journal article·2025-01

Low-temperature thermal reduction synthesis of nano-structured TiC via TiO2-template growth method

Zhenye Jiang, Na Kong, Haoyuan Xu, Yonggang Wei, Bo Li

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Abstract

Titanium carbide has attracted much attention as a transition metal carbide. This study proposed a novel method for the preparation of different-morphology nano TiC materials by direct carbothermal reduction of TiO 2. TiO 2 raw materials with different morphologies were used as template and titanium source, and highly reactive CaC 2 was served as reducing and carbonizing agents. TiC nano materials with the morphologies of particle, rod and line were successfully prepared at a low temperature of 1000 ℃ for 2 h under vacuum condition, which well inherited the morphologies of TiO 2. Moreover, the prepared different-morphology TiC materials showed total electromagnetic shielding effectiveness of higher than 60 dB, demonstrating the potential application of the different-morphology TiC in the field of electromagnetic interference shielding. This study proposes a new method for the TiC preparation under conditions of significantly lowered reduction temperature and time, and provides a new nano TiC formation path which is controlled by the "titanium template generation" mechanism.
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Research context

OpenAlex topics: Advanced materials and composites · MXene and MAX Phase Materials · Aluminum Alloys Composites Properties

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

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