Anti-oxidative quartz/carbon-braided fiber reinforced ceramizable composites modified with B4C and AlB2: Mechanical robustness, phase evolution and anti-oxidation mechanism
Source abstract
Abstract
Carbon fiber reinforced ceramizable phenolic resin matrix composites (C f/CPR) have been widely used in the field of thermal protection materials. However, the industrial application of the C f/CPR is restricted by its easy oxidation failure under high temperature condition. In this work, a novel antioxidative ceramizable composites modified with AlB 2 and B 4C (C f-Q f/CPR) were prepared by using quartz fiber-coated carbon fiber (C f-Q f) as reinforcements via co-weaving technique. The thermal stability, mechanical properties, interfacial phase evolution and anti-oxidation mechanism of the composites were investigated. The residue yield and the flexural strength of the composites after treatment at 1200°C for 15 min were 93.4 % and 62.4 MPa, increased by 5.4 % and 67.3 % compared with those of C f/CPR. Quartz fiber and ceramic protective layer showed synergistic effect to improve the oxidation resistance of carbon fiber and PyC, confirming good high temperature mechanical properties and oxidation resistance of as-received composites.
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Research context
OpenAlex topics: Advanced ceramic materials synthesis · Fiber-reinforced polymer composites · Flame retardant materials and properties
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (43)
Show source-provided references
1. Advanced sandwich structures for thermal protection systems in hypersonic vehicles: a review10.1016/j.compositesb.2021.109301 ↗
2. Thermal protection systems for space vehicles: a review on technology development, current challenges and future prospects10.1016/j.actaastro.2020.06.047 ↗
3. Science and technology of polymeric ablative materials for thermal protection systems and propulsion devices: a review10.1016/j.pmatsci.2016.08.003 ↗
4. Modifying effects of in-situ grown LaB6 on composition, microstructure and ablation property of C/C-SiC-ZrC composites10.1016/j.corsci.2022.110672 ↗
5. A novel ablative material for thermal protection system: carbon fiber/polysiloxane composites10.1016/j.ast.2022.107822 ↗
6. Ablative type composites based on phenolic Resin/Nano-silicon carbide matrix reinforced by carbon fiber felt
7. Oxidation and ablation behaviors of carbon fiber/phenolic resin composites modified with borosilicate glass and polycarbosilane interface10.1016/j.jallcom.2020.154277 ↗
8. Effects of carbon nanotubes and carbon fiber reinforcements on thermal conductivity and ablation properties of carbon/phenolic composites10.1016/j.compositesb.2014.06.022 ↗
9. Geem, Decomposition of carbon/phenolic composites for aerospace heatshields: detailed speciation of phenolic resin pyrolysis products10.1016/j.ast.2021.107079 ↗
10. Thermal and mechanical properties of phenolic-based composites reinforced by carbon fibres and multiwall carbon nanotubes10.1016/j.compositesa.2015.01.015 ↗
11. Advances in antioxidation coating materials for carbon/carbon composites10.1016/j.jallcom.2021.161143 ↗
12. High temperature flexural strength, microstructure, phase evolution and anti-oxidation mechanism of Al-coated carbon fiber/boron phenolic resin ceramizable composite modified with TiB2 and B4C10.1016/j.ceramint.2023.05.029 ↗
13. Carbon fiber reinforced ultra-high temperature ceramic matrix composites: a review10.1016/j.ceramint.2019.05.065 ↗
14. Micro/nano multiscale reinforcing strategies toward extreme high-temperature applications: take carbon/carbon composites and their coatings as the examples10.1016/j.jmst.2021.03.076 ↗
15. Effect of carbon nanotubes and silicon carbide particles on ablative properties of carbon fiber phenolic matrix composites10.1016/j.vacuum.2017.11.013 ↗
16. A comparative study on the effect of carbon-based and ceramic additives on the properties of fiber reinforced polymer matrix composites for high temperature applications10.1016/j.ceramint.2021.08.356 ↗
17. Thermal properties and oxidative corrosion behaviour of HfB2-SiB6 ceramicizable phenolic resin matrix composites10.1016/j.corsci.2023.111340 ↗
18. Improved ablation resistance of carbon-phenolic composites by introducing zirconium diboride particles10.1016/j.compositesb.2012.11.007 ↗
19. Influence of ZrB nanoparticles on the mechanical and thermal behaviors of carbon nanotube reinforced resol composite10.1016/j.jmst.2016.03.021 ↗
20. Improved high-temperature mechanical property of carbon-phenolic composites by introducing titanium diboride particles10.1016/j.compositesb.2018.08.124 ↗
21. Effects of SiC content on mechanical, thermal and ablative properties of carbon/phenolic composites10.1016/j.ceramint.2020.03.170 ↗
22. Ceramizable phenolic adhesive modified by different inorganic particles: a comparative study of thermal stability, bonding strength and bonding mechanism10.1016/j.jeurceramsoc.2022.09.034 ↗
23. Oxidation and ablation behavior of a ceramizable resin matrix composite based on carbon fiber/phenolic resin
24. Time-dependent high-temperature compressive failure behavior of high-silica/boron-phenolic composites modified with boron carbide and talc10.1016/j.compscitech.2021.109226 ↗
25. Enhancement of the interlaminar performance of silica/phenolic laminates after high-temperature pyrolysis using a boron carbide/silicon carbide fibre z-pin10.1016/j.matdes.2022.110770 ↗
26. Factors affecting SiC-ZrO-MoSi2/Ni antioxidation coating made by composite plating on carbon fibres10.1080/17436753.2019.1612658 ↗
27. ZrO2f-coated Cf hybrid fibrous reinforcements and properties of their reinforced ceramicizable phenolic resin matrix composites10.1016/j.jeurceramsoc.2020.08.034 ↗
28. Electron-configuration stabilized (W,Al)B solid solutions10.1016/j.actamat.2019.05.056 ↗
29. ZrB2 ceramics doped with AlB210.1016/j.ceramint.2014.01.037 ↗
30. Boride phase formation in the production of Al-B master alloys10.1016/j.jallcom.2017.06.107 ↗
31. Effect of B4C on the microstructure and properties of B4C modified three-dimensional needled C/C-SiC composites10.1016/j.msea.2017.09.008 ↗
32. Effect of B4C on co-sintering of SiC ceramic membrane10.1016/j.ceramint.2018.11.065 ↗
33. Crystallization of quartz glass fibers during the drawing process10.1021/acs.cgd.5b00253 ↗
34. Impact of drawing stress on the tensile strength of oxide glass fibers10.1111/j.1551-2916.2010.03879.x ↗
35. Effect of medium-high temperature conditioning on the mechanical properties of single quartz fibres10.1016/j.jeurceramsoc.2023.07.048 ↗
36. Modeling initial stage of phenolic pyrolysis: graphitic precursor formation and interfacial effects10.1016/j.polymer.2010.11.018 ↗
37. Study on the pyrolysis of phenol-formaldehyde (PF) resin and modified PF resin10.1016/j.tca.2009.07.012 ↗
38. Quantitative determination of species production from phenol-formaldehyde resin pyrolysis10.1016/j.polymdegradstab.2014.12.020 ↗
39. Effects of nano-ZrSi2 on thermal stability of phenolic resin and thermal reusability of quartz–phenolic composites10.1515/ntrev-2022-0140 ↗
40. A novel Ti3SiC2-CaB6 modified Al-coated carbon fiber/boron phenolic resin ceramizable composite (ACF/BPRC) with excellent long-term oxidative corrosion resistance and high temperature load-bearing capacity
41. Enhancing oxidation resistance of carbon fibre reinforced phenolic composites by ZrO2 nanoparticles through out-of-autoclave vacuum infusion10.1016/j.compositesa.2024.108071 ↗
42. Thermal properties, oxidation corrosion behavior, and the in situ ceramization mechanism of SiB6@BPR/HF composites under high-temperature corrosion10.1016/j.corsci.2021.109913 ↗
43. Biased referencing experiments for the XPS analysis of non-conducting materials10.1016/0169-4332(86)90001-2 ↗