journal article·2023Open access

Fabrication of Transparent AlON by Gel Casting and Pressureless Sintering

Xihai JIN, Manjiang DONG, Yanmei KAN, Bo LIANG, Shaoming DONG

Journal of Inorganic Materials· Volume 38· Issue 2

Abstract

Transparent AlON possesses good mechanical and optical properties, which shows great potential for application.However, high fabrication cost seriously restricts its wide usage.To solve this problem, gel-casting and pressureless sintering of transparent AlON was tentatively studied here, with emphasis on low temperature synthesis and anti-hydrolysis treatment of AlON powder.It was found that fine AlON powder could be readily synthesized at a low temperature of 1700 ℃ by a novel carbothermal nitridation technique, using polymer coated AlN/Al 2 O 3 mixture as the starting materials.The powder obtained was submicron in size and its hydrolysis resistance could be significantly improved after surface coating with a polyurethane layer.On the basis of these findings, transparent AlON ceramics was successfully prepared through gel-casting and pressureless sintering.The material sintered at 1850 ℃ showed good optical and mechanical properties, with a high in-line transmittance of 83.1%-86.2%from ultraviolet to mid-infrared and three-point bending strength of 310 MPa.
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Research context

OpenAlex topics: Advanced ceramic materials synthesis · Injection Molding Process and Properties · Additive Manufacturing and 3D Printing Technologies

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