Preparation and Thermal Stability of Ti3SiC2 Ceramics by Polymer Derived Ceramics Method
Source abstract
Abstract
Ti3SiC2 compound can enhance the oxidation resistance of C/C composites as a modifying material t, thanks to its superior high-temperature stability, indicating significant potential for applications.In this work, titanium powder and liquid polycarbosilane (LPCS) were served as starting materials for producing Ti3SiC2 ceramic with four different phase contents by polymer derived ceramics (PDC) method at temperatures of 1200 ℃, 1300 ℃, 1400 ℃ and 1500 ℃, respectively.Effects of sintering temperature on the phase compositions and morphology of the ceramics were studied.Additionally, the
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Research context
OpenAlex topics: MXene and MAX Phase Materials · Advanced materials and composites · Advanced ceramic materials synthesis
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References (17)
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1. SU K, TIAN X K, LI S P, et al. Green synthesis, formation mech anism and oxidation of Ti3SiC2 powder from bamboo charcoal, Ti and Si. Ceramics International, 2023, 49(16):26428.10.1016/j.ceramint.2023.05.179 ↗
2. SU X J, LIU G X, DAI B, et al. Ablation mechanisms of Ti3SiC2 ceramic at 1600 ℃ in nitrogen plasma flame. Ceramics International, 2022, 48(10):14004.10.1016/j.ceramint.2022.01.285 ↗
3. 范晓孟, 殷小玮, 张立同, 等. 液硅渗透法制备Ti3SiC2改性C/C-SiC复合材料. 复合材料学报, 2012, 29(1):104.
4. XU Y L, SUN W, MIAO C M, et al. Ablation properties of C/C-UHTCs and their preparation by reactive infiltration of K2MeF6 (Me = Zr, Ti) molten salt. Journal of the European Ceramic Society, 2021, 41(11):5405.10.1016/j.jeurceramsoc.2021.04.043 ↗
5. JEITSCHKO W, NOWOTNY H. Die kristallstruktur von Ti3SiC2- ein neuer komplexearbid-typ. Monatshefte für Chemie-Chemical Monthly, 1967, 98(2):329.10.1007/BF00899949 ↗
6. BARSOUM M W, FARBER L, El-RAGHY T. Dislocations, kink bands, and room-temperature plasticity of Ti3SiC2. Metallurgical and Materials Transactions A, 1999, 30(7):1727.10.1007/s11661-999-0172-z ↗
7. BARSOUM M W, RADOVIC M. Elastic and mechanical properties of the MAX phases. Annual Review of Materials Research, 2011, 41(1):195.10.1146/annurev-matsci-062910-100448 ↗
8. ZHU J Q, MEI B C, CHEN Y L. Synthesis of Ti3SiC2 by spark plasma sintering (SPS) with the addition of aluminium. Journal of Inorganic Materials, 2003, 18(3):700.
9. YANG J S, ZHANG X Y, WANG Z, et al. Fabrication of Ti3SiC2 powders using TiH2 as the source of Ti. Ceramics International, 2012, 38(4):3509.10.1016/j.ceramint.2011.12.037 ↗
10. PANG W K, LOW I M, O’CONNOR B H, et al. Diffraction study on the thermal stability of Ti3SiC2/TiC/TiSi2 composites in vacuum. AIP Conference Proceedings, 2010, 1202: 44.
11. OO Z, LOW I M, O’CONNOR B H. Dynamic study of the thermal stability of impure Ti3SiC2 in argon and air by neutron diffraction. Physica B Condensed Matter, 2006, 385(1):499.10.1016/j.physb.2006.05.255 ↗
12. SU K, TIAN X K, LI Z Z, et al. Oxidation behavior of Ti3SiC2 powder synthesized by using biochar, Si and Ti. Ceramics International, 2023, 49(3):4863.10.1016/j.ceramint.2022.09.377 ↗
13. SUN Z M, YANG S L, HASHIMOTO H, et al. Ti3SiC2 powder synthesis from Ti/Si/TiC powder mixtures. Ceramics International, 2004, 30(7): 1873.10.1016/j.ceramint.2003.12.052 ↗
14. ZOU Y, SUN Z M, TADA S J. Effect of Al addition on low-temperature synthesis of Ti3SiC2 powder. Journal of Alloys and Compounds, 2008, 461(1):579.10.1016/j.jallcom.2007.07.090 ↗
15. 支艳敏.Ti3SiC2复合陶瓷的制备及其热稳定性的研究. 武汉: 华中科技大学硕士学位论文, 2016.
16. BARSOUM M W, EL-RAGHY T, OGBUJI L U J T. Oxidation of Ti3SiC2 in air. Journal of the Electrochemical Society, 1997, 144(7):2508.10.1149/1.1837846 ↗
17. FENG A, ORLING T, MUNIR Z A. Field-activated pressure- assisted combustion synthesis of polycrystalline Ti3SiC2. Journal of Materials Research, 1999, 14(3):925.10.1557/JMR.1999.0124 ↗