journal article·2022

Phase separation in alkali silicate glasses detected through inverse Laplace transform of 29 Si nuclear magnetic resonance echo train decay

Mark O. Bovee, Daniel Jardón-Álvarez, Deepansh Srivastava, Jingshi Wu, Philip J. Grandinetti

Journal of Materials Chemistry C· Volume 10· Issue 42
Publisher page

Abstract

The ratio of Si-29 nuclear magnetic resonance coherence lifetimes for Q 4 and Q 3 sites under magic-angle spinning and a π-pulse train in silicate glasses can detect phase separation, even at small scales where the glass appears optically homogenous.
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Research context

OpenAlex topics: NMR spectroscopy and applications · Glass properties and applications · Advanced NMR Techniques and Applications

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

Affiliations

Department of Chemistry, The Ohio State University, 120 W. 18th Avenue, Columbus, Ohio 43210-1173, USA

Science & Technology Division, SP-FR-05, Corning Research and Development Corporation, Corning, NY 14831, USA

Funding

Division of Chemistry · Division of Materials Research

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