Continuous precipitation behavior of Mg17Al12 phase during multiple steps of twinning-aging procedure in Mg-Al alloys

Twinning was regarded as an effective way to modify the precipitation in Mg alloys. Two procedures were designed to illustrate twinning-aging consequence on Mg ₁₇Al ₁₂ phase evolution. The effect of multiple steps of twinning-precipitation on the morphology and density of the continuous precipitates inside the twins and the matrix were comprehensively analyzed through phase-orientation related observation. The results show the shape of precipitates in twins was similar to that in the matrix as the CPs mostly lay on the basal planes with an asymmetric-lozenges shape. The CPs were remarkably refined and its density became much higher inside twins. Moreover, the aspect ratio of the CP plates in twins was around 45% of that in the matrix, which means the CPs inside twins became more globular. The precipitation behavior of Mg ₁₇Al ₁₂ phase inside double extension twins was different from the primary twin or the matrix. The Mg ₁₇Al ₁₂ phases lay on both basal and prismatic planes can be observed in double twins of two-step precipitation. The growth behavior of pre-precipitates in twins is different from those in the matrix. The growth rate along its thickness became higher than that in the matrix, which is probably related to dislocation-assisted diffusion at the basal plane.