. Eng. A, 2011, 528, p 2288–2298.10.1016/j.msea.2010.12.010 ↗
46. J.J. Yan, D.L. Zheng, H.X. Li, X. Jia, J.F. Sun, Y.L. Li, M. Qian and M. Yan, Selective Laser Melting of H13: Microstructure and Residual Stress, J. Mater. Sci., 2017, 52(20), p 12476–12485.10.1007/s10853-017-1380-3 ↗
47. P. Bian, J. Shi, Y. Liu and Y. Xie, Influence of Laser Power and Scanning Strategy on Residual Stress Distribution in Additively Manufactured 316L Steel, Opt. Laser Technol., 2020, 132, p 106477.10.1016/j.optlastec.2020.106477 ↗
48. A. Du Plessis, S.G.R.A. Beerlink and W.B. Du Preez, Standard Method for MicroCT-Based Additive Manufacturing Quality Control 4: Metal Powder Analysis, MethodsX, 2018, 5, p 1336–1345.10.1016/j.mex.2018.10.021 ↗
49. H. Choo, K. Sham, J. Bohling, A. Ngo, X. Xiao, Y. Ren, P.J. Depond, M.J. Matthews and E. Garlea, Effect of Laser Power on Defect, Texture, and Microstructure of a Laser Powder Bed Fusion Processed 316L Stainless Steel, Mater. Des., 2019, 164, p 107534.10.1016/j.matdes.2018.12.006 ↗
50. G. Kasperovich, J. Haubrich, J. Gussone and G. Requena, Correlation between Porosity and Processing Parameters in TiAl6V4 Produced by Selective Laser Melting, JMADE, 2016, 105, p 160–170.
51. W.E. Luecke and J.A. Slotwinski, Mechanical Properties of Austenitic Stainless Steel Made by Additive Manufacturing, J. Res. Natl. Inst. Stand. Technol., 2014, 119, p 398–418.10.6028/jres.119.015 ↗
52. T.M. Mower and M.J. Long, Materials Science & Engineering A Mechanical Behavior of Additive Manufactured, Powder-Bed Laser-Fused Materials, Mater. Sci. Eng. A, 2016, 651, p 198–213.10.1016/j.msea.2015.10.068 ↗
53. S. Yin, J. Cizek, X. Yan and R. Lupoi, Surface & Coatings Technology Annealing Strategies for Enhancing Mechanical Properties of Additively Manufactured 316L Stainless Steel Deposited by Cold Spray, Surf. Coat. Technol., 2019, 370, p 353–361.10.1016/j.surfcoat.2019.04.012 ↗
54. S. Sujith-Kumar, L. Marandi, V.K. Balla, S. Bysakh, D. Piorunek, G. Eggeler, M. Das and I. Sen, Microstructure–Property Correlations for Additively Manufactured NiTi Based Shape Memory Alloys, Materialia, 2019, 8, p 1004.
55. I.A. Segura, L.E. Murr, C.A. Terrazas, D. Bermudez, J. Mireles, V.S.V. Injeti, K. Li, B. Yu, R.D.K. Misra and R.B. Wicker, Grain Boundary and Microstructure Engineering of Inconel 690 Cladding on Stainless-Steel 316L Using Electron-Beam Powder Bed Fusion Additive Manufacturing, J. Mater. Sci. Technol., 2019, 35(2), p 351–367.10.1016/j.jmst.2018.09.059 ↗
56. G.M. Pharr and W.C. Oliver, Measurement of Thin Film Mechanical Properties Using Nanoindentation, MrS Bull, 1992, 17, p 28–33.10.1557/S0883769400041634 ↗
57. A.C. Fischer-Cripps, Nanoindentation, Springer, New York, 2004.10.1007/978-1-4757-5943-3 ↗
58. C. Tromas, J.C. Stinville, C. Templier and P. Villechaise, Hardness and Elastic Modulus Gradients in Plasma-Nitrided 316L Polycrystalline Stainless Steel Investigated by Nanoindentation Tomography, Acta Mater., 2012, 60(5), p 1965–1973.10.1016/j.actamat.2011.12.012 ↗
59. W.D. Nix and H. Gao, Indentation Size Effects in Crystalline Materials: A Law For Strain Gradient Plasticity, J. Mech. Phys. Solids, 1998, 46(3), p 411–425.10.1016/S0022-5096(97)00086-0 ↗
60. L. Cui, S. Jiang, J. Xu, R. Lin, R. Taherzadeh and J. Moverare, Revealing Relationships between Microstructure and Hardening Nature of Additively Manufactured 316L Stainless Steel, Mater. Des., 2021, 198, p 109385.10.1016/j.matdes.2020.109385 ↗
61. W. Qin, J. Li, Y. Liu, J. Kang, L. Zhu, D. Shu, P. Peng, D. She, D. Meng and Y. Li, Effects of Grain Size on Tensile Property and Fracture Morphology of 316L Stainless Steel, Mater. Lett., 2019, 254, p 116–119.10.1016/j.matlet.2019.07.058 ↗
62. M.A. Melia, J.D. Carroll, S.R. Whetten, S.N. Esmaeely, J. Locke, E. White, I. Anderson, M. Chandross, J.R. Michael, N. Argibay, E.J. Schindelholz and A.B. Kustas, Mechanical and Corrosion Properties of Additively Manufactured CoCrFeMnNi High Entropy Alloy, Addit. Manuf., 2019, 29, p 100833.
63. J. Yu, D. Kim, K. Ha, J.B. Jeon and W. Lee, Strong Feature Size Dependence of Tensile Properties and Its Microstructural Origin in Selectively Laser Melted 316L Stainless Steel, Mater. Lett., 2020, 275, p 128161.10.1016/j.matlet.2020.128161 ↗
64. M.J. Sohrabi, M. Naghizadeh and H. Mirzadeh, Deformation-Induced Martensite in Austenitic Stainless Steels: A Review, Arch. Civ. Mech. Eng., 2020, 20(4), p 1–24.10.1007/s43452-020-00130-1 ↗
65. M. Soleimani, A. Kalhor and H. Mirzadeh, Transformation-Induced Plasticity (TRIP) in Advanced Steels: A Review, Mater. Sci. Eng. A, 2020, 795, p 140023.10.1016/j.msea.2020.140023 ↗
66. M.J. Sohrabi, H. Mirzadeh and C. Dehghanian, Significance of Martensite Reversion and Austenite Stability to the Mechanical Properties and Transformation-Induced Plasticity Effect of Austenitic Stainless Steels, J. Mater. Eng. Perform., 2020, 29(5), p 3233–3242.10.1007/s11665-020-04798-7 ↗
67. W. Bleck, X. Guo and Y. Ma, The TRIP Effect and Its Application in Cold Formable Sheet Steels, Steel Res. Int., 2017, 88(10), p 35–45.10.1002/srin.201700218 ↗
68. D. Gu and H. Chen, Selective Laser Melting of High Strength and Toughness Stainless Steel Parts: The Roles of Laser Hatch Style and Part Placement Strategy, Mater. Sci. Eng. A, 2018, 725, p 419–427.10.1016/j.msea.2018.04.046 ↗