journal article·2024-09Open access

Process window and mechanical properties for thin magnesium- and zinc-wires in dieless wire drawing

Merle Braatz, Jan Bohlen, Noomane Ben Khalifa

Abstract

Abstract Due to their biodegradable properties, magnesium- and zinc-based alloys are in the focus of interest for numerous medical applications, e.g. in the form of thin wires. To achieve improved processability by using hot forming and to obtain higher diameter reductions per pass, the dieless wire drawing process is presented in this paper. In order to investigate the processability and the resulting mechanical properties, a selection of magnesium- and zinc-alloys as well as process parameters are chosen, and wire manufacturing is carried out using the dieless drawing process. The resulting process windows and mechanical properties for the selected materials are discussed. It is found that the length of the forming zone is an important indicator for the process window and the cross-sectional area reduction accuracy in the dieless wire drawing process. Furthermore, process parameter variations result in a distinct variation of the mechanical properties of the wires, whereas process temperatures close to the wire extrusion temperature result in mechanical properties similar to the as-extruded wires. Good localization of the deformation is found for forming zones of 25–75 mm length at elevated temperatures and cross-sectional area reductions of up to 30% are possible for Z1 and ZX10 in one drawing step. Graphical Abstract
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Research context

OpenAlex topics: Magnesium Alloys: Properties and Applications · Aluminum Alloys Composites Properties · Aluminum Alloy Microstructure Properties

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References (62)

Show source-provided references
1. Braatz M, Bohlen J, Ben Khalifa N (2024) Experimental and Numerical Investigation of the Forming Zone in Dieless Wire Drawing Process of Thin Biometallic Wires, in Proceedings of the 14th International Conference on the Technology of Plasticity - Current Trends in the Technology of Plasticity. pp. 479–490. https://doi.org/10.1007/978-3-031-41023-9_4910.1007/978-3-031-41023-9_49 ↗
2. Tiernan P, Hillery MT (2008) An analysis of wire manufacture using the dieless drawing method. J Manuf Process 10(1):12–20. https://doi.org/10.1016/j.manpro.2008.05.00110.1016/j.manpro.2008.05.001 ↗
3. Weiss V, Kot RA (1969) Die-less wire drawing with transformation plasticity. Wire J 2(9):182–189
4. Sekiguchi H, Kobatake K (1977) An analysis of temperature distribution in continuous dieless drawing. Nara Natl Coll Technol Res Bull 13:47–53
5. Naughton MD, Tiernan P (2007) Requirements of a dieless wire drawing system. J Mater Process Technol 191(1–3):310–313. https://doi.org/10.1016/j.jmatprotec.2007.03.05410.1016/j.jmatprotec.2007.03.054 ↗
6. Dodyim N et al (2020) Drawing of magnesium fine wire and medical application of drawn wire. Procedia Manuf 50:271–275. https://doi.org/10.1016/j.promfg.2020.08.05010.1016/j.promfg.2020.08.050 ↗
7. Ohno A et al (1982) New Tapered-Rod forming process for Coil Springs. SAE Tech Paper 820130:471–478. https://doi.org/10.4271/82013010.4271/820130 ↗
8. Hongyu W et al (2018) Analysis and study of dieless drawing process for rod based on radial direction gradient slab method. Int J Adv Manuf Technol 98(1–4):839–847. https://doi.org/10.1007/s00170-018-2282-510.1007/s00170-018-2282-5 ↗
9. Seitz J-M et al (2011) The manufacture of Resorbable suture material from Magnesium - drawing and stranding of thin wires. Adv Eng Mater 13(12):1087–1095. https://doi.org/10.1002/adem.20110015210.1002/adem.201100152 ↗
10. Tiernan P, Hillery MT (2004) Dieless wire drawing - an experimental and numerical analysis. J Mater Process Technol 155:1178–1183. https://doi.org/10.1016/j.jmatprotec.2004.04.17510.1016/j.jmatprotec.2004.04.175 ↗
11. Furushima T, Hirose S, Manabe K-i (2009) Effective temperature distribution and drawing speed control for stable Dieless drawing process of metal tubes. J Solid Mech Mater Eng 3(2):236–246. https://doi.org/10.1299/jmmp.3.23610.1299/jmmp.3.236 ↗
12. Milenin A et al (2018) Computer aided design of the laser dieless drawing process of tubes from magnesium alloy with take into account ductility of the material. Proc 17th Int Conf Metal Form Metal Form 2018 15:302–310. https://doi.org/10.1016/j.promfg.2018.07.22310.1016/j.promfg.2018.07.223 ↗
13. Furushima T, Manabe K (2009) Finite element Simulation with coupled Thermo-Mechanical analysis of Superplastic Dieless Tube drawing considering strain rate sensitivity. Mater Trans 50(1):161–166. https://doi.org/10.2320/matertrans.P-MRA200883710.2320/matertrans.P-MRA2008837 ↗
14. Milenin A et al (2014) Computer aided design of Wires Extrusion from biocompatible Mg-Ca Magnesium Alloy. Arch Metall Mater 59(2):551–556. https://doi.org/10.2478/amm-2014-009110.2478/amm-2014-0091 ↗
15. Furushima T, Manabe K (2007) Experimental and numerical study on deformation behavior in dieless drawing process of superplastic microtubes. J Mater Process Technol 191(1–3):59–63. https://doi.org/10.1016/j.jmatprotec.2007.03.08410.1016/j.jmatprotec.2007.03.084 ↗
16. Fortunier R, Sassoulas H, Montheillet F (1997) A thermo-mechanical analysis of stability in dieless wire drawing. Int J Mech Sci 39(5):615–627. https://doi.org/10.1016/s0020-7403(96)00060-410.1016/s0020-7403(96)00060-4 ↗
17. Pawelski O, Kolling A (1995) Calculation of the temperature distribution in dieless drawing. Steel Res 66(2):50–54. https://doi.org/10.1002/srin.19950108710.1002/srin.199501087 ↗
18. Weidig U, Steinhoff K (2008) Neue Perspektiven und Anwendungen für das frei Längen, in Umformtechnik im Spannungsfeld zwischen Plastomechanik und Werkstofftechnik, K. Steinhoff and R. Knopp, Editors. Grips media GmbH: Bad Harburg. pp. 217–231
19. Wengenroth W, Pawelski O, Rasp W (2001) Theoretical and experimental investigations into dieless drawing. Steel Res 72(10):402–405. https://doi.org/10.1002/srin.20010014110.1002/srin.200100141 ↗
20. He Y et al (2011) Processing limit maps for the stable deformation of dieless drawing. Int J Minerals Metall Mater 18(3):330–337. https://doi.org/10.1007/s12613-011-0443-810.1007/s12613-011-0443-8 ↗
21. Hwang Y-M, Liu H-H, Wang Y-T (2022) Investigations of Formability and Dynamic Recrystallization Development of Titanium alloys during Dieless Wire drawing processes. Steel Res Int 94(2). https://doi.org/10.1002/srin.20220011310.1002/srin.202200113 ↗
22. von Eynatten K, Reissner JN (2004) Dieless Drawing for Flexible Processing of Microstructure and Mechanical Properties, in Proceedings of the 34th International MATADOR Conference, S. Hinduja, Editor. Springer: London. pp. 187–192. https://doi.org/10.1007/978-1-4471-0647-0_2810.1007/978-1-4471-0647-0_28 ↗
23. Braatz M, Bohlen J, Ben Khalifa N (2022) Process Stability and Reproducibility of the Dieless drawing process for AZ31 magnesium wires. Key Eng Mater 926:389–400. https://doi.org/10.4028/p-lm7s8y10.4028/p-lm7s8y ↗
24. Kustra P et al (2023) Novel drawing technology for high area reduction manufacturing of ultra-thin brass wires. Archives Civil Mech Eng 23(3). https://doi.org/10.1007/s43452-023-00677-910.1007/s43452-023-00677-9 ↗
25. Li K (2018) Liu. Metal Flow Law of Variable Diameter Metal Wire during die drawing. CMC 2017. Springer, Singapore. DOI. https://doi.org/10.1007/978-981-13-0107-0_56.10.1007/978-981-13-0107-0_56 ↗
26. Kishimoto T, Du P, Furushima T (2022) Effect of microstructure on outer surface roughening of magnesium alloy tubes in die-less mandrel drawing. J Magnesium Alloys 10(10):2730–2744. https://doi.org/10.1016/j.jma.2022.02.00110.1016/j.jma.2022.02.001 ↗
27. Kishimoto T, Furushima T (2023) Achieving thin wall and high surface quality of magnesium alloy tubes in combined process of hollow sinking after die-less mandrel drawing. IntJ Mater Form 16(3). https://doi.org/10.1007/s12289-023-01750-710.1007/s12289-023-01750-7 ↗
28. Milenin A et al (2020) Production of zinc wire for use as a high strength biodegradable surgical threads. Procedia Manuf 50:757–760. https://doi.org/10.1016/j.promfg.2020.08.13610.1016/j.promfg.2020.08.136 ↗
29. Milenin A et al (2021) Mechanical properties, crystallographic texture, and in vitro bio-corrosion of low-alloyed Zn-Mg, produced by hot and cold drawing for biodegradable surgical wires. Archives Civil Mech Eng 21(4). https://doi.org/10.1007/s43452-021-00311-610.1007/s43452-021-00311-6 ↗
30. Seitz J-M et al (2010) The manufacture of Resorbable suture material from Magnesium. Adv Eng Mater 12(11):1099–1105. https://doi.org/10.1002/adem.20100019110.1002/adem.201000191 ↗
31. Mei D et al (2021) Corrosion behavior of mg wires for ureteral stent in artificial urine solution. Corros Sci 189:109567. https://doi.org/10.1016/j.corsci.2021.10956710.1016/j.corsci.2021.109567 ↗
32. Champagne S et al (2019) In Vitro Degradation of Absorbable Zinc Alloys in Artificial urine. Mater (Basel) 12(2). https://doi.org/10.3390/ma1202029510.3390/ma12020295 ↗
33. Venezuela J, Dargusch MS (2019) The influence of alloying and fabrication techniques on the mechanical properties, biodegradability and biocompatibility of zinc: a comprehensive review. Acta Biomater 87:1–40. https://doi.org/10.1016/j.actbio.2019.01.03510.1016/j.actbio.2019.01.035 ↗
34. Hirsch J, Al-Samman T (2013) Superior light metals by texture engineering: optimized aluminum and magnesium alloys for automotive applications. Acta Mater 61(3):818–843. https://doi.org/10.1016/j.actamat.2012.10.04410.1016/j.actamat.2012.10.044 ↗
35. Yoshida K, Koiwa A (2011) Cold drawing of Magnesium Alloy tubes for Medical. J Solid Mech Mater Eng 5(12):1071–1078. https://doi.org/10.1299/jmmp.5.107110.1299/jmmp.5.1071 ↗
36. Nienaber M et al (2022) Property profile development during wire extrusion and wire drawing of magnesium alloys AZ31 and ZX10. Mater Design 224. https://doi.org/10.1016/j.matdes.2022.11135510.1016/j.matdes.2022.111355 ↗
37. Zander D, Zumdick NA (2015) Influence of ca and zn on the microstructure and corrosion of biodegradable Mg–Ca–Zn alloys. Corros Sci 93:222–233. https://doi.org/10.1016/j.corsci.2015.01.02710.1016/j.corsci.2015.01.027 ↗
38. Li Z et al (2008) The development of binary Mg-Ca alloys for use as biodegradable materials within bone. Biomaterials 29(10):1329–1344. https://doi.org/10.1016/j.biomaterials.2007.12.02110.1016/j.biomaterials.2007.12.021 ↗
39. Meza-García E et al (2015) Influence of alloying elements and extrusion process parameter on the recrystallization process of Mg-Zn alloys. Mater Today: Proc 2:S19–S25. https://doi.org/10.1016/j.matpr.2015.05.00410.1016/j.matpr.2015.05.004 ↗
40. Li H et al (2016) The influence of Zn Content on the corrosion and wear performance of Mg-Zn-Ca Alloy in simulated body fluid. J Mater Eng Perform 25(9):3890–3895. https://doi.org/10.1007/s11665-016-2207-010.1007/s11665-016-2207-0 ↗
41. Zhang BP, Wang Y, Geng L (2011) Research on Mg-Zn-Ca Alloy as Degradable Biomaterial, in Biomaterials—Physics and Chemistry, R. Pignatello, Editor. In Tech: Zurich. pp. 183–20410.5772/23929 ↗
42. Bakhsheshi-Rad HR et al (2012) Relationship between the corrosion behavior and the thermal characteristics and microstructure of Mg–0.5Ca–xZn alloys. Corros Sci 64:184–197. https://doi.org/10.1016/j.corsci.2012.07.01510.1016/j.corsci.2012.07.015 ↗
43. Rad HRB et al (2012) Microstructure analysis and corrosion behavior of biodegradable Mg–Ca implant alloys. Mater Design 33:88–97. https://doi.org/10.1016/j.matdes.2011.06.05710.1016/j.matdes.2011.06.057 ↗
44. Palai D et al (2022) Influence of copper on the Microstructural, Mechanical, and Biological properties of commercially pure Zn-Based alloys for a potential biodegradable Implant. ACS Biomaterials Sci Eng 8(4):1443–1463. https://doi.org/10.1021/acsbiomaterials.1c0111110.1021/acsbiomaterials.1c01111 ↗
45. Tang Z et al (2017) Potential biodegradable Zn-Cu binary alloys developed for cardiovascular implant applications. J Mech Behav Biomed Mater 72:182–191. https://doi.org/10.1016/j.jmbbm.2017.05.01310.1016/j.jmbbm.2017.05.013 ↗
46. Nienaber M et al (2020) On the direct extrusion of Magnesium wires from Mg-Al-Zn Series alloys. Metals 10(9). https://doi.org/10.3390/met1009120810.3390/met10091208 ↗
47. Braatz M et al (2022) Experimental Setup of Dieless Drawing Process for Magnesium Wire, in Production at the Leading Edge of Technology. pp. 38–46. https://doi.org/10.1007/978-3-030-78424-9_510.1007/978-3-030-78424-9_5 ↗
48. Tools K (2023) Emissivity Chart for Metal Materials
49. Carolan R, Tiernan P (2009) Computer controlled system for dieless drawing of tool steel bar. J Mater Process Technol 209(7):3335–3342. https://doi.org/10.1016/j.jmatprotec.2008.07.04810.1016/j.jmatprotec.2008.07.048 ↗
50. Furushima T, Ikeda T, Manabe K (2011) Deformation and Heat Transfer Analysis for high speed Dieless drawing of AZ31 Magnesium Alloy tubes. Adv Mater Res 418–420. https://doi.org/10.4028/www.scientific.net/AMR.418-420.103610.4028/www.scientific.net/AMR.418-420.1036 ↗
51. Snedecor GW, Cochran WG (1989) Statistical methods, vol 1191, 8 edn. Ames, Iowa Iowa state University, 2
52. Kaibyshev R (2012) Dynamic recrystallization in magnesium alloys, in advances in wrought magnesium alloys. Woodhead Publishing 186–225. https://doi.org/10.1533/9780857093844.1.18610.1533/9780857093844.1.186 ↗
53. Izumi S (1987) Non-ferrous metal. The Japan Institute of Metals, pp 108–109
54. Koç E et al (2015) Influence of zinc on the microstructure, mechanical properties and in vitro corrosion behavior of magnesium–zinc binary alloys. J Alloys Compd 648:291–296. https://doi.org/10.1016/j.jallcom.2015.06.22710.1016/j.jallcom.2015.06.227 ↗
55. Chino Y et al (2011) Effects of ca on Tensile properties and Stretch Formability at Room temperature in Mg-Zn and Mg-Al Alloys. Mater Trans 52(7):1477–1482. https://doi.org/10.2320/matertrans.M201104810.2320/matertrans.M2011048 ↗
56. Cano-Castillo G et al (2020) Effect of ca and nd on the microstructural development during dynamic and static recrystallization of indirectly extruded Mg–Zn based alloys. Mater Sci Engineering: A 793. https://doi.org/10.1016/j.msea.2020.13952710.1016/j.msea.2020.139527 ↗
57. Rao KP et al (2018) Review on Hot Working Behavior and Strength of Calcium-Containing Magnesium Alloys. Adv Eng Mater 20(9). https://doi.org/10.1002/adem.20170110210.1002/adem.201701102 ↗
58. Mostaed E et al (2019) Precipitation induced room temperature superplasticity in Zn-Cu alloys. Mater Lett 244:203–206. https://doi.org/10.1016/j.matlet.2019.02.08410.1016/j.matlet.2019.02.084 ↗
59. Goodwin FE (2018) Zinc and Zinc Alloys. Springer handbook of materials data. Springer, Cham, pp 427–438. DOI: https://doi.org/10.1007/978-3-319-69743-7.H. Warlimont and W. Martienssen, Editors10.1007/978-3-319-69743-7 ↗
60. Farge JCT (1965) Recrystallization of zinc alloys. McGill University: Canada
61. Edington JW (1982) Microstructural aspects of superplasticity. Metall Trans A 13(5):703–715. https://doi.org/10.1007/bf0264238410.1007/bf02642384 ↗
62. Bednarczyk W et al (2023) Investigation of slip systems activity and grain boundary sliding in fine-grained superplastic zinc alloy. Archives Civil Mech Eng 23(4). https://doi.org/10.1007/s43452-023-00793-610.1007/s43452-023-00793-6 ↗