journal article·2020-03Open access

Microstructural Changes in Inconel 625 Alloy Fabricated by Laser-Based Powder Bed Fusion Process and Subjected to High-Temperature Annealing

Kewin Gola, Beata Dubiel, Izabela Kalemba-Rec

Abstract

Abstract The microstructure of the laser powder bed additively manufactured Inconel 625 in post-build stress-relief annealed condition and subsequently annealed at a temperature of 600 °C for 5, 100 and 500 h was investigated by means of light microscopy as well as scanning and transmission electron microscopy. Stress-relieved Inconel 625 exhibited fine cellular–dendritic microstructure characterized by the high dislocation density. Selected area electron diffraction studies allowed to demonstrate that already after 5 h of annealing at a temperature of 600 °C, precipitation of the γ′′ phase in the form of coherent nanoparticles occurred. With the prolongation of the duration of annealing at a temperature of 600 °C from 5 to 500 h, the gradual dissolution of intercellular areas and decrease in the dislocation density were accompanied by enhanced precipitation of the γ′′ phase nanoparticles.
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Research context

OpenAlex topics: Additive Manufacturing Materials and Processes · High Entropy Alloys Studies · Additive Manufacturing and 3D Printing Technologies

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References (31)

Show source-provided references
1. S. Floreen, G.E. Fuchs, and W.J. Yang, Metallurgy of alloy 625, Superalloys 718, 625 and Various Derivatives, E.A. Loria, Ed., The Minerals, Metals and Materials Society, Warrendale, 1994, p 13–3710.7449/1994/Superalloys_1994_13_37 ↗
2. V. Shankar, K.B.S. Rao, and S.L. Mannan, Microstructure and Mechanical Properties of Inconel 625 Superalloy, J. Nucl. Mater., 2001, 228, p 222–23210.1016/S0022-3115(00)00723-6 ↗
3. L.E. Shoemaker, Alloys 625 and 725: Trends in Properties and Applications, Superalloys 718, 625 and Various Derivatives, E.A. Loria, Ed., The Minerals, Metals and Materials Society, Warrendale, 2005, p 409–41810.7449/2005/Superalloys_2005_409_418 ↗
4. J.A. Gonzalez, J. Mireles, S.W. Stafford, M.A. Perez, C.A. Terrazas, and R.B. Wicker, Characterization of Inconel 625 Fabricated Using Powder-Bed-Based Additive Manufacturing Technologies, J. Mater. Process. Technol., 2018, 264, p 200–21010.1016/j.jmatprotec.2018.08.031 ↗
5. E.A. Lass, M.R. Stoudt, M.E. Williams, M.B. Katz, L.E. Levine, T.Q. Phan, T.H. Gnaeupel-Herold, and D.S. Ng, Formation of the Ni3Nb δ-Phase in Stress-Relieved Inconel 625 Produced Via Laser Powder-Bed Fusion Additive Manufacturing, Metall. Mater. Trans., 2017, 48, p 5547–555810.1007/s11661-017-4304-6 ↗
6. A. Kreitcberg, V. Brailovskia, and S. Turenneb, Effect of Heat Treatment and Hot Isostatic Pressing on the Microstructure and Mechanical Properties of Inconel 625 Alloy Processed by Laser Powder Bed Fusion, Mater. Sci. Eng. A, 2017, 689, p 1–1010.1016/j.msea.2017.02.038 ↗
7. E.A. Lass, M.R. Stoudt, M.B. Katz, and M.E. Williams, Precipitation and Dissolution of δ and γ′′ During Heat Treatment of a Laser Powder-Bed Fusion Produced Ni-Based Superalloy, Scr. Mater., 2018, 154, p 83–8610.1016/j.scriptamat.2018.05.025 ↗
8. F. Zhang, L.E. Levine, A.J. Allen, C.E. Campbell, E.A. Lass, S. Cheruvathur, M.R. Stoudt, M.E. Williams, and Y. Idell, Homogenization Kinetics of a Nickel-Based Superalloy Produced by Powder Bed Fusion Laser Sintering, Scr. Mater., 2017, 131, p 98–10210.1016/j.scriptamat.2016.12.037 ↗
9. G. Marchese, M. Lorusso, S. Parizia, E. Bassini, J.-W. Lee, F. Calignano, D. Manfredi, M. Terner, H.-U. Hong, D. Ugues, M. Lombardi, and S. Biamino, Influence of Heat Treatments on Microstructure Evolution and Mechanical Properties of Inconel 625 Processed by Laser Powder Bed Fusion, Mater. Sci. Eng. A, 2018, 729, p 64–7510.1016/j.msea.2018.05.044 ↗
10. K.N. Amato, J. Hernandez, L.E. Murr, E. Martinez, S.M. Gaytan, and P.W. Shindo, Comparison of Microstructures and Properties for a Ni-Base Superalloy (Alloy 625) Fabricated by Electron and Laser Beam Melting, J. Mater. Sci. Res., 2012, 1, p 1–41
11. T. Keller, G. Lindwall, S. Ghosh, L. Ma, B.M. Lane, F. Zhang, U.R. Kattner, E.A. Lass, J.C. Heigel, Y. Idell, M.E. Williams, A.J. Allen, J.E. Guyer, and L.E. Levine, Application of Finite Element, Phase-Field, and CALPHAD-Based Methods to Additive Manufacturing of Ni-Based Superalloy, Acta Mater., 2017, 139, p 244–25310.1016/j.actamat.2017.05.003 ↗
12. F. Zhang, L.E. Levine, A.J. Allen, M.R. Stoudt, G. Lindwall, E.A. Lass, M.E. Williams, Y. Idell, and C.E. Campbell, Effect of Heat Treatment on the Microstructural Evolution of a Nickel-Based Superalloy Additive-Manufactured by Laser Powder Bed Fusion, Acta Mater., 2018, 152, p 200–21410.1016/j.actamat.2018.03.017 ↗
13. C. Li, R. White, X.Y. Fang, M. Weaver, and Y.B. Gu, Microstructure Evolution Characteristics of Inconel 625 Alloy from Selective Laser Melting to Heat Treatment, Mater. Sci. Eng. A, 2017, 705, p 20–3110.1016/j.msea.2017.08.058 ↗
14. A. Kruse, A. Krupka, V. Schwarzkopf, C. Gamard, and T. Henningsen, Influence of Proteins on Hydrothermal Gasification and Liquefaction of Biomass. 2. Model Compounds, Ind. Eng. Chem. Res., 2007, 46, p 87–9610.1021/ie061047h ↗
15. S. Saka and D. Kusdiana, Biodiesel Fuel from Rapeseed Oil as Prepared in Supercritical Methanol, Fuel, 2001, 80, p 225–23110.1016/S0016-2361(00)00083-1 ↗
16. K. Özdenkçi, C. De Blasio, G. Sarwar, K. Melin, J. Koskinen, and V. Alopaeus, Techo-Economic Feasibility of Supercritical Water Gasification of Black Liquor, Energy, 2019, 189, p 11628410.1016/j.energy.2019.116284 ↗
17. R.K. Ham, The Determination of Dislocation Densities in Thin Films, Philos. Mag., 1961, 6, p 1183–118410.1080/14786436108239679 ↗
18. M. Calandri, S. Yin, B. Aldwell, F. Calignano, R. Lupoi, and D. Ugues, Texture and Microstructural Features at Different Length Scales in Inconel 718 Produced by Selective Laser Melting, Materials, 2019, 12, p 1–3210.3390/ma12081293 ↗
19. J.P. Kruth, M. Badrossamay, E. Yasa, J. Deckers, L. Thijs, and J. Van Humbeeck, Part and Material Properties in Selective Laser Melting of Metals, in 16th International Symposium on Electromachining, Shangai, China, 19–23 April 2010, Red Hook, NY (2014), pp. 3–14
20. G.P. Dinda, A.K. Dasqupta, and J. Mazumder, Laser Aided Direct Metal Deposition of Inconel 625 Superalloy: Microstructural Evolution and Thermal Stability, Mater. Sci. Eng. A, 2009, 509, p 98–10410.1016/j.msea.2009.01.009 ↗
21. G.K. Dey, S. Albert, D. Srivastava, M. Sundararaman, and P. Mukhopadhyay, Microstructural Studies on Rapidly Solidified Inconel 625, Mater. Sci. Eng. A, 1989, 119, p 175–18410.1016/0921-5093(89)90537-6 ↗
22. L.M. Suave, J. Cornier, P. Villechaise, A. Soula, Z. Hervier, D. Bertheau, and J. Laigo, Microstructural Evolution during Thermal Aging of Alloy 625: Impact of Temperature and Forming Process, Metall. Mater. Trans. A Phys. Metall. Mater. Sci., 2014, 45, p 2963–298210.1007/s11661-014-2256-7 ↗
23. F.J. Rizzo and J. Radavich, Microstructural Characterization of PM 625-Type Materials, Superalloys 718, 625 and Various Derivatives, E.A. Loria, Ed., The Minerals Metals and Materials Society, Warrendale, 1991, p 297–30810.7449/1991/Superalloys_1991_297_308 ↗
24. F. Cortial, J.M. Corrieu, and C. Vernot-Loier, Influence of Heat Treatments on Microstructure, Mechanical Properties, and Corrosion Resistance of Weld Alloy 625, Superalloys 718, 625 and Various Derivatives, E.A. Loria, Ed., The Minerals Metals and Materials Society, Warrendale, 1994, p 859–87010.7449/1994/Superalloys_1994_859_870 ↗
25. X. Xing, X. Di, and B. Wang, The Effect of Post-Weld Heat Treatment Temperature on the Microstructure of Inconel 625 Deposited Metal, J. Alloys Compd., 2014, 593, p 110–11610.1016/j.jallcom.2013.12.224 ↗
26. T.E. Abioye, D.G. McCartney, and A.T. Clare, Laser Cladding of Inconel 625 Wire for Corrosion Protection, J. Mater. Process. Technol., 2015, 217, p 232–24010.1016/j.jmatprotec.2014.10.024 ↗
27. P. Petrzak, K. Kowalski, and M. Blicharski, Analysis of Phase Transformations in Inconel 625 Alloy During Annealing, Acta Phys. Pol. A, 2016, 130, p 1041–104410.12693/APhysPolA.130.1041 ↗
28. B. Dubiel and J. Sieniawski, Precipitates in Additively Manufactured Inconel 625 Superalloy, Materials, 2019, 12, p 1–1110.3390/ma12071144 ↗
29. M. Solecka, A. Kopia, A. Radziszewska, and B. Rutkowski, Microstructure, Microsegregation and Nanohardness of CMT Clad Layers of Ni-Base Alloy on 16Mo3 Steel, J. Alloys Compd., 2018, 751, p 86–9510.1016/j.jallcom.2018.04.102 ↗
30. M. Rozmus-Górnikowska, Ł. Cieniek, M. Blicharski, and J. Kusiński, Microstructure and Microsegregation of an Inconel 625 Weld Overlay Produced on Steel Pipes by the Cold Metall Tranfer Technique, Arch. Metall. Mater., 2014, 59, p 1081–108410.2478/amm-2014-0185 ↗
31. B. Dubiel, A. Kruk, E. Stępniowska, G. Cempura, D. Geiger, P. Formanek, J. Hernandez, P. Midgley, and A. Czyrska-Filemonowicz, TEM, HRTEM, electron holography and electron tomography studies of γ′ and γ′′ nanoparticles in Inconel 718 superalloy, J. Microsc., 2009, 236, p 149–15710.1111/j.1365-2818.2009.03283.x ↗