Microstructures and mechanical properties of Mg-6Gd-1Er-0.5Zr alloy sheets produced with different rolling temperatures
Source abstract
Abstract
Abstract In this study, we investigated the microstructures and mechanical properties of Mg-6Gd-1Er-0.5Zr (GE61K) sheets. The results show that the rolling temperature has a remarkable influence on microstructures, age-hardening responses and mechanical properties of GE61K sheets. The microstructures varies with the increase in rolling temperatures, i.e. microstructures were dominated by the mixture of dynamic recrystallized (DRXed) grains and un-DRXed grains at 300 °C, by DRXed grains at 350 °C, and by un-DRXed grains at 400 °C and 450 °C. Rolling at 300 °C leads to a formation of the bimodal microstructure which contains equilibrium Mg5(Gd, Er) precipitates and a large number of dislocations. These dislocations leads to a formation of novel chain-like precipitates which comprise dominant β', β′F (or β′T), tail-like “hexagonal ring” layers, individual “zig-zag” chain and individual “hexagonal ring”, eventually improving age-hardening responses. The chain-like precipitates are beneficial for achieving a good strength-ductility balance by dividing the matrix into nano-scale units and forming subsequent honeycomb structures. As a result, the R-300 °C sheet shows good mechanical properties, i.e. ultimate tensile strength (UTS) of 367 ± 3 MPa, yield strength (YS) of 349 ± 4 MPa and elongation (EL) of 9.1 ± 1.5%, respectively. However, such strength-ductility balance is destroyed sharply as soon as the rolling temperature increases to 400 °C because of the microstructure variations.
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Research context
OpenAlex topics: Magnesium Alloys: Properties and Applications · Aluminum Alloys Composites Properties · Hydrogen Storage and Materials
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (56)
Show source-provided references
1. Gd-Mg (gadolinium-magnesium), Gd-Mg (gadolinium-magnesium)
2. Microstructure evolution in isochronally heat treated Mg-Gd alloys10.1002/(SICI)1521-396X(199910)175:2<491::AID-PSSA491>3.0.CO;2-F ↗
3. Microstructure evolution in a Mg-15Gd-0.5Zr (wt%) alloy during isothermal aging at 250 °C10.1016/j.msea.2006.06.018 ↗
4. Structural changes of precipitates in an Mg–5 at%Gd alloy studied by transmission electron microscopy10.2320/matertrans.48.10 ↗
5. Effects of precipitate shape and orientation on dispersion strengthening in magnesium alloys10.1016/S1359-6462(02)00497-9 ↗
6. Development of high-strength magnesium alloys via combined processes of extrusion, rolling and ageing10.1016/j.scriptamat.2011.01.042 ↗
7. Achieving high strength-ductility in a wrought Mg-9Gd-3Y-0.5Zr alloy by modifying with minor La addition10.1016/j.jallcom.2021.161062 ↗
8. Towards strength-ductility synergy through a novel technique of multi-pass lowered-temperature drawing in AZ31 magnesium alloys10.1016/j.jallcom.2021.159604 ↗
9. Effects of pre-annealing on microstructure and mechanical properties of as-extruded Mg-Gd-Y-Zn-Zr alloy
10. High strength and ductility Mg-8Gd-3Y-0.5Zr alloy with bimodal structure and nano-precipitates10.1016/j.jmst.2019.10.024 ↗
11. Obtaining ultra-high strength and ductility in a Mg–Gd–Er–Zn–Zr alloy via extrusion, pre-deformation and two-stage aging10.1007/s40195-020-01132-x ↗
12. A simulation study of β1 precipitation on dislocations in an Mg–rare earth alloy10.1016/j.actamat.2014.04.054 ↗
13. Dislocations-induced precipitates and their effect on mechanical properties of Mg-Gd-Y-Zr alloy10.1016/j.jma.2019.05.009 ↗
14. On the possibility to reduce ECAP deformation temperature in magnesium: deformation behavior, dynamic recrystallization and mechanical properties10.1016/j.msea.2021.141103 ↗
15. Development of low-alloyed and rare-earth-free magnesium alloys having ultra-high strength10.1016/j.actamat.2018.03.002 ↗
16. Correlation of plastic deformation and dynamic recrystallization in magnesium alloy ZK6010.1016/S1359-6454(01)00020-9 ↗
17. Unveiling the formation of basal texture variations based on twinning and dynamic recrystallization in AZ31 magnesium alloy during extrusion10.1016/j.actamat.2018.07.014 ↗
18. Orientation dependent slip and twinning during compression and tension of strongly textured magnesium AZ31 alloy10.1016/j.msea.2010.02.008 ↗
19. Twinning, dynamic recovery and recrystallization in hot worked MgeAleZn alloy10.1016/S0921-5093(02)00007-2 ↗
20. The synergy effect of fine and coarse grains on enhanced ductility of bimodal-structured Mg alloys10.1016/j.jallcom.2018.11.229 ↗
21. Ductility improvement of Mg alloys by solid solution: ab initio modeling, synthesis and mechanical properties10.1016/j.actamat.2014.02.011 ↗
22. Effect of rolling passes on the microstructures and mechanical properties of Mg-Gd-Y-Zr alloy sheets10.1016/j.msea.2014.09.018 ↗
23. Development of extraordinary high-strength-toughness Mg alloy via combined processes of repeated plastic working and hot extrusion10.1016/j.msea.2013.02.030 ↗
24. Remarkably enhanced mechanical properties of Mg-8Gd-1Er-0.5Zr alloy on the route of extrusion, rolling and aging10.1016/j.matlet.2017.10.003 ↗
25. Dynamic precipitation and recrystallization in Mg-9 wt%Al during equal-channel angular extrusion: a comparative study to conventional aging10.1016/j.actamat.2019.04.046 ↗
26. Grain refinement of magnesium alloys by zirconium: formation of equiaxed grains10.1016/j.scriptamat.2005.11.002 ↗
27. Precipitation in Mg-Gd-Y-Zr alloy: atomic-scale insights into structures and transformations10.1016/j.matchar.2016.04.015 ↗
28. Precipitation evolution and hardening in Mg-Sm-Zn-Zr alloys10.1016/j.actamat.2016.03.068 ↗
29. Solute clusters and GP zones in binary Mg-RE alloys10.1016/j.actamat.2015.12.047 ↗
30. A detailed HAADF-STEM study of precipitate evolution in Mg-Gd alloy10.1016/j.jallcom.2018.10.193 ↗
31. Formation of and interaction between β′F and β′ phases in a Mg-Gd alloy10.1016/j.jallcom.2017.04.004 ↗
32. Mechanical properties of Mg-8Gd-3Y-0.5Zr alloy with bimodal grain size distributions10.1016/j.jma.2017.09.004 ↗
33. Bimodally grained microstructure development during hot extrusion of Mg-2.4Zn-0.1Ag-0.1 Ca-0.16Zr (at%) alloys10.1016/j.actamat.2009.07.057 ↗
34. Mechanical properties of nanocrystalline materials10.1016/j.pmatsci.2005.08.003 ↗
35. Effects of extrusion ratio and temperature on the mechanical properties and microstructure of as-extruded Mg-Gd-Y-(Nd/Zn)-Zr alloys10.1016/j.msea.2019.138080 ↗
36. Twinning and the ductility of magnesium alloys: Part I: “tension” twins10.1016/j.msea.2006.12.037 ↗
37. Activation mode dependent {1 0ī 2} twinning characteristics in a polycrystalline magnesium alloy10.1016/j.scriptamat.2009.10.027 ↗
38. Microstructure and mechanical properties of AZX912 magnesium alloy extruded at different temperatures10.1016/j.msea.2016.10.032 ↗
39. Fabrication of Mg-Al-Zn-Mn alloy sheets with homogeneous fine-grained structures using high strain-rate rolling in a wide temperature range10.1016/j.msea.2012.09.022 ↗
40. Effects of different stretching routes on microstructure and mechanical properties of AZ31B magnesium alloy sheets10.1016/j.jmst.2015.07.011 ↗
41. Effect of rolling speeds on texture modification and mechanical properties of the AZ31 sheet by a combination of equal channel angular rolling and continuous bending at high temperature10.1016/j.jallcom.2018.07.242 ↗
42. Improved stretch formability of AZ31 sheet via texture control by introducing a continuous bending channel into equal channel angular rolling10.1016/j.jmatprotec.2018.05.012 ↗
43. Improving strength and formability of rolled AZ31 sheet by two-step twinning deformation10.1007/s11837-019-03894-x ↗
44. Effect of pre-straining on twinning, texture and mechanical behavior of magnesium alloys A–review10.1016/j.jmrt.2020.10.023 ↗
45. Effect of Y for enhanced age hardening response and mechanical properties of Mg–Gd–Y–Zr alloys10.1016/j.msea.2006.11.096 ↗
46. Characterization of precipitate phases in a Mg–Dy-Gd-Nd alloy10.1016/j.jallcom.2006.08.059 ↗
47. A super high-strength Mg-Gd-Y-Zn-Mn alloy fabricated by hot extrusion and strain aging10.1016/j.matdes.2019.107666 ↗
48. Microstructures and mechanical properties of the Mg–8Gd–4Y–Nd–Zn–3Si (wt%) alloy10.1016/j.msea.2013.01.056 ↗
49. J. Effects of Nd addition on the microstructure and mechanical properties of extruded Mg-6Gd-2.5Y-0.5Zr alloy10.1007/s11665-017-3089-5 ↗
50. Effect of hot-rolling on microstructures and mechanical properties of extruded mg-6Gd-3.2Y-xZn-0.5Zr sheet10.1007/s11665-012-0238-8 ↗
51. Effect of pre-deformation on microstructure and mechanical properties of WE43 magnesium alloy10.1016/j.msea.2017.02.082 ↗
52. Effect of thermo-mechanical treatment on the microstructure and mechanical properties of a Mg–6Gd–2Nd–0.5Zr alloy10.1016/j.msea.2006.11.033 ↗
53. Enhanced age hardening response and creep resistance of Mg–Gd alloys containing Zn10.1016/j.scriptamat.2005.07.004 ↗
54. Precipitation in a Mg–10Gd–3Y–0.4Zr (wt%) alloy during isothermal ageing at 250 °C10.1016/j.jallcom.2005.11.046 ↗
55. A simulation study of the distribution of β′ precipitates in a crept Mg-Gd-Zr alloy10.1016/j.commatsci.2016.12.021 ↗
56. Physical metallurgy of light alloys