article·2002-01-01

Solventothermal Synthesis and Characterization of Thiotungstate Crystals at Low Temperature

Yan Dong

Abstract

The tetrathiotungstate crystals (NH4)2WS4 and K2WS4 were first synthesized by the solventothermal technique by using water-alcohol as solvent at low temperature, and characterized by SEM, XRD, ED techniques. Results show that their crystal phases are pure and their shapes are good. The synthesis procedure is simple and high yield, produces less pollution.
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Research context

OpenAlex topics: Organometallic Compounds Synthesis and Characterization · Polyoxometalates: Synthesis and Applications

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