article·2006-01-01

Effect of Ultrasonic Field on Preparation of Sb_2O_3 by Neutralization Method

Qiu Ke

Abstract

The preparation of ultrafine cubic Sb_2O_3 was studied by using oxychloride (Sb_4O_5Cl_2) neutralized with ammonia under ultrasonic field.The results show that Sb_2O_3 obtained in the process is cubic crystalline and well-dispersed,which has an average particle size of 0.777μm when the ultrasonic power is 100W,the ultrasonic time is 30min,and the temperature is 20℃.The effects of ultrasonic power,time,ratios of distilled water to oxychloride,and temperature on the crystal structure and particle size of the Sb_2O_3 formed were investigated by means of XRD,SEM and laser sizer.
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OpenAlex topics: Catalysis and Oxidation Reactions · Petroleum Processing and Analysis

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