Noncontact measurement of density and thermal properties of SS 316L powder bed through flash thermography
Source abstract
Abstract
Purpose Powder bed density is a key parameter in powder bed additive manufacturing (AM) processes but is not easily monitored. This research evaluates the possibility of non-invasively estimating the density of an AM powder bed via its thermal properties measured using flash thermography (FT). Design/methodology/approach The thermal diffusivity and conductivity of the samples were found by fitting an analytical model to the measured surface temperature after flash of the powder on a polymer substrate, enabling the estimation of the powder bed density. Findings FT estimated powder bed was within 8% of weight-based density measurements and the inferred thermal properties are consistent with literature findings. However, multiple flashes were necessary to ensure precise measurements due to noise in the experimental data and the similarity of thermal properties between the powder and substrate. Originality/value This paper emphasizes the capability of Flash Thermography (FT) for non-contact measurement of SS 316 L powder bed density, offering a pathway to in-situ monitoring for powder bed AM methods including binder jetting (BJ) and powder bed fusion. Despite the limitations of the current approach, the density knowledge and thermal properties measurements have the potential to enhance process development and thermal modeling powder bed AM processes, aiding in understanding the powder packing and thermal behavior.
Source: crossref · Quality: baseline
Research context
OpenAlex topics: Thermography and Photoacoustic Techniques · Additive Manufacturing and 3D Printing Technologies · Additive Manufacturing Materials and Processes
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (43)
Show source-provided references
1. On the measurement of relative powder-bed compaction density in powder-bed additive manufacturing processes10.1016/j.matdes.2018.06.030 ↗
2. Thermal conductivity of metal powder and consolidated material fabricated via selective laser melting10.4028/www.scientific.net/KEM.523-524.244 ↗
3. Pulsed photothermal modeling of layered materials10.1063/1.336690 ↗
4. Flow behavior of powder particles in layering process of selective laser melting: numerical modeling and experimental verification based on discrete element method10.1016/j.ijmachtools.2017.08.004 ↗
5. Influence of drop velocity and droplet spacing on the equilibrium saturation level in binder jetting
6. Impact of part thickness and drying conditions on saturation limits in binder jet additive manufacturing10.1016/j.addma.2020.101127 ↗
7. Front-flash thermal imaging characterization of continuous fiber ceramic composites
8. Development of methods to identify thermophysical properties of complex media
9. A method for measuring powder bed density in binder jet additive manufacturing process and the powder feedstock characteristics influencing the powder bed density
10. Effect of layer thickness and printing orientation on mechanical properties and dimensional accuracy of 3D printed porous samples for bone tissue engineering10.1371/journal.pone.0108252 ↗
11. Fabrication of barium titanate by binder jetting additive manufacturing technology10.1016/j.ceramint.2015.01.108 ↗
12. Discrete element simulation and experimental study of powder spreading process in additive manufacturing10.1016/j.powtec.2016.11.002 ↗
13. Early-time pulse-echo thermal wave imaging
14. Binding mechanisms in selective laser sintering and selective laser melting10.1108/13552540510573365 ↗
15. Metal binder jetting additive manufacturing: a literature review
16. Investigation the effect of particle size distribution on processing parameters optimisation in selective laser melting process
17. In-situ lock-in thermographic measurement of powder layer thermal diffusivity and thickness in laser powder bed fusion10.1016/j.addma.2023.103726 ↗
18. Nondestructive evaluation of materials by infrared thermography
19. Effect of fine powder particles on quality of binder jetting parts10.1016/j.addma.2020.101587 ↗
20. Binder jet 3D printing–process parameters, materials, properties, modeling, and challenges10.1016/j.pmatsci.2020.100707 ↗
21. Application of flash-pulse thermography methods for quantitative thickness inspection of coatings made by different thermal spraying technologies10.1016/j.surfcoat.2020.126748 ↗
22. Flash method of determining thermal diffusivity, heat capacity, and thermal conductivity10.1063/1.1728417 ↗
23. Impact of pulse length on the accuracy of defect depth measurements in pulse thermography
24. Non-destructive evaluation (NDE) of aerospace composites: flaw characterisation
25. 1998
26. Multilayer material characterization using thermographic signal reconstruction
27. Reconstruction and enhancement of active thermographic image sequences10.1117/1.1566969 ↗
28. Solutions, M. (2014), “EOS M 290 The additive manufacturing system for the production of serial components, spare parts and functional prototypes directly in metal. [online]”, available at: https://engineering.cmu.edu/next/_files/documents/eos-m-290-description.pdf.
29. Method for determining defect depth using thermal imaging
30. Analysis of pulsed thermography methods for defect depth prediction10.1115/1.2165211 ↗
31. 2010
32. Pulsed thermal imaging measurement of thermal properties for thermal barrier coatings based on a multilayer heat transfer model10.1115/1.4027551 ↗
33. 2012
34. A review of process development steps for new material systems in three dimensional printing (3DP)10.1016/j.jmapro.2009.03.002 ↗
35. Defect measurement limits using flash thermography with application to additive manufacturing10.1016/j.ndteint.2022.102615 ↗
36. Sinter structure analysis of titanium structures fabricated via binder jetting additive manufacturing10.1016/j.matdes.2018.06.038 ↗
37. Reconstruction of size and depth of simulated defects in austenitic steel plate using pulsed infrared thermography10.1016/j.infrared.2012.02.004 ↗
38. 3-dimensional heat transfer modeling for laser powder-bed fusion additive manufacturing with volumetric heat sources based on varied thermal conductivity and absorptivity10.1016/j.optlastec.2018.08.012 ↗
39. Improved non-destructive testing of carbon fiber reinforced polymer (CFRP) composites using pulsed thermograph10.1016/j.polymertesting.2015.06.016 ↗
40. Binder jetting: a review of process, materials, and methods10.1016/j.addma.2019.05.031 ↗
41. Binder-jet printing of fine stainless steel powder with varied final density10.1007/s11837-016-2177-6 ↗
42. AISI Type 316L Stainless Steel (2024), “Annealed sheet [online]”, available at: www.matweb.com/search/datasheet_print.aspx?matguid=1336be6d0c594b55afb5ca8bf1f3e042.
43. SANDVIK (2022), “osprey® 316l for additive manufacturing ”, [Online], available at: www.metalpowder.sandvik/siteassets/metal-powder/datasheets/osprey-316l-am-austenitic-stainless-steels.pdf.