journal article·2023-10Open access

Grain boundary serration tuning and its effect on hot workability of a wrought superalloy

Tso-Wei Chen, Pei-Te Wang, Yung-Chang Kang, Bo-Cheng Wu, Nien-Ti Tsou, Uwe Glatzel, Stéphane Gorsse, An-Chou Yeh

Abstract

This study aims to elucidate the underlying mechanism of grain boundary serration and investigate its effects on hot workability of U720Li superalloy. Industrial scale as-cast ingots were subjected to heat treatments at 1180 °C followed by different cooling rates (15 °C/s, 0.1 °C/s, 0.02 °C/s and 0.003 °C/s) prior hot deformation. With 15 °C/s fast cooling, samples possessed straight boundaries and fine L1 2 structured γ’ particles dispersion. When the cooling rate was decreased to 0.1 °C/s and below, continuous and discontinuous precipitation of the γ` phase led to the formations of Type-I and Type-II grain boundary serrations, respectively. Lamellar γ/γ’ behind the mobile grain boundary was observed for Type-II boundary, which exhibited larger degree of undulation than that of Type-I boundary. With increasing fractions of Type-II boundary, the hot formability of U720Li was significantly improved during compression tests at 1000 °C; 70 % reduction ratio (true strain=1.2) could be achieved without crack formation. This work presents a simple process route to improve the hot deformability of U720Li fabricated on an industrial scale.
Source: expertdata · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: High Temperature Alloys and Creep · Nuclear Materials and Properties · Microstructure and mechanical properties

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (48)

Show source-provided references
1. The interactions between fatigue, creep and environmental damage in Ti 6246 and Udimet 720Li10.1016/j.ijfatigue.2005.06.029 ↗
2. High temperature low cycle fatigue behaviour of UDIMET 720 Li superalloy10.1016/S0142-1123(02)00043-9 ↗
3. Development of Udimet 720 for high strength disk applications
4. Oxidation behavior of several chromia-forming commercial nickel-base superalloys10.1007/BF02134783 ↗
5. The manufacture and evaluation of a large turbine
6. Ni-based superalloys for turbine discs10.1007/s11837-999-0005-y ↗
7. R. Couturier, H. Burlet, S. Terzi, S. Dubiez, L. Guetaz, G. Raisson, Process Development and Mechanical Properties of Alloy U720LI for High Temperature Turbine Disks, In: Proceedings of the Tenth International Symposium on Superalloys,[S. l.][sn], (2004) 351–359.10.7449/2004/Superalloys_2004_351_359 ↗
8. Hot deformation behavior of nickel-based superalloy GH4720Li10.1016/S1006-706X(12)60023-5 ↗
9. Hot deformation behavior and processing workability of a Ni-based alloy10.1016/j.jallcom.2018.08.010 ↗
10. Role of carbides on hot deformation behavior and dynamic recrystallization of hard-deformed superalloy U720Li10.1016/j.msea.2021.141293 ↗
11. Microstructure evolution and processing map of superalloy GH720Li during isothermal compression10.4028/www.scientific.net/MSF.747-748.588 ↗
12. An optimization method of upsetting process for homogenized, nickel-based superalloy Udimet 720Li ingot considering both cracking and recrystallization10.1016/j.jmatprotec.2019.01.013 ↗
13. Deformation characteristics of isothermally forged UDIMET 720 nickel-base superalloy10.1007/s11661-005-0284-z ↗
14. Effect of cooling rate on gleeble hot ductility of UDIMET alloy 720 billet
15. M. Zhao, H. Hu, L. Rong, Heat treatment method for realizing grain boundary sawtooth of iron-nickel-based alloy, in, Institute of Metal Research of CAS, China, 2019.
16. On the mechanism of serrated grain boundary formation in Ni-based superalloys10.1016/0001-6160(83)90202-X ↗
17. Serrated grain boundary formation potential of Ni-based superalloys and its implications10.1007/BF02656707 ↗
18. On the formation of serrated grain boundaries and fan type structures in an advanced polycrystalline nickel-base superalloy10.1016/j.jmatprotec.2008.03.008 ↗
19. On the formation of irregular-shaped gamma prime and serrated grain boundaries in a nickel-based superalloy during continuous cooling10.1016/j.matchar.2012.11.012 ↗
20. Effects of serrated grain boundaries on the crack growth in austenitic heat-resisting steels during high-temperature creep10.1007/BF01106799 ↗
21. Formation and application of grain boundary serrations10.1179/cmq.1995.34.3.219 ↗
22. The effect of grain boundary serration on creep resistance in a wrought nickel-based superalloy10.1016/j.msea.2009.03.071 ↗
23. Effect of serrated grain boundaries on the creep property of Inconel 718 superalloy10.1016/j.msea.2011.10.014 ↗
24. Effect of serrated grain boundary on stress corrosion cracking of alloy 60010.1016/j.net.2018.05.009 ↗
25. Formation of serrated grain boundaries and their effect on the mechanical properties in a P/M nickel base superalloy
26. Grain boundary serration in nickel-based superalloy inconel 600: generation and effects on mechanical behavior10.1007/s11661-018-4671-7 ↗
27. Microstructure and mechanical property development in superalloy U720LI
28. Controlling the grain boundary morphology and secondary γ′ precipitate size distribution in Ni-base superalloys10.1016/j.jallcom.2018.10.031 ↗
29. Fiji: an open-source platform for biological-image analysis10.1038/nmeth.2019 ↗
30. Atomsk: a tool for manipulating and converting atomic data files10.1016/j.cpc.2015.07.012 ↗
31. DREAM.3D: a digital representation environment for the analysis of microstructure in 3D10.1186/2193-9772-3-5 ↗
32. Second nearest-neighbor modified embedded-atom-method potential10.1103/PhysRevB.62.8564 ↗
33. Molecular dynamics for near melting temperatures simulations of metals using modified embedded-atom method10.1016/j.jpcs.2017.09.001 ↗
34. Fast parallel algorithms for short-range molecular dynamics10.1006/jcph.1995.1039 ↗
35. Visualization and analysis of atomistic simulation data with OVITO–the Open Visualization Tool
36. Extracting dislocations and non-dislocation crystal defects from atomistic simulation data10.1088/0965-0393/18/8/085001 ↗
37. Structural characterization of deformed crystals by analysis of common atomic neighborhood10.1016/j.cpc.2007.05.018 ↗
38. Heat treatment of UDIMET 720Li: the effect of microstructure on properties10.1016/S0921-5093(98)00867-3 ↗
39. Discontinuous reactions in solids10.1179/095066001101528402 ↗
40. On the competition between continuous and discontinuous precipitations in binary Mg-Al alloys
41. Competition between continuous and discontinuous precipitation in L12-strengthened high-entropy alloys10.1016/j.intermet.2022.107655 ↗
42. Thermo-Calc & DICTRA, computational tools for materials science10.1016/S0364-5916(02)00037-8 ↗
43. Mechanisms of formation of serrated grain boundaries in nickel base superalloys
44. The mechanism of ductility dip cracking in nickel-chromium alloys: subsolidus cracking results from global stresses produced during fusion welding and local stresses generated when coherent or partially coherent second phases form
45. The growth of γ’ precipitates in nickel-base superalloys10.1016/0001-6160(83)90062-7 ↗
46. Observations of cellular transformation products in nickel-base superalloys10.1007/BF00737041 ↗
47. On the prediction of the yield stress of unimodal and multimodal γ’ Nickel-base superalloys10.1016/j.actamat.2015.07.048 ↗
48. Modeling material properties of lead-free solder alloys10.1007/s11664-007-0218-1 ↗