Preparation and Thermal Sensitive Characteristics of the Co0.8Mn0.8Ni0.9Fe0.5O4 Nanometer Powders
Source abstract
Abstract
采用共沉淀法,以NH4HCO3为沉淀剂制备了Co0.8Mn0.8Ni0.9Fe0.5O4 负温度系数(NTC)热敏电阻纳米粉体材料, 研究了不同预烧温度对材料相结构的影响, 探讨了不同烧结工艺对NTC热敏电阻材料微观结构和热敏性能的影响. 采用X射线衍射(XRD)、综合热分析(TG/DTA)、红外(FT-IR)、扫描电子显微技术(SEM)和激光粒度分析仪对制备的样品进行了表征. 结果表明, 750℃预烧后的粉体为纯尖晶石相, 晶粒粒度为32.1nm, 颗粒粒径在50~100nm范围内. 通过对不同烧结程序的对比研究发现, 当烧结程序为:840℃、1200℃各保温2h, 升降温速率为1℃/min时, 样品电学性能较好:ρ25℃=1183Ω·cm, B25/50=3034K. 分析表明, 该烧结程序能有效改善热敏电阻材料的微观结构和热敏性能. 根据ln ρ-1/T曲线斜率计算了经不同工艺烧结后热敏电阻材料的激活能在0.26eV左右.
Source: openalex_inverted_index · Quality: baseline
Research context
OpenAlex topics: Electrical and Thermal Properties of Materials · Ferroelectric and Piezoelectric Materials · Advanced Sensor Technologies Research
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (9)
Show source-provided references
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