journal article·2019-12

Direct fabrication mechanism of pre-sintered Si3N4 ceramic with ultra-high porosity by laser additive manufacturing

Zheng-Hua Wei, Li-Jin Cheng, Yi-Xin Ma, An-Nan Chen, Xiao-Feng Guo, Jia-Min Wu, Yu-Sheng Shi

Scripta Materialia· Volume 173
Publisher page

Abstract

Abstract Complex structural Si3N4 ceramics with ultra-high porosity were innovatively formed by selective laser sintering (SLS) technology without any binder. Due to rapid cooling rate, the high temperature phase constituent and microstructure of the SLSed Si3N4 poly hollow microspheres (PHMS) were preserved, thus revealing the bonding mechanism of Si3N4 under the nonequilibrium heat source. Si3N4 PHMS are bonded by microvilli composed of bamboo-structure SiO2 nanofiber clusters, stacked SiO2 nanospheres and smooth α-Si3.72N4 nanowires. Finally, the pre-sintered Si3N4 ceramics with a porosity of 80% are directly fabricated in the atmosphere by SLS, which have the enough strength to satisfy the post-treatment requirements.
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Research context

OpenAlex topics: Additive Manufacturing and 3D Printing Technologies · Advanced ceramic materials synthesis · Bone Tissue Engineering Materials

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

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